CA2296699A1 - Purification of hydroxylamine - Google Patents

Purification of hydroxylamine Download PDF

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Publication number
CA2296699A1
CA2296699A1 CA002296699A CA2296699A CA2296699A1 CA 2296699 A1 CA2296699 A1 CA 2296699A1 CA 002296699 A CA002296699 A CA 002296699A CA 2296699 A CA2296699 A CA 2296699A CA 2296699 A1 CA2296699 A1 CA 2296699A1
Authority
CA
Canada
Prior art keywords
hydroxylamine
purification
ion exchange
bed
acid ion
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CA002296699A
Other languages
French (fr)
Other versions
CA2296699C (en
Inventor
Floyd L. Riddle
Francis W. Michelotti
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Air Products and Chemicals Inc
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of CA2296699A1 publication Critical patent/CA2296699A1/en
Application granted granted Critical
Publication of CA2296699C publication Critical patent/CA2296699C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/14—Hydroxylamine; Salts thereof
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/14—Hydroxylamine; Salts thereof
    • C01B21/1481—Purification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Treatment Of Water By Ion Exchange (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Physical Water Treatments (AREA)
  • Removal Of Specific Substances (AREA)
  • Polarising Elements (AREA)
  • Electrical Discharge Machining, Electrochemical Machining, And Combined Machining (AREA)
  • Seal Device For Vehicle (AREA)

Abstract

The invention provides a method for purification of hydroxylamine so as to have a substantial reduction of cations and anions. The method involves passing a solution of hydroxylamine through at least one strong acid ion exchange bed and then through at least one strong base anion exchange resin bed. The strong acid ion exchange bed is preconditioned with dilute hydrochloric acid.
CA002296699A 1997-07-16 1998-05-21 Purification of hydroxylamine Expired - Fee Related CA2296699C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US08/895,361 1997-07-16
US08/895,361 US5788946A (en) 1997-07-16 1997-07-16 Purification of hydroxylamine
PCT/US1998/010445 WO1999003780A1 (en) 1997-07-16 1998-05-21 Purification of hydroxylamine

Publications (2)

Publication Number Publication Date
CA2296699A1 true CA2296699A1 (en) 1999-01-28
CA2296699C CA2296699C (en) 2003-08-05

Family

ID=25404400

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002296699A Expired - Fee Related CA2296699C (en) 1997-07-16 1998-05-21 Purification of hydroxylamine

Country Status (16)

Country Link
US (1) US5788946A (en)
EP (1) EP1017621B1 (en)
JP (1) JP3567206B2 (en)
KR (1) KR100485849B1 (en)
CN (1) CN1130307C (en)
AT (1) ATE246145T1 (en)
AU (1) AU7500898A (en)
CA (1) CA2296699C (en)
DE (1) DE69816842T2 (en)
DK (1) DK1017621T3 (en)
ES (1) ES2203954T3 (en)
ID (1) ID22371A (en)
MY (1) MY118717A (en)
NO (1) NO20000203L (en)
TW (1) TW424081B (en)
WO (1) WO1999003780A1 (en)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19806578A1 (en) 1998-02-17 1999-08-19 Basf Ag Production of aqueous hydroxylamine solution containing essentially no metal ions, used in electronics industry
US7329354B2 (en) * 1998-06-09 2008-02-12 Ppt Technologies, Llc Purification of organic solvent fluids
DE19936594A1 (en) 1999-08-04 2001-02-08 Basf Ag Process for the preparation of high-purity stabilized hydroxylamine solutions
US6355179B1 (en) 1999-12-10 2002-03-12 Basf Corporation Decomposition of residual hydroxylamine by hydrogen peroxide treatment
US6350614B1 (en) * 2000-02-07 2002-02-26 Concept Sciences, Inc System for the ion exchange purification of hydroxylamine
JP4582602B2 (en) * 2000-03-24 2010-11-17 ビーエーエスエフ ソシエタス・ヨーロピア Hydroxylamine aqueous solution and process for producing the same
ATE315004T1 (en) * 2001-09-06 2006-02-15 IMPROVED METHOD FOR PRODUCING HIGHLY CONCENTRATED HYDROXYLAMINE SOLUTIONS
US20060077958A1 (en) * 2004-10-08 2006-04-13 Satya Mallya Method of and system for group communication
JP4578999B2 (en) * 2005-02-10 2010-11-10 昭和電工株式会社 Method for producing hydroxylamine
JP4578998B2 (en) * 2005-02-10 2010-11-10 昭和電工株式会社 Method for producing hydroxylamine
CN112723328B (en) * 2020-12-17 2022-03-11 浙江锦华新材料股份有限公司 Preparation method of high-purity solid hydroxylamine hydrochloride

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5534764B2 (en) * 1972-06-02 1980-09-09
US4147623A (en) * 1977-10-28 1979-04-03 Allied Chemical Corporation Hydroxylamine purification via ion exclusion
US4202765A (en) * 1977-10-28 1980-05-13 Allied Chemical Corporation Hydroxylamine purification via cation exchange
US4166842A (en) * 1977-10-28 1979-09-04 Allied Chemical Corporation Hydroxylamine purification via liquid/liquid extraction
DE3607998A1 (en) * 1986-03-11 1987-09-17 Basf Ag METHOD FOR PROCESSING HYDROXYLAMINE OR WATER CONTAINING ITS SALTS
US5318762A (en) * 1992-12-09 1994-06-07 Olin Corporation Process for treating aqueous solutions of hydroxylamine salts containing excess acid
HRP960601B1 (en) * 1995-12-20 2001-12-31 Basf Ag Process for separating medium boiling substances from a mixture of low, medium and high boiling substances

Also Published As

Publication number Publication date
KR20010021915A (en) 2001-03-15
ID22371A (en) 1999-10-07
EP1017621B1 (en) 2003-07-30
MY118717A (en) 2005-01-31
ES2203954T3 (en) 2004-04-16
DE69816842D1 (en) 2003-09-04
EP1017621A1 (en) 2000-07-12
US5788946A (en) 1998-08-04
KR100485849B1 (en) 2005-04-28
JP3567206B2 (en) 2004-09-22
DE69816842T2 (en) 2004-04-22
AU7500898A (en) 1999-02-10
CN1269766A (en) 2000-10-11
NO20000203L (en) 2000-03-02
NO20000203D0 (en) 2000-01-14
TW424081B (en) 2001-03-01
JP2001510133A (en) 2001-07-31
WO1999003780A1 (en) 1999-01-28
CN1130307C (en) 2003-12-10
EP1017621A4 (en) 2000-10-18
ATE246145T1 (en) 2003-08-15
CA2296699C (en) 2003-08-05
DK1017621T3 (en) 2003-10-27

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