CA2963535A1 - Procede de fabrication d'un alliage pour tube de reformage - Google Patents
Procede de fabrication d'un alliage pour tube de reformage Download PDFInfo
- Publication number
- CA2963535A1 CA2963535A1 CA2963535A CA2963535A CA2963535A1 CA 2963535 A1 CA2963535 A1 CA 2963535A1 CA 2963535 A CA2963535 A CA 2963535A CA 2963535 A CA2963535 A CA 2963535A CA 2963535 A1 CA2963535 A1 CA 2963535A1
- Authority
- CA
- Canada
- Prior art keywords
- precipitates
- alloy
- type
- carbides
- microstructure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- 229910045601 alloy Inorganic materials 0.000 title claims abstract description 56
- 239000000956 alloy Substances 0.000 title claims abstract description 56
- 238000004519 manufacturing process Methods 0.000 title claims description 12
- 238000002407 reforming Methods 0.000 title claims description 12
- 239000002244 precipitate Substances 0.000 claims abstract description 56
- 150000001247 metal acetylides Chemical class 0.000 claims abstract description 23
- 229910052804 chromium Inorganic materials 0.000 claims abstract description 18
- 229910052759 nickel Inorganic materials 0.000 claims abstract description 13
- 229910052758 niobium Inorganic materials 0.000 claims abstract description 13
- 229910052742 iron Inorganic materials 0.000 claims abstract description 12
- 239000011159 matrix material Substances 0.000 claims abstract description 11
- 229910052719 titanium Inorganic materials 0.000 claims abstract description 11
- 238000007711 solidification Methods 0.000 claims abstract description 5
- 230000008023 solidification Effects 0.000 claims abstract description 5
- 239000011651 chromium Substances 0.000 claims description 25
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 22
- 238000000034 method Methods 0.000 claims description 15
- 230000008569 process Effects 0.000 claims description 14
- 238000010438 heat treatment Methods 0.000 claims description 13
- 239000000203 mixture Substances 0.000 claims description 13
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 12
- 239000000126 substance Substances 0.000 claims description 12
- 229910000599 Cr alloy Inorganic materials 0.000 claims description 4
- 229910000640 Fe alloy Inorganic materials 0.000 claims description 4
- 229910000990 Ni alloy Inorganic materials 0.000 claims description 4
- 230000001747 exhibiting effect Effects 0.000 claims description 4
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 3
- 230000005526 G1 to G0 transition Effects 0.000 claims description 3
- 229930195733 hydrocarbon Natural products 0.000 claims description 2
- 150000002430 hydrocarbons Chemical class 0.000 claims description 2
- -1 and/or M(C Inorganic materials 0.000 abstract description 8
- 230000004913 activation Effects 0.000 abstract 1
- 238000001556 precipitation Methods 0.000 description 19
- 239000010955 niobium Substances 0.000 description 14
- 239000010936 titanium Substances 0.000 description 8
- 230000032683 aging Effects 0.000 description 6
- 229910001566 austenite Inorganic materials 0.000 description 6
- 210000004027 cell Anatomy 0.000 description 6
- 230000005496 eutectics Effects 0.000 description 5
- 230000008859 change Effects 0.000 description 4
- 230000009466 transformation Effects 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
- 230000005540 biological transmission Effects 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 229910052799 carbon Inorganic materials 0.000 description 3
- 238000004581 coalescence Methods 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 230000006911 nucleation Effects 0.000 description 3
- 238000010899 nucleation Methods 0.000 description 3
- 238000003786 synthesis reaction Methods 0.000 description 3
- 238000011282 treatment Methods 0.000 description 3
- 238000002441 X-ray diffraction Methods 0.000 description 2
- 238000003483 aging Methods 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 229910052729 chemical element Inorganic materials 0.000 description 2
- 210000004443 dendritic cell Anatomy 0.000 description 2
- 230000006866 deterioration Effects 0.000 description 2
- 238000001887 electron backscatter diffraction Methods 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 238000010587 phase diagram Methods 0.000 description 2
- 230000035882 stress Effects 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000000788 chromium alloy Substances 0.000 description 1
- UFGZSIPAQKLCGR-UHFFFAOYSA-N chromium carbide Chemical compound [Cr]#C[Cr]C#[Cr] UFGZSIPAQKLCGR-UHFFFAOYSA-N 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000002028 premature Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229910021332 silicide Inorganic materials 0.000 description 1
- FVBUAEGBCNSCDD-UHFFFAOYSA-N silicide(4-) Chemical compound [Si-4] FVBUAEGBCNSCDD-UHFFFAOYSA-N 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 229910003470 tongbaite Inorganic materials 0.000 description 1
- 229910000859 α-Fe Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C1/00—Making non-ferrous alloys
- C22C1/02—Making non-ferrous alloys by melting
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
- C22C38/40—Ferrous alloys, e.g. steel alloys containing chromium with nickel
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D6/00—Heat treatment of ferrous alloys
- C21D6/004—Heat treatment of ferrous alloys containing Cr and Ni
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D6/00—Heat treatment of ferrous alloys
- C21D6/02—Hardening by precipitation
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D9/00—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
- C21D9/08—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for tubular bodies or pipes
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C30/00—Alloys containing less than 50% by weight of each constituent
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/02—Ferrous alloys, e.g. steel alloys containing silicon
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/04—Ferrous alloys, e.g. steel alloys containing manganese
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
- C22C38/40—Ferrous alloys, e.g. steel alloys containing chromium with nickel
- C22C38/44—Ferrous alloys, e.g. steel alloys containing chromium with nickel with molybdenum or tungsten
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
- C22C38/40—Ferrous alloys, e.g. steel alloys containing chromium with nickel
- C22C38/46—Ferrous alloys, e.g. steel alloys containing chromium with nickel with vanadium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
- C22C38/40—Ferrous alloys, e.g. steel alloys containing chromium with nickel
- C22C38/48—Ferrous alloys, e.g. steel alloys containing chromium with nickel with niobium or tantalum
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
- C22C38/40—Ferrous alloys, e.g. steel alloys containing chromium with nickel
- C22C38/50—Ferrous alloys, e.g. steel alloys containing chromium with nickel with titanium or zirconium
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D2211/00—Microstructure comprising significant phases
- C21D2211/001—Austenite
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D2211/00—Microstructure comprising significant phases
- C21D2211/004—Dispersions; Precipitations
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/50—Fuel cells
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Physics & Mathematics (AREA)
- Heat Treatment Of Steel (AREA)
- Solid-Phase Diffusion Into Metallic Material Surfaces (AREA)
- Powder Metallurgy (AREA)
- Manufacture Of Alloys Or Alloy Compounds (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
Microstructure d'un alliage pour tube pour reformeurs présentant une matrice austénitique caractérisée en ce que: i) des précipités primaires micrométriques sous la forme de carbures de type M23C6 avec M=Fe, Ni ou Cr et/ou de type M(C,N) avec M==Nb ou Ti se forment pendant la solidification de l'alliage : ii) des précipités secondaires nanométriques sous la forme de carbures de type M23C6 avec M=Fe, Ni ou Cr et de type M(C,N) avec M=Nb ou Ti se forment pendant la mise en service du tube; et iii) une quantité de précipités intermétalliques de type Ni16Si7Nb6 comprise entre 0,1 et 0,3 % se forme pendant l'utilisation du tube.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1459653 | 2014-10-08 | ||
| FR1459653A FR3027032B1 (fr) | 2014-10-08 | 2014-10-08 | Microstructure d'un alliage pour tube de reformage |
| PCT/FR2015/052483 WO2016055710A1 (fr) | 2014-10-08 | 2015-09-16 | Procédé de fabrication d'un alliage pour tube de reformage |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA2963535A1 true CA2963535A1 (fr) | 2016-04-14 |
Family
ID=52130420
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2963535A Abandoned CA2963535A1 (fr) | 2014-10-08 | 2015-09-16 | Procede de fabrication d'un alliage pour tube de reformage |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US10501831B2 (fr) |
| EP (1) | EP3204529B1 (fr) |
| CN (1) | CN106804111A (fr) |
| CA (1) | CA2963535A1 (fr) |
| ES (1) | ES2971742T3 (fr) |
| FR (1) | FR3027032B1 (fr) |
| WO (1) | WO2016055710A1 (fr) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112481445B (zh) * | 2020-11-30 | 2022-05-06 | 马鞍山市鑫龙特钢有限公司 | 一种提升40Cr合金钢材塑韧性的热加工工艺方法 |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5873950A (en) * | 1996-06-13 | 1999-02-23 | Inco Alloys International, Inc. | Strengthenable ethylene pyrolysis alloy |
| JP3888282B2 (ja) * | 2002-10-17 | 2007-02-28 | 住友金属工業株式会社 | オーステナイト系ステンレス鋼帯およびその製造方法 |
| EP1605073B1 (fr) * | 2003-03-20 | 2011-09-14 | Sumitomo Metal Industries, Ltd. | Utilisation d'un acier inoxydable austenitique |
| EP1605072B1 (fr) * | 2003-03-20 | 2012-09-12 | Sumitomo Metal Industries, Ltd. | Acier inoxydable destine a venir en contact avec du gaz hydrogene haute pression, cuve et equipement contenant ledit acier |
| WO2004111285A1 (fr) * | 2003-06-10 | 2004-12-23 | Sumitomo Metal Industries, Ltd. | Acier inoxydable austénitique destiné à être utilisé en présence d'hydrogène et procédé de production dudit acier |
| ES2395726T3 (es) * | 2003-10-20 | 2013-02-14 | Kubota Corporation | Acero colado termo-resistente para tubo de reacción de producción de hidrógeno siende excelente en cuanto a ductilidad frente al envejecimiento y resistencia frente a la ruptura por deformación plástica |
| EP1739200A1 (fr) * | 2005-06-28 | 2007-01-03 | UGINE & ALZ FRANCE | Bande en acier inoxydable austenitique présentant un aspect de surface brillant et d'excellentes caractéristiques mécaniques |
| DE102009039552B4 (de) * | 2009-09-01 | 2011-05-26 | Thyssenkrupp Vdm Gmbh | Verfahren zur Herstellung einer Eisen-Chrom-Legierung |
| CN103620077B (zh) * | 2011-06-24 | 2016-02-03 | 新日铁住金株式会社 | 耐渗碳性金属材料 |
| WO2016005724A1 (fr) * | 2014-07-10 | 2016-01-14 | Doncasters Paralloy | Alliage de faible ductilité |
| EP3176277B1 (fr) * | 2014-07-29 | 2020-05-06 | Nippon Steel & Sumikin Stainless Steel Corporation | Matériau d'acier inoxydable ferritique pour pile à combustible, et son procédé de production |
| GB201415624D0 (en) * | 2014-09-04 | 2014-10-22 | Doncasters Paralloy | Low strain high ductility alloy |
| WO2016099738A1 (fr) * | 2014-12-16 | 2016-06-23 | Exxonmobil Research And Engineering Company | Tubes de traitement de raffinerie de formation d'alumine avec élément de mélange |
-
2014
- 2014-10-08 FR FR1459653A patent/FR3027032B1/fr active Active
-
2015
- 2015-09-16 CA CA2963535A patent/CA2963535A1/fr not_active Abandoned
- 2015-09-16 ES ES15788461T patent/ES2971742T3/es active Active
- 2015-09-16 CN CN201580054879.0A patent/CN106804111A/zh active Pending
- 2015-09-16 US US15/517,405 patent/US10501831B2/en active Active
- 2015-09-16 WO PCT/FR2015/052483 patent/WO2016055710A1/fr active Application Filing
- 2015-09-16 EP EP15788461.0A patent/EP3204529B1/fr active Active
Also Published As
| Publication number | Publication date |
|---|---|
| FR3027032B1 (fr) | 2021-06-18 |
| WO2016055710A1 (fr) | 2016-04-14 |
| US20170298484A1 (en) | 2017-10-19 |
| CN106804111A (zh) | 2017-06-06 |
| FR3027032A1 (fr) | 2016-04-15 |
| EP3204529A1 (fr) | 2017-08-16 |
| EP3204529B1 (fr) | 2024-01-24 |
| ES2971742T3 (es) | 2024-06-06 |
| US10501831B2 (en) | 2019-12-10 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FZDE | Discontinued |
Effective date: 20211207 |
|
| FZDE | Discontinued |
Effective date: 20211207 |