CA2306256A1 - Radiation activation and screening of catalyst libraries for catalyst evaluation and reactors therefor - Google Patents

Radiation activation and screening of catalyst libraries for catalyst evaluation and reactors therefor Download PDF

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Publication number
CA2306256A1
CA2306256A1 CA002306256A CA2306256A CA2306256A1 CA 2306256 A1 CA2306256 A1 CA 2306256A1 CA 002306256 A CA002306256 A CA 002306256A CA 2306256 A CA2306256 A CA 2306256A CA 2306256 A1 CA2306256 A1 CA 2306256A1
Authority
CA
Canada
Prior art keywords
catalyst
product
reactant
screening
microreactor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
CA002306256A
Other languages
English (en)
French (fr)
Inventor
Martin Philip Atkins
Selim Mehmet Senkan
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
LASER CATALYST SYSTEMS Inc
BP Chemicals Ltd
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from GBGB9807836.3A external-priority patent/GB9807836D0/en
Application filed by Individual filed Critical Individual
Publication of CA2306256A1 publication Critical patent/CA2306256A1/en
Abandoned legal-status Critical Current

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Classifications

    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J49/00—Particle spectrometers or separator tubes
    • H01J49/02—Details
    • H01J49/10—Ion sources; Ion guns
    • H01J49/16—Ion sources; Ion guns using surface ionisation, e.g. field-, thermionic- or photo-emission
    • H01J49/161—Ion sources; Ion guns using surface ionisation, e.g. field-, thermionic- or photo-emission using photoionisation, e.g. by laser
    • H01J49/162—Direct photo-ionisation, e.g. single photon or multi-photon ionisation
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
    • G01N31/10—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using catalysis
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0046—Sequential or parallel reactions, e.g. for the synthesis of polypeptides or polynucleotides; Apparatus and devices for combinatorial chemistry or for making molecular arrays
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00279—Features relating to reactor vessels
    • B01J2219/00306—Reactor vessels in a multiple arrangement
    • B01J2219/00313—Reactor vessels in a multiple arrangement the reactor vessels being formed by arrays of wells in blocks
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00497—Features relating to the solid phase supports
    • B01J2219/00527—Sheets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00583—Features relative to the processes being carried out
    • B01J2219/00585—Parallel processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00583—Features relative to the processes being carried out
    • B01J2219/00596—Solid-phase processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00583—Features relative to the processes being carried out
    • B01J2219/00603—Making arrays on substantially continuous surfaces
    • B01J2219/00605—Making arrays on substantially continuous surfaces the compounds being directly bound or immobilised to solid supports
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00583—Features relative to the processes being carried out
    • B01J2219/00603—Making arrays on substantially continuous surfaces
    • B01J2219/00659—Two-dimensional arrays
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/0068—Means for controlling the apparatus of the process
    • B01J2219/00702—Processes involving means for analysing and characterising the products
    • B01J2219/00707—Processes involving means for analysing and characterising the products separated from the reactor apparatus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00718—Type of compounds synthesised
    • B01J2219/00745—Inorganic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00718—Type of compounds synthesised
    • B01J2219/00745—Inorganic compounds
    • B01J2219/00747—Catalysts
    • C—CHEMISTRY; METALLURGY
    • C40—COMBINATORIAL TECHNOLOGY
    • C40B—COMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
    • C40B30/00—Methods of screening libraries
    • C40B30/08—Methods of screening libraries by measuring catalytic activity
    • C—CHEMISTRY; METALLURGY
    • C40—COMBINATORIAL TECHNOLOGY
    • C40B—COMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
    • C40B40/00—Libraries per se, e.g. arrays, mixtures
    • C40B40/18—Libraries containing only inorganic compounds or inorganic materials
    • C—CHEMISTRY; METALLURGY
    • C40—COMBINATORIAL TECHNOLOGY
    • C40B—COMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
    • C40B60/00—Apparatus specially adapted for use in combinatorial chemistry or with libraries
    • C40B60/14—Apparatus specially adapted for use in combinatorial chemistry or with libraries for creating libraries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Molecular Biology (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Organic Chemistry (AREA)
  • Optics & Photonics (AREA)
  • Engineering & Computer Science (AREA)
  • Plasma & Fusion (AREA)
  • Catalysts (AREA)
  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
CA002306256A 1997-10-10 1998-10-08 Radiation activation and screening of catalyst libraries for catalyst evaluation and reactors therefor Abandoned CA2306256A1 (en)

Applications Claiming Priority (7)

Application Number Priority Date Filing Date Title
US94920397A 1997-10-10 1997-10-10
US08/949,203 1997-10-10
GB9807836.3 1998-04-14
GBGB9807836.3A GB9807836D0 (en) 1998-04-14 1998-04-14 Reactors
US8741798A 1998-05-29 1998-05-29
US09/087,417 1998-05-29
PCT/GB1998/003023 WO1999019724A1 (en) 1997-10-10 1998-10-08 Radiation activation and screening of catalyst libraries for catalyst evaluation and reactors therefor

Publications (1)

Publication Number Publication Date
CA2306256A1 true CA2306256A1 (en) 1999-04-22

Family

ID=27269278

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002306256A Abandoned CA2306256A1 (en) 1997-10-10 1998-10-08 Radiation activation and screening of catalyst libraries for catalyst evaluation and reactors therefor

Country Status (12)

Country Link
EP (1) EP1019713A1 (de)
JP (1) JP2001520380A (de)
KR (1) KR20010031021A (de)
CN (1) CN1281551A (de)
AU (1) AU736438B2 (de)
BR (1) BR9812909A (de)
CA (1) CA2306256A1 (de)
ID (1) ID24631A (de)
NO (1) NO20001787L (de)
NZ (1) NZ503731A (de)
PL (1) PL339834A1 (de)
WO (1) WO1999019724A1 (de)

Families Citing this family (37)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6426226B1 (en) 1997-10-10 2002-07-30 Laboratory Catalyst Systems Llc Method and apparatus for screening catalyst libraries
DE19822077A1 (de) * 1998-05-16 1999-11-18 Studiengesellschaft Kohle Mbh Kombinatorisches Verfahren zur Herstellung und Charakterisierung von kristallinen und amorphen Materialbibliotheken im Mikrogramm-Maßstab
US6240790B1 (en) * 1998-11-09 2001-06-05 Agilent Technologies, Inc. Device for high throughout sample processing, analysis and collection, and methods of use thereof
NZ511228A (en) * 1998-11-12 2003-01-31 Bp Chem Int Ltd Method and apparatus for screening catalyst libraries using addressable microreactors
US7491677B2 (en) 1999-01-15 2009-02-17 Basf Catalysts Llc Combinatorial synthesis
US6749814B1 (en) * 1999-03-03 2004-06-15 Symyx Technologies, Inc. Chemical processing microsystems comprising parallel flow microreactors and methods for using same
DE19913076A1 (de) * 1999-03-23 2000-10-19 Hahn Schickard Ges Vorrichtung und Verfahren zum Aufbringen von Mikrotröpfchen auf ein Substrat
WO2001034290A2 (en) 1999-11-09 2001-05-17 Sri International Array for generating combinatorial libraries
DE19959974A1 (de) * 1999-12-13 2001-06-21 Basf Ag Verfahren zur Herstellung von Materialbibliotheken durch elektrochemische Abscheidung
US6770245B2 (en) 1999-12-15 2004-08-03 Uop Llc Multiple parallel processing assembly
US6627445B1 (en) 1999-12-15 2003-09-30 Uop Llc Process for simultaneously evaluating a plurality of catalysts
US6342185B1 (en) 1999-12-15 2002-01-29 Uop Llc Combinatorial catalytic reactor
US6368865B1 (en) 1999-12-15 2002-04-09 Uop Llc Combinatorial process for performing catalytic chemical reactions
CA2327419C (en) 1999-12-15 2009-01-13 Uop Llc Combinatorial catalytic reactor
US6776963B1 (en) 1999-12-15 2004-08-17 Uop Llc Multiple parallel catalytic reactor assembly
US6576196B1 (en) 1999-12-15 2003-06-10 Uop Llc Multiple parallel catalytic reactor assembly
DE10004816A1 (de) 2000-02-04 2001-08-09 Hte Gmbh Verfahren und Vorrichtung zur kombinatorischen Herstellung und Testung von Materialbibliotheken durch photoakustische Analysemethoden
US6627571B1 (en) 2000-03-01 2003-09-30 Symyx Technologies, Inc. Method and system for the situ synthesis of a combinatorial library of supported catalyst materials
DE10012847A1 (de) 2000-03-16 2001-09-27 Hte Gmbh Verfahren und Vorrichtung zur kombinatorischen Herstellung und Testung von Materialbibliotheken durch Anwendung mindestens zweier Analysemethoden
WO2002004112A2 (en) 2000-07-07 2002-01-17 Symyx Technologies, Inc. Methods for analysis of heterogeneous catalysts in a multi-variable screening reactor
DE10036633B4 (de) * 2000-07-27 2005-03-10 Hte Ag The High Throughput Exp Anordnung in modularer Bauweise und Verfahren zur paralellen Testung einer Mehrzahl von Bausteinen einer Materialbibliothek
AU2001283076A1 (en) * 2000-08-14 2002-02-25 Chevron U.S.A. Inc. Use of microchannel reactors in combinatorial chemistry
GB2366793B (en) * 2000-09-13 2005-03-09 Imperial College Chemical processing system and method
US6923939B1 (en) 2001-07-05 2005-08-02 Uop Llc Heat activated membrane introduction apparatus and method for screening materials
US6974665B2 (en) 2001-09-06 2005-12-13 University Of Nebraska In situ screening to optimize variables in organic reactions
US6808685B2 (en) 2001-09-17 2004-10-26 Uop Llc Apparatus and method for generating a plurality of isolated effluents
US7063982B1 (en) 2002-03-12 2006-06-20 Uop Llc Process of vaporizing and reacting a liquid feed
US6989131B2 (en) 2002-03-12 2006-01-24 Uop Llc Catalytic reactor with integral evaporator
US20030173205A1 (en) 2002-03-12 2003-09-18 Arne Karlsson Process vessel with integral evaporator
US6949267B2 (en) 2002-04-08 2005-09-27 Engelhard Corporation Combinatorial synthesis
ES2199080B1 (es) * 2002-07-16 2005-02-16 Universidad Politecnica De Valencia Soporte rotatorio y aparato para la caracterizacion multiple espectroscopica de muestras de materiales solidos.
DE10234564B4 (de) * 2002-07-25 2005-06-02 Senslab-Gesellschaft Zur Entwicklung Und Herstellung Bioelektrochemischer Sensoren Mbh Biosensor
US7141217B2 (en) 2002-12-05 2006-11-28 Uop Llc Elevated pressure apparatus and method for generating a plurality of isolated effluents
US7267987B2 (en) 2003-01-06 2007-09-11 Uop Llc Process and assembly for simultaneously evaluating a plurality of catalysts
JP4630263B2 (ja) * 2006-11-27 2011-02-09 古河電気工業株式会社 マイクロ化学反応装置
JP4532458B2 (ja) * 2006-11-27 2010-08-25 古河電気工業株式会社 マイクロ化学反応装置
JP4630264B2 (ja) * 2006-11-27 2011-02-09 古河電気工業株式会社 マイクロ化学反応装置の製造方法

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4099923A (en) * 1977-01-17 1978-07-11 The Standard Oil Company Automatic catalytic screening unit
JP2769205B2 (ja) * 1989-09-16 1998-06-25 株式会社日立製作所 粒子状物質の分析方法、その装置及びこれを利用した超純水製造管理システム
US6063633A (en) * 1996-02-28 2000-05-16 The University Of Houston Catalyst testing process and apparatus

Also Published As

Publication number Publication date
CN1281551A (zh) 2001-01-24
KR20010031021A (ko) 2001-04-16
JP2001520380A (ja) 2001-10-30
WO1999019724A1 (en) 1999-04-22
NO20001787D0 (no) 2000-04-06
AU736438B2 (en) 2001-07-26
NO20001787L (no) 2000-06-09
EP1019713A1 (de) 2000-07-19
BR9812909A (pt) 2002-02-05
AU9449498A (en) 1999-05-03
PL339834A1 (en) 2001-01-02
ID24631A (id) 2000-07-27
NZ503731A (en) 2001-05-25

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