CH179672A - Process for the preparation of a monoazo dye. - Google Patents
Process for the preparation of a monoazo dye.Info
- Publication number
- CH179672A CH179672A CH179672DA CH179672A CH 179672 A CH179672 A CH 179672A CH 179672D A CH179672D A CH 179672DA CH 179672 A CH179672 A CH 179672A
- Authority
- CH
- Switzerland
- Prior art keywords
- monoazo dye
- preparation
- sulfonic acid
- dye
- naphthol
- Prior art date
Links
Landscapes
- Coloring (AREA)
Description
Verfahren zur Herstellung eines Monoazofar bstoffes. Voliegendes Patent bezieht sich auf ein Verfahren zur Herstellung eines Monoazo- farbstoffes, dadurch gekennzeichnet, dass man die Diazoverbindung der 1 -Anrino-2.4.5- trimethylberizol-6-sulfosärrre mit der 2-Acetyl- arnino-8-naphthol-6-sulfosäur,e kuppelt.
Der neue Farbstoff stellt nach dem Trock nen ein orange gefärbtes, leicht in Wasser lösliches Pulver dar und färbt Wolle in ega- len hervorragend lichtechten lebhaften roten Tönen. <I>Beispiel:</I> 21,5 kg 1-Anrino-2.4.5-trimethylbenzol- 6-sulfosäure werden in der üblichen Weise diazotiert. Die erhaltene Diazolösung lässt man in eine kalte Lösung von 29 kg 2-Acetyl- amino-8-naphthol-6-sulfosäure laufen und stumpft die freie Säure durch Zugabe von Natriumbicarbonat oder Soda ab.
Nach be endeter Kupplung wird der Farbstoff durch Aussalzen isoliert.
Process for the production of a monoazo dye. The present patent relates to a process for the production of a monoazo dye, characterized in that the diazo compound of the 1-anrino-2,4.5-trimethylberizole-6-sulfonic acid is mixed with the 2-acetyl-amino-8-naphthol-6-sulfonic acid , e clutch.
After drying, the new dye is an orange-colored powder that is easily soluble in water and dyes wool in level, excellent lightfast, lively red tones. <I> Example: </I> 21.5 kg 1-anrino-2,4,5-trimethylbenzene-6-sulfonic acid are diazotized in the usual way. The diazo solution obtained is allowed to run into a cold solution of 29 kg of 2-acetylamino-8-naphthol-6-sulfonic acid and the free acid is blunted by adding sodium bicarbonate or soda.
After coupling has ended, the dye is isolated by salting out.
Claims (1)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE179672X | 1933-08-22 | ||
CH176032T | 1935-01-26 |
Publications (1)
Publication Number | Publication Date |
---|---|
CH179672A true CH179672A (en) | 1935-09-15 |
Family
ID=25719787
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH179672D CH179672A (en) | 1933-08-22 | 1934-07-27 | Process for the preparation of a monoazo dye. |
Country Status (1)
Country | Link |
---|---|
CH (1) | CH179672A (en) |
-
1934
- 1934-07-27 CH CH179672D patent/CH179672A/en unknown
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