CL2019003462A1 - Proceso para extraer cannabinoides de materia prima vegetal de cannabis mediante el uso del salmuera - Google Patents

Proceso para extraer cannabinoides de materia prima vegetal de cannabis mediante el uso del salmuera

Info

Publication number
CL2019003462A1
CL2019003462A1 CL2019003462A CL2019003462A CL2019003462A1 CL 2019003462 A1 CL2019003462 A1 CL 2019003462A1 CL 2019003462 A CL2019003462 A CL 2019003462A CL 2019003462 A CL2019003462 A CL 2019003462A CL 2019003462 A1 CL2019003462 A1 CL 2019003462A1
Authority
CL
Chile
Prior art keywords
oil
ethanol
brine
mixture
cannabis plant
Prior art date
Application number
CL2019003462A
Other languages
English (en)
Inventor
Ryan Delmoral Ko
Brock Hughes
Krupal Devendra Pal
Alexzander Samuelsson
Original Assignee
Nextleaf Solutions Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US15/721,344 external-priority patent/US9987567B1/en
Application filed by Nextleaf Solutions Ltd filed Critical Nextleaf Solutions Ltd
Publication of CL2019003462A1 publication Critical patent/CL2019003462A1/es

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/0288—Applications, solvents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/028—Flow sheets
    • B01D11/0284—Multistage extraction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/0292—Treatment of the solvent
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/08—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in rotating vessels; Atomisation on rotating discs
    • B01D3/085—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in rotating vessels; Atomisation on rotating discs using a rotary evaporator
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/40—Extractive distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/004—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by obtaining phenols from plant material or from animal material
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/50—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by reactions decreasing the number of carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
    • C07C37/74—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/86—Purification; separation; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C39/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
    • C07C39/18—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring monocyclic with unsaturation outside the aromatic ring
    • C07C39/19—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring monocyclic with unsaturation outside the aromatic ring containing carbon-to-carbon double bonds but no carbon-to-carbon triple bonds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C39/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
    • C07C39/23—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring polycyclic, containing six-membered aromatic rings and other rings, with unsaturation outside the aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
    • C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D311/78—Ring systems having three or more relevant rings
    • C07D311/80—Dibenzopyrans; Hydrogenated dibenzopyrans
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/16—Systems containing only non-condensed rings with a six-membered ring the ring being unsaturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Botany (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Fats And Perfumes (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

Proceso para extraer cannabinoides de materia prima vegetal de cannabis, el que comprende los pasos de: agregar etanol al material vegetal de cannabis seco y molido para formar una mezcla inicial; girar la mezcla inicial para separar una mezcla de aceite crudo y etanol de la mezcla inicial; tratar la mezcla de aceite crudo y etanol con medios para eliminar componentes no deseados de los mismos; evaporar etanol de la mezcla tratada de aceite crudo y etanol para dejar aceite; lavar el aceite con salmuera; descarboxilar el aceite lavado con salmuera para formar aceite descarboxilado; y destilar el aceite descarboxilado para obtener cannabinoides
CL2019003462A 2017-09-29 2019-11-27 Proceso para extraer cannabinoides de materia prima vegetal de cannabis mediante el uso del salmuera CL2019003462A1 (es)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US15/721,344 US9987567B1 (en) 2017-09-29 2017-09-29 Cannabinoid extraction process and system
US201862675620P 2018-05-23 2018-05-23
US201862676261P 2018-05-24 2018-05-24
US15/993,457 US10413843B2 (en) 2017-09-29 2018-05-30 Cannabinoid extraction and distillation
US16/112,033 US10406453B2 (en) 2017-09-29 2018-08-24 Cannabinoid extraction process using brine

Publications (1)

Publication Number Publication Date
CL2019003462A1 true CL2019003462A1 (es) 2020-03-06

Family

ID=65896924

Family Applications (1)

Application Number Title Priority Date Filing Date
CL2019003462A CL2019003462A1 (es) 2017-09-29 2019-11-27 Proceso para extraer cannabinoides de materia prima vegetal de cannabis mediante el uso del salmuera

Country Status (14)

Country Link
US (1) US10406453B2 (es)
EP (1) EP3645027A4 (es)
AU (2) AU2018340881B2 (es)
BR (1) BR112019026417B1 (es)
CA (1) CA3063960C (es)
CL (1) CL2019003462A1 (es)
CO (2) CO2019014964A2 (es)
IL (3) IL269173B (es)
MA (1) MA49527A (es)
MX (1) MX2019012109A (es)
NZ (1) NZ757625A (es)
PE (1) PE20200397A1 (es)
WO (1) WO2019060986A1 (es)
ZA (1) ZA201906293B (es)

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US20180206518A1 (en) 2016-04-15 2018-07-26 Ronald Silver Method of making cannabis oil hydrophilic using emulsifiers and related cannabinoid compositions
CA3021093A1 (en) 2016-04-15 2017-10-19 Sre Wellness, Inc. Cannabis infused sweeteners and other compositions
US10239808B1 (en) 2016-12-07 2019-03-26 Canopy Holdings, LLC Cannabis extracts
US10478747B2 (en) * 2017-11-10 2019-11-19 NextLeaf Solutions Ltd. Closed loop chilled solvent feed for cannabinoid extraction
US10245525B1 (en) * 2017-11-10 2019-04-02 NextLeaf Solutions Ltd. Closed-loop multi-stage chilled filter system
US11202771B2 (en) 2018-01-31 2021-12-21 Treehouse Biotech, Inc. Hemp powder
CA3073093A1 (en) 2018-08-03 2020-02-06 Biomass Oil Separation Solutions, Llc Processes and apparatus for extraction of substances and enriched extracts from plant material
US10570350B1 (en) * 2018-08-17 2020-02-25 Evello International, LLC Systems and methods of cannabis oil extraction
US10688410B2 (en) 2018-08-17 2020-06-23 Evello International, LLC Systems and methods of cannabis oil extraction
CA3119729A1 (en) 2018-10-10 2020-04-16 Treehouse Biotech, Inc. Synthesis of cannabigerol
US10765966B2 (en) * 2019-02-06 2020-09-08 Heinkel Filtering Systems. Inc. Biomass extraction and centrifugation systems and methods
WO2020191098A1 (en) * 2019-03-20 2020-09-24 Quality Resources, Llc Method of producing purified cannabis extracts
US10569189B1 (en) * 2019-05-17 2020-02-25 NextLeaf Solutions Ltd. Method for acetylation of cannabinoids
CA3105910C (en) 2019-06-12 2021-04-27 Nectar Health Sciences Inc. Methods for extraction, processing, and purification of a selected family of target compounds from cannabis
US10799546B1 (en) 2019-07-26 2020-10-13 Biomass Oil Separation Solutions, Llc Modular, integrated process and apparatus for extracting, refining and remediating active substances from plant material
WO2021016718A1 (en) * 2019-07-31 2021-02-04 Canopy Growth Corporation Separation of cannabinoids from mixtures thereof by distillation
US11326124B2 (en) 2019-09-13 2022-05-10 Halcyon Holdings, Llc Recirculating high pressure lipid (HPL) extractor, infuser and bonder, and system and method of use thereof
CA3157507A1 (en) * 2019-10-10 2021-04-15 Jamaican Brew House A terpene-reduced cannabinoid adjunct
US10858303B1 (en) 2019-10-30 2020-12-08 Heinkel Filtering Systems, Inc. Cannabidiol isolate production systems and methods
US10751640B1 (en) 2019-10-30 2020-08-25 Heinkel Filtering Systems, Inc. Cannabidiol isolate production systems and methods
CN112755584A (zh) * 2020-12-15 2021-05-07 鲁南制药集团股份有限公司 一种高效萃取离心装置
CA3202408A1 (en) * 2020-12-18 2022-06-23 Matthew Havis FINLEY Facile purification of cannabinoid acids

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US20130079531A1 (en) * 2011-09-27 2013-03-28 Rm3 Labs LLC Process for the Rapid Extraction of Active Ingredients from Herbal Materials
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EP3250200A4 (en) * 2015-01-31 2018-09-19 Constance Therapeutics, Inc. Methods for preparation of cannabis oil extracts and compositions
US11040295B2 (en) * 2015-02-06 2021-06-22 Joseph Francis Payack Method and apparatus for extracting plant oils using ethanol water
NL2015304B1 (nl) * 2015-08-13 2017-02-28 Ernest Bruining Wernard Extractie inrichting en een extractie werkwijze voor extractie van cannabis.
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Also Published As

Publication number Publication date
NZ757625A (en) 2019-12-20
US20190099696A1 (en) 2019-04-04
AU2018340881B2 (en) 2019-12-05
IL269173A (en) 2019-11-28
IL269173B (en) 2020-05-31
EP3645027A4 (en) 2021-05-19
IL269422B (en) 2020-05-31
CA3063960A1 (en) 2019-04-04
IL269306B (en) 2020-05-31
IL269422A (en) 2019-11-28
AU2019250112B2 (en) 2019-12-05
AU2018340881A1 (en) 2019-10-17
MX2019012109A (es) 2020-02-12
MA49527A (fr) 2021-05-19
US10406453B2 (en) 2019-09-10
PE20200397A1 (es) 2020-02-26
EP3645027A1 (en) 2020-05-06
BR112019026417A2 (pt) 2020-07-21
CA3063960C (en) 2020-03-10
WO2019060986A1 (en) 2019-04-04
CO2019014964A2 (es) 2020-01-17
BR112019026417B1 (pt) 2020-12-01
AU2019250112A1 (en) 2019-10-31
ZA201906293B (en) 2020-09-30
CO2020007209A2 (es) 2020-06-19
IL269306A (en) 2019-11-28

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