CA2861294C - Polymorphs of n- (2 -methoxybenzoyl) -4- [(methylaminocarbonyl) amino] benzenesulfonamide - Google Patents

Polymorphs of n- (2 -methoxybenzoyl) -4- [(methylaminocarbonyl) amino] benzenesulfonamide Download PDF

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Publication number
CA2861294C
CA2861294C CA2861294A CA2861294A CA2861294C CA 2861294 C CA2861294 C CA 2861294C CA 2861294 A CA2861294 A CA 2861294A CA 2861294 A CA2861294 A CA 2861294A CA 2861294 C CA2861294 C CA 2861294C
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CA
Canada
Prior art keywords
polymorph
powder
ray diffraction
diffraction pattern
herbicide
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Active
Application number
CA2861294A
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English (en)
French (fr)
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CA2861294A1 (en
Inventor
Ian Kevin Jones
Neil George
John Hone
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Syngenta Ltd
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Syngenta Ltd
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Publication of CA2861294A1 publication Critical patent/CA2861294A1/en
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Publication of CA2861294C publication Critical patent/CA2861294C/en
Active legal-status Critical Current
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C311/00—Amides of sulfonic acids, i.e. compounds having singly-bound oxygen atoms of sulfo groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
    • C07C311/30—Sulfonamides, the carbon skeleton of the acid part being further substituted by singly-bound nitrogen atoms, not being part of nitro or nitroso groups
    • C07C311/45—Sulfonamides, the carbon skeleton of the acid part being further substituted by singly-bound nitrogen atoms, not being part of nitro or nitroso groups at least one of the singly-bound nitrogen atoms being part of any of the groups, X being a hetero atom, Y being any atom, e.g. N-acylaminosulfonamides
    • C07C311/46—Y being a hydrogen or a carbon atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C311/00—Amides of sulfonic acids, i.e. compounds having singly-bound oxygen atoms of sulfo groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
    • C07C311/50—Compounds containing any of the groups, X being a hetero atom, Y being any atom
    • C07C311/51—Y being a hydrogen or a carbon atom
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/32—Ingredients for reducing the noxious effect of the active substances to organisms other than pests, e.g. toxicity reducing compositions, self-destructing compositions
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
    • A01N47/30—Derivatives containing the group >N—CO—N aryl or >N—CS—N—aryl
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/42—Separation; Purification; Stabilisation; Use of additives
    • C07C303/44—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/13—Crystalline forms, e.g. polymorphs

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  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Plant Pathology (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Agronomy & Crop Science (AREA)
  • Toxicology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CA2861294A 2012-02-09 2013-02-08 Polymorphs of n- (2 -methoxybenzoyl) -4- [(methylaminocarbonyl) amino] benzenesulfonamide Active CA2861294C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
GB1202393.3 2012-02-09
GBGB1202393.3A GB201202393D0 (en) 2012-02-09 2012-02-09 Polymorphs
PCT/EP2013/052534 WO2013117691A1 (en) 2012-02-09 2013-02-08 Polymorphs of n- (2 -methoxybenzoyl) -4- [ (methylaminocarbonyl) amino] benzenesulfonamide

Publications (2)

Publication Number Publication Date
CA2861294A1 CA2861294A1 (en) 2013-08-15
CA2861294C true CA2861294C (en) 2021-01-26

Family

ID=45929988

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2861294A Active CA2861294C (en) 2012-02-09 2013-02-08 Polymorphs of n- (2 -methoxybenzoyl) -4- [(methylaminocarbonyl) amino] benzenesulfonamide

Country Status (21)

Country Link
US (2) US9284269B2 (cg-RX-API-DMAC7.html)
EP (1) EP2812312B1 (cg-RX-API-DMAC7.html)
JP (1) JP2015506968A (cg-RX-API-DMAC7.html)
KR (1) KR102011475B1 (cg-RX-API-DMAC7.html)
CN (2) CN106431999A (cg-RX-API-DMAC7.html)
AU (1) AU2013217972B2 (cg-RX-API-DMAC7.html)
BR (1) BR112014019669B1 (cg-RX-API-DMAC7.html)
CA (1) CA2861294C (cg-RX-API-DMAC7.html)
CO (1) CO7061088A2 (cg-RX-API-DMAC7.html)
DK (1) DK2812312T3 (cg-RX-API-DMAC7.html)
EA (1) EA027024B1 (cg-RX-API-DMAC7.html)
ES (1) ES2637329T3 (cg-RX-API-DMAC7.html)
GB (1) GB201202393D0 (cg-RX-API-DMAC7.html)
HU (2) HUE033170T2 (cg-RX-API-DMAC7.html)
MX (1) MX346113B (cg-RX-API-DMAC7.html)
MY (1) MY169048A (cg-RX-API-DMAC7.html)
PL (1) PL2812312T3 (cg-RX-API-DMAC7.html)
RS (1) RS56170B1 (cg-RX-API-DMAC7.html)
UA (1) UA113540C2 (cg-RX-API-DMAC7.html)
WO (1) WO2013117691A1 (cg-RX-API-DMAC7.html)
ZA (1) ZA201405452B (cg-RX-API-DMAC7.html)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
UA119191C2 (uk) 2014-12-15 2019-05-10 Байєр Кропсайєнс Акцієнгезелльшафт Кристалічні форми мононатрієвої солі форамсульфурону
KR102566177B1 (ko) 2016-12-20 2023-08-14 에프엠씨 코포레이션 제초성 술폰아미드의 다형체
CA3047050A1 (en) * 2016-12-22 2018-06-28 Syngenta Participations Ag Polymorphs
GB201622007D0 (en) * 2016-12-22 2017-02-08 And See Cambridge Display Tech Ltd Syngenta Participations Ag Polymorphs
US11634442B2 (en) * 2017-07-18 2023-04-25 Basf Se Methods for the purification of L-glufosinate
EP4521930A1 (en) 2022-05-10 2025-03-19 Syngenta Crop Protection AG Composition and method for controlling weeds
WO2023222725A1 (en) 2022-05-16 2023-11-23 Syngenta Crop Protection Ag Composition and method for controlling weeds in turfgrass
CN118702704A (zh) * 2023-06-19 2024-09-27 江苏艾迪药业股份有限公司 多环氨基甲酰基吡啶酮衍生物的钠盐晶型及其制备方法和应用

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4834908A (en) 1987-10-05 1989-05-30 Basf Corporation Antagonism defeating crop oil concentrates
ES2054088T3 (es) * 1988-10-20 1994-08-01 Ciba Geigy Ag Sulfamoilfenilureas.
US5215570A (en) 1988-10-20 1993-06-01 Ciba-Geigy Corporation Sulfamoylphenylureas
JP3298158B2 (ja) * 1992-07-06 2002-07-02 住友化学工業株式会社 カーバメート化合物およびその製造方法
EA001470B1 (ru) 1996-03-15 2001-04-23 Новартис Аг Синергетическая гербицидная композиция и способ борьбы с сорняками
DE19621522A1 (de) * 1996-05-29 1997-12-04 Hoechst Schering Agrevo Gmbh Neue N-Acylsulfonamide, neue Mischungen aus Herbiziden und Antidots und deren Verwendung
DE19742951A1 (de) * 1997-09-29 1999-04-15 Hoechst Schering Agrevo Gmbh Acylsulfamoylbenzoesäureamide, diese enthaltende nutzpflanzenschützende Mittel und Verfahren zu ihrer Herstellung
DE19827855A1 (de) * 1998-06-23 1999-12-30 Hoechst Schering Agrevo Gmbh Kombinationen aus Herbiziden und Safenern
DE19961465A1 (de) * 1998-12-21 2000-07-06 Novartis Ag Herbizides Mittel
JP2004002393A (ja) * 2002-04-19 2004-01-08 Nissan Chem Ind Ltd 結晶多形インド−ル化合物およびその製造方法
JP4484023B2 (ja) * 2003-10-14 2010-06-16 日産化学工業株式会社 保存安定性の良好な農薬組成物
CN102977011A (zh) * 2005-11-23 2013-03-20 马克特辛姆化学工厂有限公司 制备吡啶胺及其新型多晶形物的方法
NZ575890A (en) * 2006-10-13 2011-07-29 Basf Se Anhydrous crystalline phenyluracil
WO2009007344A1 (en) * 2007-07-12 2009-01-15 Basf Se Novel crystalline form of 3-(difluormethyl)-1-methyl-n -(3',4',5'-trifluor[1,1'-biphenyl]-2-yl)-1h-pyrazol-4-carboxamide
US20100304967A1 (en) * 2007-11-01 2010-12-02 Syngenta Crop Protection, Inc. Method of protecting rice crops
CN102884050B (zh) * 2010-02-23 2014-05-28 日本化药株式会社 2-乙基-3,7-二甲基-6-(4-(三氟甲氧基)苯氧基)喹啉-4-基甲基碳酸酯的稳定晶体、其制备方法以及包含该晶体的农用化学组合物

Also Published As

Publication number Publication date
CA2861294A1 (en) 2013-08-15
US20160152562A1 (en) 2016-06-02
GB201202393D0 (en) 2012-03-28
DK2812312T3 (en) 2017-08-21
AU2013217972A1 (en) 2014-08-14
RS56170B1 (sr) 2017-11-30
HUE033170T2 (en) 2017-11-28
WO2013117691A1 (en) 2013-08-15
PL2812312T3 (pl) 2017-10-31
KR102011475B1 (ko) 2019-08-16
UA113540C2 (xx) 2017-02-10
MX346113B (es) 2017-03-08
ZA201405452B (en) 2015-10-28
BR112014019669A8 (pt) 2017-07-11
HUS2300030I1 (hu) 2023-10-28
CN106431999A (zh) 2017-02-22
EA027024B1 (ru) 2017-06-30
BR112014019669B1 (pt) 2020-11-17
EP2812312B1 (en) 2017-05-31
AU2013217972B2 (en) 2016-11-24
US9475765B2 (en) 2016-10-25
EP2812312A1 (en) 2014-12-17
MY169048A (en) 2019-02-08
JP2015506968A (ja) 2015-03-05
CN104114536A (zh) 2014-10-22
US9284269B2 (en) 2016-03-15
MX2014009617A (es) 2014-11-10
KR20140123542A (ko) 2014-10-22
ES2637329T3 (es) 2017-10-11
CO7061088A2 (es) 2014-09-19
US20150005166A1 (en) 2015-01-01
EA201400881A1 (ru) 2015-01-30
BR112014019669A2 (cg-RX-API-DMAC7.html) 2017-06-20

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