CA2935611C - Method for extracting lignin - Google Patents

Method for extracting lignin Download PDF

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Publication number
CA2935611C
CA2935611C CA2935611A CA2935611A CA2935611C CA 2935611 C CA2935611 C CA 2935611C CA 2935611 A CA2935611 A CA 2935611A CA 2935611 A CA2935611 A CA 2935611A CA 2935611 C CA2935611 C CA 2935611C
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CA
Canada
Prior art keywords
extraction
lignin
biomass
aqueous solution
reaction mixture
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Active
Application number
CA2935611A
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English (en)
French (fr)
Other versions
CA2935611A1 (en
Inventor
Sebastian VON SCHOULTZ
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
CH-Bioforce Oy
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CH-Bioforce Oy
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by CH-Bioforce Oy filed Critical CH-Bioforce Oy
Publication of CA2935611A1 publication Critical patent/CA2935611A1/en
Application granted granted Critical
Publication of CA2935611C publication Critical patent/CA2935611C/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07G—COMPOUNDS OF UNKNOWN CONSTITUTION
    • C07G1/00—Low-molecular-weight derivatives of lignin
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B1/00—Preparatory treatment of cellulose for making derivatives thereof, e.g. pre-treatment, pre-soaking, activation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08H—DERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
    • C08H6/00—Macromolecular compounds derived from lignin, e.g. tannins, humic acids
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
    • C10L5/00—Solid fuels
    • C10L5/02—Solid fuels such as briquettes consisting mainly of carbonaceous materials of mineral or non-mineral origin
    • C10L5/34—Other details of the shaped fuels, e.g. briquettes
    • C10L5/36—Shape
    • C10L5/363—Pellets or granulates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
    • C10L5/00—Solid fuels
    • C10L5/40—Solid fuels essentially based on materials of non-mineral origin
    • C10L5/44—Solid fuels essentially based on materials of non-mineral origin on vegetable substances
    • C10L5/442—Wood or forestry waste
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C1/00—Pretreatment of the finely-divided materials before digesting
    • D21C1/10—Physical methods for facilitating impregnation
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C3/00—Pulping cellulose-containing materials
    • D21C3/02—Pulping cellulose-containing materials with inorganic bases or alkaline reacting compounds, e.g. sulfate processes
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C3/00—Pulping cellulose-containing materials
    • D21C3/04—Pulping cellulose-containing materials with acids, acid salts or acid anhydrides
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C3/00—Pulping cellulose-containing materials
    • D21C3/22—Other features of pulping processes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
    • C10L2200/00—Components of fuel compositions
    • C10L2200/04—Organic compounds
    • C10L2200/0461—Fractions defined by their origin
    • C10L2200/0469—Renewables or materials of biological origin
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
    • C10L2290/00—Fuel preparation or upgrading, processes or apparatus therefore, comprising specific process steps or apparatus units
    • C10L2290/06—Heat exchange, direct or indirect
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
    • C10L2290/00—Fuel preparation or upgrading, processes or apparatus therefore, comprising specific process steps or apparatus units
    • C10L2290/30—Pressing, compressing or compacting
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
    • C10L2290/00—Fuel preparation or upgrading, processes or apparatus therefore, comprising specific process steps or apparatus units
    • C10L2290/54—Specific separation steps for separating fractions, components or impurities during preparation or upgrading of a fuel
    • C10L2290/544—Extraction for separating fractions, components or impurities during preparation or upgrading of a fuel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/30—Fuel from waste, e.g. synthetic alcohol or diesel

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Inorganic Chemistry (AREA)
  • Biochemistry (AREA)
  • Materials Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Biodiversity & Conservation Biology (AREA)
  • Ecology (AREA)
  • Forests & Forestry (AREA)
  • Wood Science & Technology (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)
  • Processing Of Solid Wastes (AREA)
  • Compounds Of Unknown Constitution (AREA)
  • Paper (AREA)
CA2935611A 2014-01-10 2015-01-09 Method for extracting lignin Active CA2935611C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FI20145018 2014-01-10
FI20145018A FI127582B (en) 2014-01-10 2014-01-10 Procedure for extracting lignin
PCT/FI2015/050011 WO2015104460A1 (en) 2014-01-10 2015-01-09 Method for extracting lignin

Publications (2)

Publication Number Publication Date
CA2935611A1 CA2935611A1 (en) 2015-07-16
CA2935611C true CA2935611C (en) 2022-09-20

Family

ID=52423729

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2935611A Active CA2935611C (en) 2014-01-10 2015-01-09 Method for extracting lignin

Country Status (11)

Country Link
US (1) US10407452B2 (enExample)
EP (1) EP3092337B1 (enExample)
CN (1) CN106029978B (enExample)
BR (1) BR112016015776B1 (enExample)
CA (1) CA2935611C (enExample)
ES (1) ES2994201T3 (enExample)
FI (1) FI127582B (enExample)
HU (1) HUE069996T2 (enExample)
PL (1) PL3092337T3 (enExample)
RU (1) RU2682348C2 (enExample)
WO (1) WO2015104460A1 (enExample)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20140271443A1 (en) * 2013-03-15 2014-09-18 University Of Tennessee Research Foundation High Glass Transition Lignins and Lignin Derivatives for the Manufacture of Carbon and Graphite Fibers
SG10202107085TA (en) 2015-04-10 2021-08-30 Comet Biorefining Inc Methods and compositions for the treatment of cellulosic biomass and products produced thereby
CN107487871A (zh) * 2017-09-19 2017-12-19 常州市丰瑞电子有限公司 一种环保型无磷缓蚀阻垢剂的制备方法
CN108179644B (zh) * 2017-12-21 2019-11-12 中国科学院青岛生物能源与过程研究所 一种从生物质中提取木质素的方法
CN120092937A (zh) 2018-05-10 2025-06-06 彗星生物炼制公司 含有葡萄糖和半纤维素的组合物及其用途
PH12021552859A1 (en) 2019-05-10 2022-12-19 Comet Biorefining Inc Materials and methods for producing arabinoxylan compositions
BR112022005525A2 (pt) * 2019-09-25 2022-06-21 Shell Int Research Pré-tratamento de alimentos lignocelulósicos para a produção de glicóis
DE102020101915A1 (de) * 2020-01-28 2021-07-29 Holger Wondraczek Verfahren zum Extrahieren von Xylanverbindungen aus zerkleinerten Holzbestandteilen
CN111958730B (zh) * 2020-08-10 2021-12-07 齐鲁工业大学 抑制木质素缩合的方法

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1008104B (de) * 1955-11-17 1957-05-09 Escher Wyss Gmbh Einrichtung zum kontinuierlichen Evakuieren und Traenken von faserhaltigen Stoffen der Zellstoffindustrie
US3278367A (en) * 1963-02-14 1966-10-11 Aqua Chem Inc Method of producing wood pulp including steaming, vacuum, and impregnation
US5207870A (en) * 1988-02-08 1993-05-04 Osmo Aho Process and equipment for pretreatment of cellulosic raw material
DE19916347C1 (de) * 1999-04-12 2000-11-09 Rhodia Acetow Ag Verfahren zum Auftrennen lignocellulosehaltiger Biomasse
BRPI0612944B1 (pt) * 2005-04-12 2017-11-28 E.I.Du Pont De Nemours And Company Method of production of target substance
BRPI0621525B1 (pt) 2006-03-29 2016-06-14 Virginia Tech Intell Prop processos para fracionar biomssa lignocelulosica baseado em celulose-solvente com condições reacionais moderadas e reciclagem dos reagentes
US20090098617A1 (en) * 2007-10-10 2009-04-16 Murray Burke Enzymatic treatment under vacuum of lignocellulosic materials
EP2421911B1 (en) * 2009-04-23 2014-06-18 Greenfield Ethanol Inc. Separation of reactive cellulose from lignocellulosic biomass with high lignin content
US8986437B2 (en) 2009-10-23 2015-03-24 David H. Blount Delignification of biomass containing lignin and production of adhesive and methods of making lignin cellulose compositions
EP2580245A1 (en) 2010-06-10 2013-04-17 Lali, Arvind Mallinath Process for fractionation of biomass
US20120125551A1 (en) * 2010-11-23 2012-05-24 E. I. Du Pont De Nemours And Company Biomass pretreatment process for a packed bed reactor
ITTO20120012A1 (it) * 2012-01-11 2013-07-12 Beta Renewables Spa Fase di idrolisi migliorata condotta sotto vuoto.
WO2013124461A2 (en) 2012-02-24 2013-08-29 Chemtex Italia S.P.A. Continuous process for conversion of lignin to useful compounds
CN103122594B (zh) 2012-11-19 2014-03-12 山东轻工业学院 一种溶解浆的生产方法
US20150045543A1 (en) * 2013-08-12 2015-02-12 Melvin Mitchell Isolation method for water insoluble components of a biomass and products provided therefrom
CA2927330A1 (en) * 2013-10-15 2015-04-23 Cellulosic Ethanol Technologies, Llc Process and system for high solids fermentation

Also Published As

Publication number Publication date
BR112016015776B1 (pt) 2022-07-12
RU2016127258A (ru) 2018-02-14
US10407452B2 (en) 2019-09-10
WO2015104460A1 (en) 2015-07-16
CA2935611A1 (en) 2015-07-16
FI20145018A7 (fi) 2015-07-11
EP3092337A1 (en) 2016-11-16
US20160326203A1 (en) 2016-11-10
CN106029978B (zh) 2021-08-20
RU2682348C2 (ru) 2019-03-19
ES2994201T3 (en) 2025-01-20
CN106029978A (zh) 2016-10-12
EP3092337C0 (en) 2024-10-23
EP3092337B1 (en) 2024-10-23
BR112016015776A2 (enExample) 2017-08-08
RU2016127258A3 (enExample) 2018-08-02
HUE069996T2 (hu) 2025-04-28
FI127582B (en) 2018-09-14
PL3092337T3 (pl) 2025-02-24

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