CH179673A - Process for the preparation of a monoazo dye. - Google Patents
Process for the preparation of a monoazo dye.Info
- Publication number
- CH179673A CH179673A CH179673DA CH179673A CH 179673 A CH179673 A CH 179673A CH 179673D A CH179673D A CH 179673DA CH 179673 A CH179673 A CH 179673A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation
- dye
- sulfonic acid
- monoazo dye
- acetylamino
- Prior art date
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Verfahren zur Herstellung eines ltlonoazofarbstoffes. Vorliegendes Patent bezieht sieh auf ein Verfahren zur Herstellung eines DIonoazofarb- stoffes, dadurch gekennzeichnet, dass man die Diazoverbindung der 1-Amino-2.4-dimethyl- beiizol-6-sulfosäure mit der 1-Acetylamino-5- naphthol-7-sulfosäure kuppelt.
Der neue Farbstoff ist ein oranges Pulver und färbt Wolle in egalen leuchtend gelb stichig roten Tönen von hervorragender Licht echtheit.
Beispiel: 20,1 kg 1-Amino-2.4-dirnethylbenzol-6- sulfosäure werden in der üblichen Weise dia- zotiert. Die erhaltene Diazolösung lässt man in eine kalte Lösung von 29 kg 1-Acetyl- amino-5-naphthol-7-sulfosäure laufen und stumpft die freie Säure durch Zugabe von Natriumbicarbonat oder Soda ab. Nach be endeter Kupplung wird der Farbstoff durch Aussalzen isoliert.
Process for the preparation of an itlonoazo dye. The present patent relates to a process for the preparation of a dionoazo dye, characterized in that the diazo compound of 1-amino-2,4-dimethyl-bizol-6-sulfonic acid is coupled with 1-acetylamino-5-naphthol-7-sulfonic acid.
The new dye is an orange powder and dyes wool in even, bright yellow, pungent red tones with excellent lightfastness.
Example: 20.1 kg of 1-amino-2,4-dirnethylbenzene-6-sulfonic acid are diazotized in the usual way. The diazo solution obtained is allowed to run into a cold solution of 29 kg of 1-acetylamino-5-naphthol-7-sulfonic acid and the free acid is blunted by adding sodium bicarbonate or soda. After coupling has ended, the dye is isolated by salting out.
Claims (1)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE179673X | 1933-08-22 | ||
CH176032T | 1935-01-26 |
Publications (1)
Publication Number | Publication Date |
---|---|
CH179673A true CH179673A (en) | 1935-09-15 |
Family
ID=25719788
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH179673D CH179673A (en) | 1933-08-22 | 1934-07-27 | Process for the preparation of a monoazo dye. |
Country Status (1)
Country | Link |
---|---|
CH (1) | CH179673A (en) |
-
1934
- 1934-07-27 CH CH179673D patent/CH179673A/en unknown
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