CA968805A - Process for preparation of d,1-alpha-tocopherol - Google Patents

Process for preparation of d,1-alpha-tocopherol

Info

Publication number
CA968805A
CA968805A CA135,025A CA135025A CA968805A CA 968805 A CA968805 A CA 968805A CA 135025 A CA135025 A CA 135025A CA 968805 A CA968805 A CA 968805A
Authority
CA
Canada
Prior art keywords
tocopherol
alpha
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
CA135,025A
Other languages
English (en)
Other versions
CA135025S (en
Inventor
Sheldon B. Greenbaum
Walter Hacke
Herman Horn
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Diamond Shamrock Corp
Original Assignee
Diamond Shamrock Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Diamond Shamrock Corp filed Critical Diamond Shamrock Corp
Application granted granted Critical
Publication of CA968805A publication Critical patent/CA968805A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
    • C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D311/04—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
    • C07D311/58—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4
    • C07D311/70—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4 with two hydrocarbon radicals attached in position 2 and elements other than carbon and hydrogen in position 6
    • C07D311/72—3,4-Dihydro derivatives having in position 2 at least one methyl radical and in position 6 one oxygen atom, e.g. tocopherols

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pyrane Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CA135,025A 1971-02-25 1972-02-18 Process for preparation of d,1-alpha-tocopherol Expired CA968805A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US11904871A 1971-02-25 1971-02-25

Publications (1)

Publication Number Publication Date
CA968805A true CA968805A (en) 1975-06-03

Family

ID=22382303

Family Applications (1)

Application Number Title Priority Date Filing Date
CA135,025A Expired CA968805A (en) 1971-02-25 1972-02-18 Process for preparation of d,1-alpha-tocopherol

Country Status (8)

Country Link
US (1) US3708505A (enExample)
JP (1) JPS5341154B1 (enExample)
CA (1) CA968805A (enExample)
DE (1) DE2208795C3 (enExample)
FR (1) FR2126214B1 (enExample)
GB (1) GB1371701A (enExample)
IL (1) IL38718A (enExample)
IT (1) IT990452B (enExample)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4055575A (en) * 1975-03-20 1977-10-25 Scm Corporation Synthesis of dehydrophytol and vitamin E
US4191692A (en) * 1976-02-20 1980-03-04 Basf Aktiengesellschaft Manufacture of tocopherol
DE2606830C3 (de) * 1976-02-20 1981-08-27 Basf Ag, 6700 Ludwigshafen Verfahren zur Herstellung von Tocopherol
JPS6019309B2 (ja) * 1976-09-29 1985-05-15 日清製粉株式会社 高純度ｄｌ−α−トコフエロ−ルの製造法
DE3203487A1 (de) * 1982-02-03 1983-08-11 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von tocopherylacetat oder tocopherylpropionat
DE4208477A1 (de) * 1992-03-17 1993-09-23 Basf Ag Verfahren zur herstellung von vitamin e
US5663376A (en) † 1994-07-27 1997-09-02 Eisai Co., Ltd. Process for the preparation of α-tocopherol
FR2733977B1 (fr) * 1995-05-10 1997-07-04 Rhone Poulenc Nutrition Animal Procede de preparation de phenols substitues
ATE233254T1 (de) * 1996-01-05 2003-03-15 Hoffmann La Roche Verfahren zur herstellung von d,l-alpha- tocopherol in gegenwart einer perfluoralkylensulfonsäure als katalysator
US6005122A (en) * 1996-12-23 1999-12-21 Basf Aktiengesellschaft Preparation of α-tocopherol or α-tocopheryl acetate by reacting trimethylhydroquinone and phytol or isophytol, with recycling of the zinc halide condensation catalyst
ES2264230T3 (es) * 1998-04-06 2006-12-16 Dsm Ip Assets B.V. Procedimiento par ala obtencion de d,1-alfa-tocoferol, en un disolvente de carbonato y en presencia de un catalizador de acido conteniendo azufre.
FR2784104B1 (fr) * 1998-09-18 2002-12-27 Rhone Poulenc Nutrition Animal Procede de preparation de la vitamine e
ATE298330T1 (de) 2000-11-22 2005-07-15 Basf Ag Verfahren zur kontinuierlichen acylierung von chromanolesterderivaten
WO2004046126A1 (en) * 2002-11-21 2004-06-03 Dsm Ip Assets B.V. Manufacture of tocopheryl acetate
KR101154117B1 (ko) * 2003-01-13 2012-06-11 디에스엠 아이피 어셋츠 비.브이. α-토코페릴 아세테이트의 제조방법
KR101140519B1 (ko) * 2004-06-11 2012-04-30 디에스엠 아이피 어셋츠 비.브이. 크로만 유도체, 특히 α-토코페롤 및 그의 알카노에이트의제조 방법
CN106565659B (zh) * 2016-11-01 2019-06-18 万华化学集团股份有限公司 一种制备维生素e乙酸酯的方法
CN108409704A (zh) * 2018-01-24 2018-08-17 上海优合生物科技有限公司 一种高纯度生育酚琥珀酸酯盐的制备方法

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2411968A (en) * 1938-03-31 1946-12-03 Hoffmann La Roche Process for the preparation of synthetic dl-tocopherols
US2411969A (en) * 1938-03-31 1946-12-03 Hoffmann La Roche Process for the preparation of synthetic dl-tocopherols

Also Published As

Publication number Publication date
DE2208795B2 (de) 1978-03-09
DE2208795C3 (de) 1978-11-02
JPS5341154B1 (enExample) 1978-10-31
IL38718A0 (en) 1972-04-27
IL38718A (en) 1975-02-10
IT990452B (it) 1975-06-20
FR2126214A1 (enExample) 1972-10-06
GB1371701A (en) 1974-10-23
US3708505A (en) 1973-01-02
DE2208795A1 (de) 1972-08-31
FR2126214B1 (enExample) 1977-07-15

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