CN100341441C - Black tourmaline containing tobacco product and its making method and uses - Google Patents
Black tourmaline containing tobacco product and its making method and uses Download PDFInfo
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- CN100341441C CN100341441C CNB03129331XA CN03129331A CN100341441C CN 100341441 C CN100341441 C CN 100341441C CN B03129331X A CNB03129331X A CN B03129331XA CN 03129331 A CN03129331 A CN 03129331A CN 100341441 C CN100341441 C CN 100341441C
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- cigarette
- aphrizite
- smoking article
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Abstract
The present invention discloses a cigarette product and a preparation method thereof. The cigarette product contains 0.1 to 20 wt% of black tourmalines whose particle diameters are from 0.1 to 100 micrometres; the preparation method comprises the following steps: (a) the black tourmalines are crashed till the particle diameters are from 0.1 to 100 micrometres by stage treatment; (b) the black tourmalines are added into the raw materials of the cigarette product, wherein the black tourmalines account for 0.1 to 20 wt% of the cigarette product; (c) the cigarette product is prepared. The present invention also discloses the functions of the reductions of fume, nicotine and tar content and improvement of mouth feel of the cigarette product.
Description
Technical field
The present invention relates to smoking article, particularly contain the smoking article of aphrizite.Also relate to its preparation method and be used to reduce smoking nicotine, reduce tar content and improve the purposes of mouthfeel.
Background technology
As everyone knows, smoking is sizable for the threat of human health.The nicotine that tobacco discharged in smoking process, carbon monoxide, smoking nicotine etc. not only to smoker itself, are very large to environment on every side and involuntary smoker's harm.Effectively reduce these pollutions and harm along with improving constantly of social civilization degree more and more seems most important.
For the aerial release of tar content, CO, smoking nicotine that reduces cigarette, country has formulated certain standard.Tar is to measure by YC/T29, the regulation tar content is low＜and 12.0mg, in＜16.0mg, height＜23.0mg.For human beings'health,, require in the world tar content to be dropped to below the 12.0mg in the end of this century in order to reduce pollution.The atmospheric environment of GB/T16447-1996 tobacco and tobacco product, adjusting and test, GB/T16450-1996 conventional analysis smoking machine, definition and standard conditions.The standard-required carbon monoxide is reduced to＜15.0mg, and the smoking nicotine sense organ is made moderate progress just can illustrate that oneself reduces 0.1mg.
In recent years, there are many researchers to explore for the harmful substance that how to reduce cigarette.For example, CN1252245, Guo Cancheng, on November 23rd, 1999 submitted to, disclosed the method that a kind of biological tobacco reduces tar.This method is to use the metal porphyrins spray solution on pipe tobacco, and the tar of tobacco and pernicious gas CO, NO content are descended.Metal porphyrins is the analog of human-body biological enzyme, can promote BaP and CO, NO to reduce.
Aphrizite contains tens kinds of trace elements of abundant needed by human: magnesium, sulphur, iron, potassium, calcium, sodium, copper, zinc, cobalt, phosphorus, titanium, selenium or the like.Because of the content of magnesium and iron is the highest tourmaline that becomes black.Its chemical constitution more complicated, its chemical general formula are WX
8Y (BO
3)
3Si
6O
18(OH, F)
4, W=Na wherein, K, Ca; X=Mn, Mg, Li, Fe, Al; Y=V, Fe, Cr, Al.Tourmaline capable is used for various fields, for example water activation, sewage disposal, washing, preparation soil and fertilizer etc.At present, the data record is not arranged as yet, tourmaline is used for the tobacco detoxifcation.In.
Summary of the invention
The objective of the invention is to use aphrizite as raw material, cigarette is carried out the anion detoxifcation, the tar in releasing and the reduction cigarette and the method for smoking nicotine, and the product of this method preparation.
One aspect of the present invention provides a kind of smoking article, and these goods contain the particle diameter of 0.1-20% weight at the 0.1-100 micron, and 0.5-50 micron preferably is more preferably the aphrizite of 4-25 micron.
In one embodiment of the invention, smoking article is selected from cigarette paper, filter tip, cigarette with filter tip, cigarette case, Cigarette container, cigarette tin, cigarette case Jie sheet.
In another embodiment of the present invention, smoking article preferably contains the aphrizite of 0.5-10% weight, more preferably contains the aphrizite of 1-5% weight.
Aspect second of the present invention, a kind of method for preparing smoking article is provided, comprise step:
(a) the classified processing of aphrizite being crushed to particle diameter is the 0.1-100 micron;
(b) tourmaline that will account for total goods raw material 0.1-20% weight mixes the smoking article raw material;
(c) make smoking article.
In one embodiment of the invention, will account for overall package material 0.5-10% weight, the aphrizite of preferred 1-5% weight mixes the smoking article raw material.
In another embodiment of the present invention, the particle diameter of this aphrizite is the 0.5-50 micron preferably, is more preferably the 4-25 micron.
Also have among the embodiment of the present invention, the product that this method makes is selected from cigarette paper, filter tip, cigarette with filter tip, cigarette case, Cigarette container, cigarette tin, cigarette case Jie sheet.
The purposes of smoking article of the present invention is provided aspect the 3rd of the present invention, and this product is used to reduce smoking nicotine, reduces tar content and improves mouthfeel.
Description of drawings
Fig. 1 has shown that the particle diameter with the aphrizite powder of method preparation of the present invention distributes.
The specific embodiment
The inventor finds that under study for action after aphrizite carried out the nanometer technology ultra-fine grinding, along with diminishing of particle diameter, the infra-red radiation and the anion-generating capacity that are sent changed.When particle diameter reached the 4.85um left and right sides, its infra-red radiation was up to 0.95, and anion-generating capacity is 1600/cm
3, infra-red radiation and anion can effectively decompose harmful poisonous substance and reach 70%.
Through the aphrizite powder of the ultra-fine technical finesse of nanometer, its anion usefulness can be removed carcinogen BaP, smoking nicotine, carbon monoxide and the ammonia in the cigarette.Also can improve simultaneously the oxygen metabolism in the human body, improve the lung definition.
Aphrizite is an inorganic matter, and its stability is good, and is nontoxic, and detoxifying effect is good, and the industrialization cost is low.In to tobacco removing smoking nicotine and detoxifcation deodorizing, this product can also replenish essential various trace elements in the human body, plays and reduces pollution, protection environment, wholesome social benefit and economic benefit.
Smoking article among the present invention is meant Jie's sheet of the cigarette paper, cigarette case, Cigarette container, cigarette tin and the insertion cigarette case that are used for containers of cigarettes etc., under these situations aphrizite is mixed in the paper pulp, uses the conventional method dry forming.This term also comprises the cigarette filter that aphrizite is mixed with the sponge fiber and make, and this filter tip and pipe tobacco one are reinstated the cigarette that the cigarette paper parcel forms.
The used concrete consumption of aphrizite of the present invention is the 0.1-20% weight of total goods raw material.With this ratio, the aphrizite consumption that is converted to every cigarette is a 0.005%-1% weight.
The preparation of micron order aphrizite
Under the normal temperature and pressure state, carry out classification and handle, aphrizite is crushed to the 0.1-100 micron with airslide disintegrating mill.
Fig. 1 is seen in the distribution of aphrizite powder.
According to infra-red radiation as a result diameter of particle reach as high as 0.93 when the 4.85um, then get powder particle diameter mean value 3.96um, use the LS particle size analyzer to carry out the test of granularity and distribution thereof.See table 1 for details.
Table 1: sample powder particle size key dimension parameter
| Particle diameter/um | Volume cumulative distribution % | Account for total distributed % |
| 1.459 | 10 | 10 |
| 2.000 | 17.07 | 7.07 |
| 2.494 | 25 | 7.94 |
| 3.960 | 50 | 25 |
| 5.00 | 65.58 | 15.58 |
| 5.781 | 75 | 9.92 |
| 7.60 | 90 | 15 |
| 8.00 | 92.16 | 2.16 |
| 10.00 | 98.34 | 6.18 |
| 14.00 | 100 | 10.66 |
The anion incidence of aphrizite powder
Tester: ITC-201A air ion concentration tester
Entrust Shanghai City environment-friendly products quality supervision and test master station with this tester, measured every cubic metre negative ion concentration according to standard method.
Table 2: sample anion-generating capacity and grain size parameter
| Sample | Particle diameter/um | Anion-generating capacity/cm 3(static state) | Anion-generating capacity/cm 3(dynamically) |
| A | 0.1 | 300 | 1200 |
| B | 10.00 | 395 | 1580 |
| C | 25.00 | 400 | 1600 |
| D | 100.00 | 350 | 1400 |
This shows: the particle diameter of sample powder is not thin more good more.When particle diameter is distributed in 25 microns, can reach maximum anion incidence.Particle between the 0.1-100 micron all has obvious effect.
Following examples adopt the prepared aphrizite powder of embodiment 1.
Embodiment 3
Prepare cigarette paper with aphrizite
With 5% weight 10 aphrizites are mixed in the 200g cigarette paper paper pulp, stir, pave normal temperature and dry and make cigarette paper.Roll 0.75 a gram/commercially available pipe tobacco (seven wolves) with it, make cigarette.
Embodiment 4
Prepare cigarette filter with aphrizite
With 5% weight the aphrizite powder is mixed in the 200g sponge fiber, be compacted into cigarette filter.Itself and 0.75 a gram/commercially available pipe tobacco (seven wolves) are reinstated the commercial cigarettes paper roll and risen, make cigarette with filter tip.
Prepare cigarette case with aphrizite
The aphrizite powder is mixed with 200 gram vinyon powder or 200g paper pulp with 5% weight, pour mould or oven dry compacting and the folding cigarette case of making into.
Prepare cigarette case Jie sheet with aphrizite
The aphrizite powder is mixed with 200g plastic powders or paper pulp with 5% weight, be pressed into Jie's sheet of 5cm * 5cm in the cigarette case.The every heavy 1g of Jie's sheet.
Prepare cigarette tin with aphrizite
50g aphrizite powder is mixed in 1 kilogram of plastic pellet, pour press molding in the mould into, make 5 cylindrical cigarette tins.Each cigarette tin can be adorned 100 cigarettes, heavy 200g.
Embodiment 8
The tobacco detoxifcation test of aphrizite goods
Tested the smoke panel test contrast of human body according to the method for standard GB 5606.4-1996 for various cigarette.
10 people are divided into 2 groups, before the cigarette divisional processing of each plate and after handling, respectively exhaust 1.
A. embodiment 3 and 4 cigarette of making is made suction immediately behind the cigarette.
B. cigarette is placed on embodiment 5,6,7 made cigarette case, cigarette bucket, puts into Jie's sheet that makes, place and began suction in 30 minutes later on, check.
Table 3 provides the result.Wherein A and B are the cigarette that the application's method is made, and A1 and B1 are original commercially available cigarette.Shown in the table is the result that tobacco product obtained with the aphrizite manufacturing of 5% weight.In cigarette, during suction to experience harmony good more, assorted gas is few more, excitant is low more, illustrates that the tar content of this cigarette is low more, the nicotine flue gas is few more.And pleasant impression is not pungent, does not have niff, illustrates that the mouthfeel of cigarette is good more.
The suction report of the cigarette that table 3-A embodiment 3 prepared cigarette paper wrap up
| | Gloss | 6 | Fragrance 36 | | Assorted gas 16 | Excitant 16 | | Add up to | |||||||||||||||
| The mark section | A | B | C | A | B | C | A | B | C | A | B | C | A | B | C | A | B | C | |||||
| Sample | Board is other | 6 | 4 | 2 | 36 | 28 | 18 | 6 | 4 | 2 | 16 | 12 | 9 | 16 | 13 | 11 | 20 | 14 | 8 | 100 | |||
| A | Double Happiness | √ | √ | √ | √ | √ | √ | 90 | |||||||||||||||
| A1 | Double Happiness | √ | √ | √ | √ | √ | √ | 62 | |||||||||||||||
| B | Seven wolves | √ | √ | √ | √ | √ | √ | 86 | |||||||||||||||
| B 1 | Seven wolves | √ | √ | √ | √ | √ | √ | 52 | |||||||||||||||
The suction parcel of the cigarette with filter tip that table 3-B embodiment 4 is prepared
| Project | Gloss | |||
| 6 | Fragrance 36 | | Assorted gas 16 | Excitant 16 | | Add up to | ||||||||||||||
| The mark section | A | B | C | A | B | C | A | B | C | A | B | C | A | B | C | A | B | C | ||
| Sample | Board is other | 6 | 4 | 2 | 36 | 28 | 18 | 6 | 4 | 2 | 16 | 12 | 9 | 16 | 13 | 11 | 20 | 14 | 8 | 100 |
| A | Double Happiness | √ | √ | √ | √ | √ | √ | 90 | ||||||||||||
| A 1 | Double Happiness | √ | √ | √ | √ | √ | √ | 66 | ||||||||||||
| B | Seven wolves | √ | √ | √ | √ | √ | √ | 86 | ||||||||||||
| B 1 | Seven wolves | √ | √ | √ | √ | √ | √ | 52 |
The cigarette that table 3-C packs with the cigarette case of embodiment 5 preparations
| Project | Gloss | |||
| 6 | Fragrance 36 | | Assorted gas 16 | Excitant 16 | | Add up to | ||||||||||||||
| The mark section | A | B | C | A | B | C | A | B | C | A | B | C | A | B | C | A | B | C | ||
| Sample | Board is other | 6 | 4 | 2 | 36 | 28 | 18 | 6 | 4 | 2 | 16 | 12 | 9 | 16 | 13 | 11 | 20 | 14 | 8 | 100 |
| A | Double Happiness | √ | √ | √ | √ | √ | √ | 80 | ||||||||||||
| A 1 | Double Happiness | √ | √ | √ | √ | √ | √ | 66 | ||||||||||||
| B | Seven wolves | √ | √ | √ | √ | √ | √ | 76 | ||||||||||||
| B 1 | Seven wolves | √ | √ | √ | √ | √ | √ | 52 |
The cigarette that table 3-D packs with cigarette case Jie sheet of embodiment 6 preparations.
| | Gloss | 6 | Fragrance 36 | | Assorted gas 16 | Excitant 16 | | Add up to | |||||||||||||||
| The mark section | A | B | C | A | B | C | A | B | C | A | B | C | A | B | C | A | B | C | |||||
| Sample | Board is other | 6 | 4 | 2 | 36 | 28 | 18 | 6 | 4 | 2 | 16 | 2 | 9 | 16 | 13 | 11 | 20 | 14 | 8 | 100 | |||
| A | Double Happiness | √ | √ | √ | √ | √ | √ | 74 | |||||||||||||||
| A 1 | Double Happiness | √ | √ | √ | √ | √ | √ | 66 | |||||||||||||||
| B | Seven wolves | √ | √ | √ | √ | √ | √ | 70 | |||||||||||||||
| B 1 | Seven wolves | √ | √ | √ | √ | √ | √ | 52 | |||||||||||||||
The cigarette that table 3-E packs with the cigarette tin of embodiment 7 preparations
| Project | Gloss | |||
| 6 | Fragrance 36 | | Assorted gas 16 | Excitant 16 | | Add up to | ||||||||||||||
| The mark section | A | B | C | A | B | C | A | B | C | A | B | C | A | B | C | A | B | C | ||
| Sample | Board is other | 6 | 4 | 2 | 36 | 28 | 18 | 6 | 4 | 2 | 16 | 12 | 9 | 16 | 13 | 11 | 20 | 14 | 8 | 100 |
| A | Double Happiness | √ | √ | √ | √ | √ | √ | 82 | ||||||||||||
| A 1 | Double Happiness | √ | √ | √ | √ | √ | √ | 66 | ||||||||||||
| B | Seven wolves | √ | √ | √ | √ | √ | √ | 75 | ||||||||||||
| B 1 | Seven wolves | √ | √ | √ | √ | √ | √ | 52 |
This shows that with the cigarette that the aphrizite goods were handled, smoking nicotine and tar content all have obvious decline, mouthfeel is improved.
Embodiment 9
Repeat the process of embodiment 6 and made cigarette case Jie sheet, difference is with 0.5%, 1%, the aphrizite of 10% and 20% weight is replaced the aphrizite of original 5% weight, test with embodiment 8 same methods, the result can reduce the nicotine flue gas and the tar content of cigarette equally, improves the mouthfeel of cigarette.Only along with the minimizing of content, the time that needs to place than long just can reach same effect.When content was higher, the time of placement can reach same effect than weak point.
Though illustrate and described preference of the present invention, should understand those skilled in the art and can make various changes according to the instruction of this paper, these change without prejudice to scope of the present invention.
Claims (8)
1. a smoking article is characterized in that, these goods contain the aphrizite of the particle diameter of 0.1-20% weight at the 4-25 micron.
2. smoking article as claimed in claim 1 is characterized in that, described goods are selected from cigarette paper, filter tip, cigarette with filter tip, cigarette case, Cigarette container, cigarette tin, cigarette case Jie sheet.
3. smoking article as claimed in claim 1 is characterized in that described goods contain the aphrizite of 0.5-10% weight.
4. the method for claim 1 is characterized in that, described goods contain the aphrizite of 1-5% weight.
5. method for preparing smoking article is characterized in that the method comprising the steps of:
(a) the classified processing of aphrizite being crushed to particle diameter is the 4-25 micron;
(b) tourmaline that will account for total goods raw material 0.1-20% weight mixes the smoking article raw material;
(c) make smoking article.
6. method as claimed in claim 5 is characterized in that, the aphrizite that accounts for total goods raw material 0.5-10% weight is mixed the smoking article raw material.
7. method as claimed in claim 5 is characterized in that, the aphrizite that accounts for total goods raw material 1-5% weight is mixed smoking article.
8. method as claimed in claim 5 is characterized in that, described goods are selected from cigarette paper, filter tip, cigarette with filter tip, cigarette case, Cigarette container, cigarette tin, cigarette case Jie sheet.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB03129331XA CN100341441C (en) | 2003-06-18 | 2003-06-18 | Black tourmaline containing tobacco product and its making method and uses |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB03129331XA CN100341441C (en) | 2003-06-18 | 2003-06-18 | Black tourmaline containing tobacco product and its making method and uses |
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| Publication Number | Publication Date |
|---|---|
| CN1565289A CN1565289A (en) | 2005-01-19 |
| CN100341441C true CN100341441C (en) | 2007-10-10 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101637307B (en) * | 2009-06-16 | 2011-01-26 | 成进学 | Cigarette fiber filter tip powerfully filtering off toxic matters and releasing microelement anions |
| CN103222683B (en) * | 2012-06-28 | 2014-03-26 | 湖北中烟工业有限责任公司 | Cigarette filter rod provided with natural mineral and plant fiber composite additive |
| CN103082412A (en) * | 2013-02-05 | 2013-05-08 | 大亚科技股份有限公司 | Ternary composite filter stick with tourmaline added |
| CN112155248B (en) * | 2020-11-02 | 2022-12-30 | 桂林市鲍姑红艾医药科技有限公司 | Preparation method of wormwood health cigarette |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1002781A (en) * | 1964-08-07 | 1965-08-25 | George Milton Jacobson | Cigarette filter |
| JPH09299073A (en) * | 1996-05-11 | 1997-11-25 | Takashi Sato | Healthy cigarette |
-
2003
- 2003-06-18 CN CNB03129331XA patent/CN100341441C/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1002781A (en) * | 1964-08-07 | 1965-08-25 | George Milton Jacobson | Cigarette filter |
| JPH09299073A (en) * | 1996-05-11 | 1997-11-25 | Takashi Sato | Healthy cigarette |
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|---|---|
| CN1565289A (en) | 2005-01-19 |
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