CA2028831A1 - Process for the fabrication of acryloyl chloride - Google Patents

Process for the fabrication of acryloyl chloride

Info

Publication number
CA2028831A1
CA2028831A1 CA2028831A CA2028831A CA2028831A1 CA 2028831 A1 CA2028831 A1 CA 2028831A1 CA 2028831 A CA2028831 A CA 2028831A CA 2028831 A CA2028831 A CA 2028831A CA 2028831 A1 CA2028831 A1 CA 2028831A1
Authority
CA
Canada
Prior art keywords
acryloyl chloride
catalyst
acrylic acid
fabrication
phenylchloroform
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CA2028831A
Other languages
French (fr)
Other versions
CA2028831C (en
Inventor
Paul Grosius
Jean-Francois Croizy
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Arkema France SA
Original Assignee
Norsolor SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Norsolor SA filed Critical Norsolor SA
Publication of CA2028831A1 publication Critical patent/CA2028831A1/en
Application granted granted Critical
Publication of CA2028831C publication Critical patent/CA2028831C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/58—Preparation of carboxylic acid halides
    • C07C51/60—Preparation of carboxylic acid halides by conversion of carboxylic acids or their anhydrides or esters, lactones, salts into halides with the same carboxylic acid part

Abstract

Acryloyl chloride is obtained by the reaction of acrylic acid on phenylchloroform, in the presence of at least one Lewis acid as catalyst and at least one polymerisation inhibiting agent. According to the invention, the catalyst is chosen among zinc oxide and zirconium tetrchloride and the reaction is brought to a temperature of at least 105 DEG C. In a preferred embodiment, the acrylic acid is added to the medium consisting of phenylchloroform, the catalyst and the polymerization inhibitor, and brought to a temperature of at least 105 DEG C, whereby the acryloyl chloride formed distils as soon as the acrylic acid is introduced. Acryloyl chloride is a highly reactive synthesis intermediate.
CA002028831A 1989-03-06 1990-01-18 Process for the fabrication of acryloyl chloride Expired - Fee Related CA2028831C (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR8902918A FR2643901B1 (en) 1989-03-06 1989-03-06 PROCESS FOR THE MANUFACTURE OF ACRYLOYL CHLORIDE
FR89/02918 1989-03-06

Publications (2)

Publication Number Publication Date
CA2028831A1 true CA2028831A1 (en) 1990-09-07
CA2028831C CA2028831C (en) 1997-05-20

Family

ID=9379411

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002028831A Expired - Fee Related CA2028831C (en) 1989-03-06 1990-01-18 Process for the fabrication of acryloyl chloride

Country Status (10)

Country Link
EP (1) EP0387116B1 (en)
JP (1) JPH04502765A (en)
AT (1) ATE98212T1 (en)
CA (1) CA2028831C (en)
DD (1) DD295625A5 (en)
DE (1) DE69005000T2 (en)
DK (1) DK0387116T3 (en)
ES (1) ES2060973T3 (en)
FR (1) FR2643901B1 (en)
WO (1) WO1990010616A1 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20100044186A (en) * 2007-06-28 2010-04-29 쓰리엠 이노베이티브 프로퍼티즈 컴파니 Process for forming alpha, beta-unsaturated carbonyl halides
CN109553526B (en) * 2018-12-18 2022-07-05 杭州盛弗泰新材料科技有限公司 Continuous production method of acryloyl chloride

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1921767A (en) * 1929-05-20 1933-08-08 Dow Chemical Co Method of making acid halides
US1963749A (en) * 1932-07-30 1934-06-19 Monsanto Chemicals Manufacture of aromatic dicarboxylic acid chlorides
DE3422576A1 (en) * 1984-06-18 1985-12-19 Hoechst Ag, 6230 Frankfurt METHOD FOR PRODUCING HALOGENATED ALIPHATIC CARBONIC ACID FLUORIDES

Also Published As

Publication number Publication date
ES2060973T3 (en) 1994-12-01
FR2643901B1 (en) 1991-09-06
DE69005000D1 (en) 1994-01-20
EP0387116A1 (en) 1990-09-12
WO1990010616A1 (en) 1990-09-20
DE69005000T2 (en) 1994-04-28
ATE98212T1 (en) 1993-12-15
FR2643901A1 (en) 1990-09-07
CA2028831C (en) 1997-05-20
DK0387116T3 (en) 1994-02-14
JPH04502765A (en) 1992-05-21
EP0387116B1 (en) 1993-12-08
DD295625A5 (en) 1991-11-07

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