CA2259535C - Procede de production de composition detergente - Google Patents
Procede de production de composition detergente Download PDFInfo
- Publication number
- CA2259535C CA2259535C CA002259535A CA2259535A CA2259535C CA 2259535 C CA2259535 C CA 2259535C CA 002259535 A CA002259535 A CA 002259535A CA 2259535 A CA2259535 A CA 2259535A CA 2259535 C CA2259535 C CA 2259535C
- Authority
- CA
- Canada
- Prior art keywords
- surfactant
- particle size
- premix
- nonionic surfactant
- micrometers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000000034 method Methods 0.000 title claims abstract description 24
- 230000008569 process Effects 0.000 title claims abstract description 23
- 239000000203 mixture Substances 0.000 title claims description 17
- 239000003599 detergent Substances 0.000 title claims description 14
- 239000002245 particle Substances 0.000 claims abstract description 73
- 239000002736 nonionic surfactant Substances 0.000 claims abstract description 36
- 239000000654 additive Substances 0.000 claims abstract description 24
- 239000004094 surface-active agent Substances 0.000 claims abstract description 18
- 239000003945 anionic surfactant Substances 0.000 claims abstract description 17
- 238000002156 mixing Methods 0.000 claims abstract description 15
- 238000005507 spraying Methods 0.000 claims abstract description 6
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 34
- 239000011236 particulate material Substances 0.000 claims description 13
- 229910000323 aluminium silicate Inorganic materials 0.000 claims description 11
- 238000009826 distribution Methods 0.000 claims description 5
- MWNQXXOSWHCCOZ-UHFFFAOYSA-L sodium;oxido carbonate Chemical compound [Na+].[O-]OC([O-])=O MWNQXXOSWHCCOZ-UHFFFAOYSA-L 0.000 claims description 4
- 239000007844 bleaching agent Substances 0.000 claims description 2
- 239000010457 zeolite Substances 0.000 description 28
- 229910021536 Zeolite Inorganic materials 0.000 description 25
- -1 fatty acid esters Chemical class 0.000 description 21
- 239000000047 product Substances 0.000 description 15
- 235000014113 dietary fatty acids Nutrition 0.000 description 13
- 239000000194 fatty acid Substances 0.000 description 13
- 229930195729 fatty acid Natural products 0.000 description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 11
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical group [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 9
- 150000004665 fatty acids Chemical class 0.000 description 9
- 238000005342 ion exchange Methods 0.000 description 9
- 239000000463 material Substances 0.000 description 9
- 239000007921 spray Substances 0.000 description 8
- 125000000217 alkyl group Chemical group 0.000 description 7
- 229910021653 sulphate ion Inorganic materials 0.000 description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerol Natural products OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 6
- 150000004996 alkyl benzenes Chemical class 0.000 description 6
- 239000000843 powder Substances 0.000 description 6
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 5
- 230000000996 additive effect Effects 0.000 description 5
- 239000007859 condensation product Substances 0.000 description 5
- 239000012530 fluid Substances 0.000 description 5
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 4
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 4
- 150000001298 alcohols Chemical class 0.000 description 4
- 150000001412 amines Chemical class 0.000 description 4
- 229910001424 calcium ion Inorganic materials 0.000 description 4
- 125000004432 carbon atom Chemical group C* 0.000 description 4
- 238000004090 dissolution Methods 0.000 description 4
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 4
- 239000003760 tallow Substances 0.000 description 4
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 3
- 238000005054 agglomeration Methods 0.000 description 3
- 230000002776 aggregation Effects 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- 230000009435 amidation Effects 0.000 description 2
- 238000007112 amidation reaction Methods 0.000 description 2
- 239000002518 antifoaming agent Substances 0.000 description 2
- 239000013522 chelant Substances 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 239000000499 gel Substances 0.000 description 2
- 230000002209 hydrophobic effect Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 229920000058 polyacrylate Polymers 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 description 2
- 235000011152 sodium sulphate Nutrition 0.000 description 2
- YGUMVDWOQQJBGA-VAWYXSNFSA-N 5-[(4-anilino-6-morpholin-4-yl-1,3,5-triazin-2-yl)amino]-2-[(e)-2-[4-[(4-anilino-6-morpholin-4-yl-1,3,5-triazin-2-yl)amino]-2-sulfophenyl]ethenyl]benzenesulfonic acid Chemical group C=1C=C(\C=C\C=2C(=CC(NC=3N=C(N=C(NC=4C=CC=CC=4)N=3)N3CCOCC3)=CC=2)S(O)(=O)=O)C(S(=O)(=O)O)=CC=1NC(N=C(N=1)N2CCOCC2)=NC=1NC1=CC=CC=C1 YGUMVDWOQQJBGA-VAWYXSNFSA-N 0.000 description 1
- KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- IMROMDMJAWUWLK-UHFFFAOYSA-N Ethenol Chemical group OC=C IMROMDMJAWUWLK-UHFFFAOYSA-N 0.000 description 1
- MBBZMMPHUWSWHV-BDVNFPICSA-N N-methylglucamine Chemical compound CNC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO MBBZMMPHUWSWHV-BDVNFPICSA-N 0.000 description 1
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 1
- 239000004115 Sodium Silicate Substances 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- ZUBJEHHGZYTRPH-KTKRTIGZSA-N [(z)-octadec-9-enyl] hydrogen sulfate Chemical compound CCCCCCCC\C=C/CCCCCCCCOS(O)(=O)=O ZUBJEHHGZYTRPH-KTKRTIGZSA-N 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 150000008051 alkyl sulfates Chemical class 0.000 description 1
- 125000002947 alkylene group Chemical group 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 239000003093 cationic surfactant Substances 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 229910052681 coesite Inorganic materials 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 229910052906 cristobalite Inorganic materials 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 238000000280 densification Methods 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- UZABCLFSICXBCM-UHFFFAOYSA-N ethoxy hydrogen sulfate Chemical class CCOOS(O)(=O)=O UZABCLFSICXBCM-UHFFFAOYSA-N 0.000 description 1
- 235000019387 fatty acid methyl ester Nutrition 0.000 description 1
- 150000002193 fatty amides Chemical class 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 150000002314 glycerols Chemical class 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 125000001165 hydrophobic group Chemical group 0.000 description 1
- 150000004702 methyl esters Chemical class 0.000 description 1
- CQDGTJPVBWZJAZ-UHFFFAOYSA-N monoethyl carbonate Chemical class CCOC(O)=O CQDGTJPVBWZJAZ-UHFFFAOYSA-N 0.000 description 1
- 235000014366 other mixer Nutrition 0.000 description 1
- 239000005022 packaging material Substances 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 229920000151 polyglycol Polymers 0.000 description 1
- 239000010695 polyglycol Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229940071089 sarcosinate Drugs 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 239000001509 sodium citrate Substances 0.000 description 1
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 description 1
- 229910052911 sodium silicate Inorganic materials 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 229910052682 stishovite Inorganic materials 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 229910052905 tridymite Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
- C11D11/0088—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads the liquefied ingredients being sprayed or adsorbed onto solid particles
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
La présente invention concerne un procédé comprenant les étapes suivantes: (i) mélange d'au moins deux additifs non tensioactifs pour former un prémélange; (ii) pulvérisation de la totalité du tensioactif non ionique sur le prémélange afin de former une première particule intermédiaire; (iii) mélange de la première particule intermédiaire avec une seconde particule intermédiaire, cette dernière comprenant pratiquement la totalité des tensioactifs anioniques et étant exempte du tensioactif non ionique.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP96201854.5 | 1996-07-04 | ||
| EP96201854A EP0816485B1 (fr) | 1996-07-04 | 1996-07-04 | Procédé de préparation de compositions détergentes |
| PCT/US1997/011281 WO1998001520A2 (fr) | 1996-07-04 | 1997-06-27 | Procede de production de composition detergente |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2259535A1 CA2259535A1 (fr) | 1998-01-15 |
| CA2259535C true CA2259535C (fr) | 2002-10-01 |
Family
ID=8224140
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA002259535A Expired - Fee Related CA2259535C (fr) | 1996-07-04 | 1997-06-27 | Procede de production de composition detergente |
Country Status (10)
| Country | Link |
|---|---|
| EP (1) | EP0816485B1 (fr) |
| JP (1) | JPH11514033A (fr) |
| CN (1) | CN1195834C (fr) |
| AR (1) | AR008062A1 (fr) |
| AT (1) | ATE312901T1 (fr) |
| BR (1) | BR9710199A (fr) |
| CA (1) | CA2259535C (fr) |
| DE (1) | DE69635575T2 (fr) |
| ES (1) | ES2253747T3 (fr) |
| WO (1) | WO1998001520A2 (fr) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6156718A (en) * | 1996-07-04 | 2000-12-05 | The Procter & Gamble Company | Process for making detergent compositions |
| EP1115836A1 (fr) * | 1998-09-25 | 2001-07-18 | The Procter & Gamble Company | Composition de detergent granulaire presentant une solubilite et un aspect ameliores |
| US6964945B1 (en) | 1998-09-25 | 2005-11-15 | The Procter & Gamble Company | Solid detergent compositions |
| WO2000018874A1 (fr) * | 1998-09-25 | 2000-04-06 | The Procter & Gamble Company | Composition detergente granulaire a aspect et a solubilite ameliores |
| US6906022B1 (en) * | 1998-09-25 | 2005-06-14 | The Procter & Gamble Company | Granular detergent compositions having homogenous particles and process for producing same |
| BR9914047A (pt) * | 1998-09-25 | 2001-06-19 | Procter & Gamble | Composições detergentes granulares tendo perfis de solubilidade aperfeiçoados |
| US6673766B1 (en) * | 1998-09-25 | 2004-01-06 | The Procter & Gamble Company | Solid detergent compositions containing mixtures of surfactant/builder particles |
| JP2002528600A (ja) | 1998-10-26 | 2002-09-03 | ザ、プロクター、エンド、ギャンブル、カンパニー | 外観と溶解性の改良された粒状洗剤組成物の製造方法 |
| US6602846B1 (en) | 1999-06-14 | 2003-08-05 | Kao Corporation | Method for producing single nucleus detergent particles |
| EP1187904B1 (fr) * | 1999-06-21 | 2004-08-11 | The Procter & Gamble Company | Procede de fabrication d'une composition granulaire detergente |
| US6951837B1 (en) | 1999-06-21 | 2005-10-04 | The Procter & Gamble Company | Process for making a granular detergent composition |
| US6833346B1 (en) * | 1999-06-21 | 2004-12-21 | The Procter & Gamble Company | Process for making detergent particulates |
| GB0111863D0 (en) * | 2001-05-15 | 2001-07-04 | Unilever Plc | Granular composition |
| DE102006029007A1 (de) * | 2006-06-24 | 2008-01-03 | Cognis Ip Management Gmbh | Feste Tenside in granularer Form |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4136051A (en) * | 1974-02-25 | 1979-01-23 | Henkel Kommanditgesellschaft Auf Aktien (Henkel Kgaa) | Pourable washing compositions containing a luminosilicates and non-ionics and method for their preparation |
| JPS6189300A (ja) * | 1984-10-09 | 1986-05-07 | ライオン株式会社 | 非イオン界面活性剤を含む粒状洗剤組成物の製造方法 |
| TW240243B (fr) * | 1992-03-12 | 1995-02-11 | Kao Corp | |
| DE4209435A1 (de) * | 1992-03-24 | 1993-09-30 | Henkel Kgaa | Granulares, nichtionische Tenside enthaltendes, phosphatfreies Additiv für Wasch- und Reinigungsmittel |
| TR27586A (tr) * | 1992-09-01 | 1995-06-13 | Procter & Gamble | Yüksek yogunlukla zerre deterjanin yapilmasi icin islem ve islem ile yapilan bilesimler. |
-
1996
- 1996-07-04 AT AT96201854T patent/ATE312901T1/de not_active IP Right Cessation
- 1996-07-04 EP EP96201854A patent/EP0816485B1/fr not_active Expired - Lifetime
- 1996-07-04 DE DE69635575T patent/DE69635575T2/de not_active Expired - Fee Related
- 1996-07-04 ES ES96201854T patent/ES2253747T3/es not_active Expired - Lifetime
-
1997
- 1997-06-27 JP JP10505241A patent/JPH11514033A/ja active Pending
- 1997-06-27 BR BR9710199-0A patent/BR9710199A/pt not_active IP Right Cessation
- 1997-06-27 CN CNB971973946A patent/CN1195834C/zh not_active Expired - Fee Related
- 1997-06-27 CA CA002259535A patent/CA2259535C/fr not_active Expired - Fee Related
- 1997-06-27 WO PCT/US1997/011281 patent/WO1998001520A2/fr active Application Filing
- 1997-07-03 AR ARP970102992A patent/AR008062A1/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DE69635575D1 (de) | 2006-01-19 |
| DE69635575T2 (de) | 2006-09-14 |
| JPH11514033A (ja) | 1999-11-30 |
| CA2259535A1 (fr) | 1998-01-15 |
| EP0816485A1 (fr) | 1998-01-07 |
| BR9710199A (pt) | 1999-11-23 |
| CN1332790A (zh) | 2002-01-23 |
| CN1195834C (zh) | 2005-04-06 |
| AR008062A1 (es) | 1999-12-09 |
| EP0816485B1 (fr) | 2005-12-14 |
| ES2253747T3 (es) | 2006-06-01 |
| WO1998001520A2 (fr) | 1998-01-15 |
| ATE312901T1 (de) | 2005-12-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request | ||
| MKLA | Lapsed |