CA2092194A1 - Liquid detergent compositions - Google Patents

Liquid detergent compositions

Info

Publication number
CA2092194A1
CA2092194A1 CA2092194A CA2092194A CA2092194A1 CA 2092194 A1 CA2092194 A1 CA 2092194A1 CA 2092194 A CA2092194 A CA 2092194A CA 2092194 A CA2092194 A CA 2092194A CA 2092194 A1 CA2092194 A1 CA 2092194A1
Authority
CA
Canada
Prior art keywords
mixture
weight
factant
sur
maltose
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CA2092194A
Other languages
French (fr)
Other versions
CA2092194C (en
Inventor
Julie Anne Dyet
Peter Robert Foley
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Procter and Gamble Co
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=10682966&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=CA2092194(A1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Individual filed Critical Individual
Publication of CA2092194A1 publication Critical patent/CA2092194A1/en
Application granted granted Critical
Publication of CA2092194C publication Critical patent/CA2092194C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0008—Detergent materials or soaps characterised by their shape or physical properties aqueous liquid non soap compositions
    • C11D17/003—Colloidal solutions, e.g. gels; Thixotropic solutions or pastes
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38—Cationic compounds
    • C11D1/52—Carboxylic amides, alkylolamides or imides or their condensation products with alkylene oxides
    • C11D1/525—Carboxylic amides (R1-CO-NR2R3), where R1, R2 or R3 contain two or more hydroxy groups per alkyl group, e.g. R3 being a reducing sugar rest
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38—Cationic compounds
    • C11D1/65—Mixtures of anionic with cationic compounds
    • C11D1/652—Mixtures of anionic compounds with carboxylic amides or alkylol amides
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/662—Carbohydrates or derivatives
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/32—Amides; Substituted amides
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/18—Sulfonic acids or sulfuric acid esters; Salts thereof derived from amino alcohols
    • C11D1/20—Fatty acid condensates
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/29—Sulfates of polyoxyalkylene ethers
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38—Cationic compounds
    • C11D1/52—Carboxylic amides, alkylolamides or imides or their condensation products with alkylene oxides
    • C11D1/523—Carboxylic alkylolamides, or dialkylolamides, or hydroxycarboxylic amides (R1-CO-NR2R3), where R1, R2 or R3 contain one hydroxy group per alkyl group
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/72—Ethers of polyoxyalkylene glycols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/75—Amino oxides
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88—Ampholytes; Electroneutral compounds
    • C11D1/90—Betaines
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88—Ampholytes; Electroneutral compounds
    • C11D1/92—Sulfobetaines ; Sulfitobetaines

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Detergent Compositions (AREA)

Abstract

Aqueous unbuilt liquid or gel-form detergent compositions are provided comprising, from 15 % to 65 % by weight of a core surfactant mixture, comprising from 5 % to 95 % by weight of the mixture of a water soluble anionic sulphate or sulphonate sur-factant salt together and from 5 % to 95 % by weight of the mixture of one or more compounds of formula (I), wherein Z is a poly-hydroxy hydrocarbyl moiety having a linear hydrocarbyl chain with at least three hydroxy groups connected directly to the chain, said moiety being derived from glucose and mixtures thereof with maltose, the maltose comprising not more than 33 % of the mixture, R is a C6-C16 hydrocarbyl radical and R1 is a C1-C4 alkyl or C2-C4 hydroxyalkyl group, a 0.12 % s? tion of the sur-factant mixtures of the compositions having an interfacial tension (IFT) of less than 0.2 Pa.cm at 48 °C and a polypropy-lene cup (PPC) greasy soil removal value of at least 1.4 x that of the anionic surfactant component(s) alone. Preferred op-tional ingredients include amide, betaine and ethoxylated C9-C11 fatty alcohol suds modifiers.
CA002092194A 1990-09-28 1991-09-25 Liquid detergent compositions Expired - Fee Related CA2092194C (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB9021217.6 1990-09-28
GB909021217A GB9021217D0 (en) 1990-09-28 1990-09-28 Liquid detergent compositions

Publications (2)

Publication Number Publication Date
CA2092194A1 true CA2092194A1 (en) 1992-03-29
CA2092194C CA2092194C (en) 1996-11-19

Family

ID=10682966

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002092194A Expired - Fee Related CA2092194C (en) 1990-09-28 1991-09-25 Liquid detergent compositions

Country Status (31)

Country Link
EP (1) EP0550636B1 (en)
JP (1) JP3007150B2 (en)
KR (1) KR100221444B1 (en)
CN (1) CN1042236C (en)
AR (1) AR244328A1 (en)
AT (1) ATE127834T1 (en)
AU (1) AU664023B2 (en)
BR (1) BR9106935A (en)
CA (1) CA2092194C (en)
CO (1) CO4180440A1 (en)
CZ (1) CZ281716B6 (en)
DE (1) DE69113055T2 (en)
DK (1) DK0550636T3 (en)
EG (1) EG19516A (en)
ES (1) ES2077247T3 (en)
FI (1) FI931369A (en)
GB (1) GB9021217D0 (en)
GR (1) GR3017416T3 (en)
HU (1) HU213448B (en)
IE (1) IE76141B1 (en)
IN (1) IN185274B (en)
MA (1) MA22303A1 (en)
MX (1) MX9101373A (en)
MY (1) MY108070A (en)
NO (1) NO931078L (en)
NZ (1) NZ240022A (en)
PT (1) PT99087B (en)
SK (1) SK25393A3 (en)
TR (1) TR26013A (en)
TW (1) TW265361B (en)
WO (1) WO1992006171A1 (en)

Families Citing this family (47)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0602179B1 (en) * 1991-09-06 1999-06-30 The Procter & Gamble Company Detergent compositions containing calcium and polyhydroxy fatty acid amide
EP0572723A1 (en) * 1992-06-02 1993-12-08 The Procter & Gamble Company Structured liquid detergent compositions
EP0656046A4 (en) * 1992-08-21 1995-09-20 Procter & Gamble Concentrated liquid detergent composition comprising an alkyl ether sulphate and a process for making the composition.
EP0658188A4 (en) * 1992-09-01 1995-08-09 Procter & Gamble Liquid or gel detergent compositions containing calcium and stabilizing agent thereof.
US5545354A (en) * 1992-09-01 1996-08-13 The Procter & Gamble Company Liquid or gel dishwashing detergent containing a polyhydroxy fatty acid amide, calcium ions and an alkylpolyethoxypolycarboxylate
CA2143328A1 (en) * 1992-09-01 1994-03-17 Kofi Ofosu-Asante Liquid or gel dishwashing detergent containing alkyl ethoxy carboxylate, divalent ions and alkylpolyethoxypolycarboxylate
US5269974A (en) * 1992-09-01 1993-12-14 The Procter & Gamble Company Liquid or gel dishwashing detergent composition containing alkyl amphocarboxylic acid and magnesium or calcium ions
US5580849A (en) * 1992-09-01 1996-12-03 The Procter & Gamble Company Liquid or gel detergent compositions containing calcium and stabilizing agent thereof
WO1994010273A1 (en) * 1992-11-04 1994-05-11 The Procter & Gamble Company Detergent gels
JPH08503986A (en) * 1992-11-30 1996-04-30 ザ、プロクター、エンド、ギャンブル、カンパニー Low foaming mixed polyhydroxy fatty acid amide cleaning with nonionic / anionic surfactant
WO1994014947A1 (en) * 1992-12-28 1994-07-07 The Procter & Gamble Company Clear detergent gels
PE4995A1 (en) * 1993-06-30 1995-03-01 Procter & Gamble DETERGENT GEL CONTAINING ETHOXYLATED ALKYL SULPHATES AND SECONDARY SULPHONATES
DE4323253C1 (en) * 1993-07-12 1995-01-05 Henkel Kgaa Use of fatty acid N-alkyl polyhydroxyalkylamides as rinse aid for machine cleaning hard surfaces
US5417893A (en) * 1993-08-27 1995-05-23 The Procter & Gamble Company Concentrated liquid or gel light duty dishwashing detergent compositions containing calcium ions and disulfonate surfactants
US5415801A (en) * 1993-08-27 1995-05-16 The Procter & Gamble Company Concentrated light duty liquid or gel dishwashing detergent compositions containing sugar
US5474710A (en) * 1993-08-27 1995-12-12 Ofosu-Asanta; Kofi Process for preparing concentrated surfactant mixtures containing magnesium
US5415814A (en) * 1993-08-27 1995-05-16 The Procter & Gamble Company Concentrated liquid or gel light duty dishwashing detergent composition containing calcium xylene sulfonate
US5500150A (en) * 1993-09-09 1996-03-19 The Procter & Gamble Company Solidified detergent additive with n-alkoxy polyhydroxy fatty acid amide and alkoxylated surfactant
US5489393A (en) * 1993-09-09 1996-02-06 The Procter & Gamble Company High sudsing detergent with n-alkoxy polyhydroxy fatty acid amide and secondary carboxylate surfactants
EP0717766B1 (en) * 1993-09-09 1998-04-01 The Procter & Gamble Company Automatic dishwashing detergent with alkoxy or aryloxy amide surfactant
WO1995007971A1 (en) * 1993-09-14 1995-03-23 The Procter & Gamble Company Light duty liquid or gel dishwashing detergent compositions containing protease
DE4331297A1 (en) * 1993-09-15 1995-03-16 Henkel Kgaa Bar soaps
EP0659870A1 (en) * 1993-11-26 1995-06-28 The Procter & Gamble Company N-alkyl polyhydroxy fatty acid amide compositions and their method of synthesis
US5750748A (en) * 1993-11-26 1998-05-12 The Procter & Gamble Company N-alkyl polyhydroxy fatty acid amide compositions and their method of synthesis
DE4400632C1 (en) * 1994-01-12 1995-03-23 Henkel Kgaa Surfactant mixtures and compositions containing these
ES2132631T5 (en) * 1994-01-25 2011-02-17 THE PROCTER & GAMBLE COMPANY COMPOSITIONS OF LIQUID OR GELIFIED DETERGENTS FOR WASHING LOW SEVERE AND HIGH SOAPPED ACTION TABLETS CONTAINING OXIDES FROM LONG CHAIN AMINES.
US5534197A (en) * 1994-01-25 1996-07-09 The Procter & Gamble Company Gemini polyhydroxy fatty acid amides
WO1995019951A1 (en) * 1994-01-25 1995-07-27 The Procter & Gamble Company Polyhydroxy diamines and their use in detergent compositions
US5512699A (en) * 1994-01-25 1996-04-30 The Procter & Gamble Company Poly polyhydroxy fatty acid amides
DE4409321A1 (en) * 1994-03-18 1995-09-21 Henkel Kgaa Low m.pt fatty acid isethionate-based detergent mixt.
MX9605418A (en) * 1994-05-06 1997-12-31 Procter & Gamble Liquid detergent containing polyhydroxy fatty acid amide and toluene sulfonate salt.
US5500153A (en) * 1994-07-05 1996-03-19 The Procter & Gamble Company Handwash laundry detergent composition having improved mildness and cleaning performance
USH1632H (en) * 1994-08-15 1997-02-04 Shell Oil Company Liquid laundry detergent formulations
US5686603A (en) * 1995-05-04 1997-11-11 Lever Brothers Company, Division Of Conopco, Inc. Sulfated polyhydroxy compounds as anionic surfactants and a process for their manufacture
DE19533539A1 (en) 1995-09-11 1997-03-13 Henkel Kgaa O / W emulsifiers
DE19544710C2 (en) 1995-11-30 1998-11-26 Henkel Kgaa Thickener
US5932535A (en) * 1995-12-21 1999-08-03 Henkel Kommanditgesellschaft Auf Aktien Process for the production of light-colored, low-viscosity surfactant concentrates
DE19548068C1 (en) 1995-12-21 1997-06-19 Henkel Kgaa Process for the production of light colored, low viscosity surfactant concentrates
AU2602597A (en) * 1996-04-08 1997-10-29 Colgate-Palmolive Company, The Light duty liquid cleaning compositions
DE19749560C2 (en) * 1997-11-10 2002-01-10 Henkel Kgaa Skin-friendly hand dishwashing liquid
DE10018812A1 (en) 2000-04-15 2001-10-25 Cognis Deutschland Gmbh Nonionic surfactant granulate, used in surfactant, cosmetic or pharmaceutical formulation or laundry or other detergent, is obtained by granulating and simultaneously drying aqueous surfactant paste in presence of organic polymeric carrier
EP1167500A1 (en) * 2000-06-29 2002-01-02 The Procter & Gamble Company Process of cleaning a hard surface
DE102005025933B3 (en) 2005-06-06 2006-07-13 Centrotherm Photovoltaics Gmbh + Co. Kg Doping mixture for preparing and doping semiconductor surfaces, comprises a p- or n-dopant, for doping the semiconductor surfaces, water and mixture of two or more surfactants, where one of the surfactant is a non-ionic surfactant
AR072859A1 (en) 2008-05-23 2010-09-29 Colgate Palmolive Co CLEANING LIQUID METHODS AND COMPOSITIONS
CN102775831B (en) * 2012-07-31 2014-11-12 华南理工大学 Method for curing and grafting amphoteric ion gel coat on external surface on material surface by ultraviolet
US20230066622A1 (en) * 2016-10-20 2023-03-02 Eve Miller Electrified Garbage Container Cover
US11879111B2 (en) 2020-03-27 2024-01-23 Ecolab Usa Inc. Detergent compositions, cleaning systems and methods of cleaning cosmetic and other soils

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BE557103A (en) * 1956-05-14
GB2058823B (en) * 1979-09-17 1983-06-22 Unilever Ltd Dishwashing compositions
CA1151501A (en) * 1981-03-24 1983-08-09 Gilles M. Tastayre Cleaning gel, and process for its manufacture and use
GB8405266D0 (en) * 1984-02-29 1984-04-04 Unilever Plc Detergent compositions
ES8708009A1 (en) * 1984-11-07 1987-09-01 Procter & Gamble Liquid detergent compositions.
DE3711776A1 (en) * 1987-04-08 1988-10-27 Huels Chemische Werke Ag USE OF N-POLYHYDROXYALKYL Fatty Acid Amides As Thickeners For Liquid Aqueous Surfactant Systems

Also Published As

Publication number Publication date
AU8735291A (en) 1992-04-28
SK25393A3 (en) 1993-07-07
EG19516A (en) 1995-08-30
CZ281716B6 (en) 1996-12-11
DE69113055T2 (en) 1996-04-04
AU664023B2 (en) 1995-11-02
IN185274B (en) 2000-12-16
EP0550636A1 (en) 1993-07-14
IE76141B1 (en) 1997-10-08
EP0550636B1 (en) 1995-09-13
MA22303A1 (en) 1992-04-01
HUT64390A (en) 1993-12-28
WO1992006171A1 (en) 1992-04-16
BR9106935A (en) 1993-08-17
AR244328A1 (en) 1993-10-29
GB9021217D0 (en) 1990-11-14
NZ240022A (en) 1995-03-28
PT99087B (en) 2001-05-31
TR26013A (en) 1993-11-01
HU213448B (en) 1997-06-30
CA2092194C (en) 1996-11-19
FI931369A (en) 1993-04-26
CN1042236C (en) 1999-02-24
CN1062160A (en) 1992-06-24
JPH06501729A (en) 1994-02-24
DE69113055D1 (en) 1995-10-19
CO4180440A1 (en) 1995-06-07
CZ53393A3 (en) 1994-10-19
ATE127834T1 (en) 1995-09-15
NO931078L (en) 1993-05-27
TW265361B (en) 1995-12-11
ES2077247T3 (en) 1995-11-16
PT99087A (en) 1992-08-31
MY108070A (en) 1996-08-15
MX9101373A (en) 1992-05-04
NO931078D0 (en) 1993-03-24
DK0550636T3 (en) 1996-02-05
HU9300888D0 (en) 1993-07-28
KR100221444B1 (en) 1999-09-15
IE913404A1 (en) 1992-04-08
GR3017416T3 (en) 1995-12-31
FI931369A0 (en) 1993-03-26
JP3007150B2 (en) 2000-02-07

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