CH202444A - Process for the production of an acidic wool dye. - Google Patents
Process for the production of an acidic wool dye.Info
- Publication number
- CH202444A CH202444A CH202444DA CH202444A CH 202444 A CH202444 A CH 202444A CH 202444D A CH202444D A CH 202444DA CH 202444 A CH202444 A CH 202444A
- Authority
- CH
- Switzerland
- Prior art keywords
- production
- dye
- acidic
- wool dye
- acidic wool
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B51/00—Nitro or nitroso dyes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
<B>Zusatzpatent</B> zum Hauptpatent Nr. 193627. Verfahren zur Herstellung eines sauren Wollfarbstoffes. Vorliegendes Patent bezieht sich auf ein Verfahren zur Herstellung eines sauren Woll- farbstoffes, dadurch gekennzeichnet, dass man 4 . 4'-Dichlor-3 . 3'-dinitrodiphenylsulfogyd mit 4-Aminodiphenylamin-2-sulfonsäure kon densiert.
Der so erhaltene Farbstoff färbt Wolle aus saurem Bade in gelbbraunen Tönen von hervorragenden Echtheitseigenschaften. Beispiel: 52,8 Teile 4-Aminodiphenylamin-2-sul- fonsäure, 36 Teile 4. 4'-Dichlor-3. 3'-dinitro- diphenylsulfogyd und 22 Teile wasserfreies Natriumcarbonat werden mit etwa 400 Teilen Wasser mehrere Stunden unter Rühren und Rückflusskühlung zum Sieden erhitzt. Nach dem Erkalten wird der gebildete Farbstoff durch Zugabe einer geringen Menge von kon zentriertem Salzwasser abgeschieden, abge saugt, mit etwa 5%igem Salzwasser ge waschen und dann getrocknet.
<B> Additional patent </B> to main patent no. 193627. Process for the production of an acidic wool dye. The present patent relates to a process for the production of an acidic wool dye, characterized in that 4. 4'-dichloro-3. 3'-dinitrodiphenylsulfogyd condenses with 4-aminodiphenylamine-2-sulfonic acid.
The dye obtained in this way dyes wool from an acid bath in yellow-brown shades with excellent fastness properties. Example: 52.8 parts of 4-aminodiphenylamine-2-sulphonic acid, 36 parts of 4. 4'-dichloro-3. 3'-Dinitro-diphenylsulfogyd and 22 parts of anhydrous sodium carbonate are heated to boiling with about 400 parts of water for several hours with stirring and reflux cooling. After cooling, the dye formed is deposited by adding a small amount of concentrated salt water, filtered off with suction, washed with about 5% salt water and then dried.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE202444X | 1936-12-14 | ||
| CH193627T | 1937-12-13 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH202444A true CH202444A (en) | 1939-01-15 |
Family
ID=25722566
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH202444D CH202444A (en) | 1936-12-14 | 1937-12-13 | Process for the production of an acidic wool dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH202444A (en) |
-
1937
- 1937-12-13 CH CH202444D patent/CH202444A/en unknown
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