CA1314441C - Procede de realisation d'un tube de verre transparent a dopage interne, notamment pour la fabrication de fibres optiques dopees par une terre rare - Google Patents
Procede de realisation d'un tube de verre transparent a dopage interne, notamment pour la fabrication de fibres optiques dopees par une terre rareInfo
- Publication number
- CA1314441C CA1314441C CA000580205A CA580205A CA1314441C CA 1314441 C CA1314441 C CA 1314441C CA 000580205 A CA000580205 A CA 000580205A CA 580205 A CA580205 A CA 580205A CA 1314441 C CA1314441 C CA 1314441C
- Authority
- CA
- Canada
- Prior art keywords
- tube
- glass
- layer
- doping
- starting
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000011521 glass Substances 0.000 title claims abstract description 44
- 238000000034 method Methods 0.000 title claims description 38
- 239000000835 fiber Substances 0.000 title description 9
- 230000008021 deposition Effects 0.000 claims abstract description 26
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 18
- 238000004519 manufacturing process Methods 0.000 claims abstract description 18
- 239000003595 mist Substances 0.000 claims abstract description 9
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 9
- 239000013307 optical fiber Substances 0.000 claims abstract description 8
- 229910052761 rare earth metal Inorganic materials 0.000 claims abstract description 3
- 150000002910 rare earth metals Chemical class 0.000 claims abstract description 3
- 239000010410 layer Substances 0.000 claims description 57
- 238000000151 deposition Methods 0.000 claims description 48
- 239000007788 liquid Substances 0.000 claims description 23
- 238000009792 diffusion process Methods 0.000 claims description 20
- 238000010438 heat treatment Methods 0.000 claims description 20
- 238000001035 drying Methods 0.000 claims description 15
- 239000000203 mixture Substances 0.000 claims description 12
- 239000007789 gas Substances 0.000 claims description 11
- 238000011144 upstream manufacturing Methods 0.000 claims description 9
- 239000004071 soot Substances 0.000 claims description 7
- 239000006121 base glass Substances 0.000 claims description 6
- 239000012159 carrier gas Substances 0.000 claims description 4
- 238000009434 installation Methods 0.000 claims description 4
- 238000002663 nebulization Methods 0.000 claims description 4
- 239000002131 composite material Substances 0.000 claims description 2
- 239000002245 particle Substances 0.000 claims description 2
- 238000004017 vitrification Methods 0.000 claims description 2
- 238000012550 audit Methods 0.000 claims 1
- 239000011247 coating layer Substances 0.000 claims 1
- 239000006193 liquid solution Substances 0.000 abstract 1
- 239000002243 precursor Substances 0.000 description 10
- 239000002019 doping agent Substances 0.000 description 7
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 239000003153 chemical reaction reagent Substances 0.000 description 3
- 238000010348 incorporation Methods 0.000 description 3
- 230000003287 optical effect Effects 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- 238000011084 recovery Methods 0.000 description 3
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- 229910052691 Erbium Inorganic materials 0.000 description 2
- 230000005587 bubbling Effects 0.000 description 2
- 239000000969 carrier Substances 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 238000006073 displacement reaction Methods 0.000 description 2
- 238000010981 drying operation Methods 0.000 description 2
- UYAHIZSMUZPPFV-UHFFFAOYSA-N erbium Chemical compound [Er] UYAHIZSMUZPPFV-UHFFFAOYSA-N 0.000 description 2
- UOACKFBJUYNSLK-XRKIENNPSA-N Estradiol Cypionate Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H](C4=CC=C(O)C=C4CC3)CC[C@@]21C)C(=O)CCC1CCCC1 UOACKFBJUYNSLK-XRKIENNPSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 229910052779 Neodymium Inorganic materials 0.000 description 1
- 244000274883 Urtica dioica Species 0.000 description 1
- 235000009108 Urtica dioica Nutrition 0.000 description 1
- 240000004543 Vicia ervilia Species 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000012512 characterization method Methods 0.000 description 1
- 238000007596 consolidation process Methods 0.000 description 1
- 239000012792 core layer Substances 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000005137 deposition process Methods 0.000 description 1
- JXSJBGJIGXNWCI-UHFFFAOYSA-N diethyl 2-[(dimethoxyphosphorothioyl)thio]succinate Chemical compound CCOC(=O)CC(SP(=S)(OC)OC)C(=O)OCC JXSJBGJIGXNWCI-UHFFFAOYSA-N 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- HDGGAKOVUDZYES-UHFFFAOYSA-K erbium(iii) chloride Chemical compound Cl[Er](Cl)Cl HDGGAKOVUDZYES-UHFFFAOYSA-K 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000005816 glass manufacturing process Methods 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- QEFYFXOXNSNQGX-UHFFFAOYSA-N neodymium atom Chemical compound [Nd] QEFYFXOXNSNQGX-UHFFFAOYSA-N 0.000 description 1
- ATINCSYRHURBSP-UHFFFAOYSA-K neodymium(iii) chloride Chemical compound Cl[Nd](Cl)Cl ATINCSYRHURBSP-UHFFFAOYSA-K 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- -1 polytetrafluoroethylene Polymers 0.000 description 1
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 1
- 239000004810 polytetrafluoroethylene Substances 0.000 description 1
- 230000000750 progressive effect Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000001356 surgical procedure Methods 0.000 description 1
- 238000009827 uniform distribution Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/01—Manufacture of glass fibres or filaments
- C03B37/012—Manufacture of preforms for drawing fibres or filaments
- C03B37/014—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD]
- C03B37/018—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD] by glass deposition on a glass substrate, e.g. by inside-, modified-, plasma-, or plasma modified- chemical vapour deposition [ICVD, MCVD, PCVD, PMCVD], i.e. by thin layer coating on the inside or outside of a glass tube or on a glass rod
- C03B37/01884—Means for supporting, rotating and translating tubes or rods being formed, e.g. lathes
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/01—Manufacture of glass fibres or filaments
- C03B37/012—Manufacture of preforms for drawing fibres or filaments
- C03B37/014—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD]
- C03B37/018—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD] by glass deposition on a glass substrate, e.g. by inside-, modified-, plasma-, or plasma modified- chemical vapour deposition [ICVD, MCVD, PCVD, PMCVD], i.e. by thin layer coating on the inside or outside of a glass tube or on a glass rod
- C03B37/01807—Reactant delivery systems, e.g. reactant deposition burners
- C03B37/01838—Reactant delivery systems, e.g. reactant deposition burners for delivering and depositing additional reactants as liquids or solutions, e.g. for solution doping of the deposited glass
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B2201/00—Type of glass produced
- C03B2201/06—Doped silica-based glasses
- C03B2201/30—Doped silica-based glasses doped with metals, e.g. Ga, Sn, Sb, Pb or Bi
- C03B2201/34—Doped silica-based glasses doped with metals, e.g. Ga, Sn, Sb, Pb or Bi doped with rare earth metals, i.e. with Sc, Y or lanthanides, e.g. for laser-amplifiers
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Manufacture, Treatment Of Glass Fibers (AREA)
- Glass Compositions (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR8714286 | 1987-10-16 | ||
| FR8714286A FR2621909B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1987-10-16 | 1987-10-16 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1314441C true CA1314441C (fr) | 1993-03-16 |
Family
ID=9355877
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000580205A Expired - Fee Related CA1314441C (fr) | 1987-10-16 | 1988-10-14 | Procede de realisation d'un tube de verre transparent a dopage interne, notamment pour la fabrication de fibres optiques dopees par une terre rare |
Country Status (9)
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5284500A (en) * | 1989-10-31 | 1994-02-08 | Fujitsu Limited | Process for fabricating an optical fiber preform |
| AU625144B2 (en) * | 1989-10-31 | 1992-07-02 | Fujitsu Limited | Production method for optical fiber base material |
| EP0443781A1 (en) * | 1990-02-23 | 1991-08-28 | AT&T Corp. | Method for doping optical fibers |
| FR2659755B1 (fr) * | 1990-03-16 | 1992-05-29 | Alcatel Nv | Amplificateur optique a fibre dopee a l'erbium. |
| FR2677972B1 (fr) * | 1991-06-21 | 1996-12-06 | France Telecom | Procede de fabrication de preformes pour fibres optiques et dispositif pour la mise en óoeuvre de ce procede. |
| KR0167132B1 (ko) * | 1996-03-30 | 1999-01-15 | 윤종용 | 어븀 첨가 광섬유의 제조 방법 및 장치 |
| US6192713B1 (en) | 1998-06-30 | 2001-02-27 | Sdl, Inc. | Apparatus for the manufacture of glass preforms |
| JP2000191336A (ja) * | 1998-12-28 | 2000-07-11 | Hoya Corp | 光ファイバ―プリフォ―ムの製造方法および光ファイバ―の製造方法 |
| NL2006962C2 (nl) * | 2011-06-17 | 2012-12-18 | Draka Comteq Bv | Inrichting en werkwijze voor het vervaardigen van een optische voorvorm. |
| CN104843987A (zh) * | 2015-03-10 | 2015-08-19 | 武汉理工大学 | 粉体离子均匀掺杂石英棒的制备方法 |
| CN106698920A (zh) * | 2016-12-19 | 2017-05-24 | 中国电子科技集团公司第四十六研究所 | 一种制备有源光纤的离子溶液掺杂方法 |
| CN112408775B (zh) * | 2020-11-13 | 2022-10-18 | 烽火通信科技股份有限公司 | 一种光纤预制棒制造设备 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1496788A (en) * | 1974-09-05 | 1978-01-05 | Standard Telephones Cables Ltd | Optical fibre manufacture |
| GB1562032A (en) * | 1977-03-24 | 1980-03-05 | Standard Telephones Cables Ltd | Optical fibre manufacture |
| DE2907833A1 (de) * | 1979-02-28 | 1980-09-11 | Siemens Ag | Verfahren zur herstellung von beschichteten glaskoerpern |
| GB2043619B (en) * | 1979-03-07 | 1983-01-26 | Standard Telephones Cables Ltd | Optical fibre and optical fibre preform manufacture |
| IT1119362B (it) * | 1979-09-10 | 1986-03-10 | Cselt Centro Studi Lab Telecom | Procedimento ed apparecchiatura per la produzione di preforme per fibre ottiche |
| CA1166527A (en) * | 1979-09-26 | 1984-05-01 | Shiro Takahashi | Method and apparatus for producing multi-component glass fiber preform |
| FR2473497B2 (fr) * | 1980-01-09 | 1985-07-05 | Editions Filmees | Procede et installation de fabrication de preforme pour fibres optiques |
| GB2199029B (en) * | 1985-08-13 | 1990-09-05 | Simon Blanchette Poole | Fabrication of optical fibres |
| GB8610053D0 (en) * | 1986-04-24 | 1986-05-29 | British Telecomm | Glass fibre |
| DE3733880A1 (de) * | 1987-10-07 | 1989-04-20 | Schott Glaswerke | Verfahren zur herstellung eines lichtwellenleiters |
| US4848998A (en) * | 1988-01-21 | 1989-07-18 | Polaroid Corporation | Selective volitization method for preparing fiber optics |
| JPH08135148A (ja) * | 1994-11-08 | 1996-05-28 | Sekisui Chem Co Ltd | 複合床材 |
-
1987
- 1987-10-16 FR FR8714286A patent/FR2621909B1/fr not_active Expired - Lifetime
-
1988
- 1988-10-10 ES ES198888116745T patent/ES2026238T3/es not_active Expired - Lifetime
- 1988-10-10 DE DE8888116745T patent/DE3864649D1/de not_active Expired - Lifetime
- 1988-10-10 AT AT88116745T patent/ATE66905T1/de not_active IP Right Cessation
- 1988-10-10 EP EP88116745A patent/EP0311942B1/fr not_active Expired - Lifetime
- 1988-10-14 JP JP63259261A patent/JP2549901B2/ja not_active Expired - Lifetime
- 1988-10-14 CA CA000580205A patent/CA1314441C/fr not_active Expired - Fee Related
- 1988-10-14 US US07/257,666 patent/US4952225A/en not_active Expired - Fee Related
-
1991
- 1991-11-21 GR GR91401798T patent/GR3003169T3/el unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EP0311942A1 (fr) | 1989-04-19 |
| FR2621909B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1990-01-19 |
| JP2549901B2 (ja) | 1996-10-30 |
| DE3864649D1 (de) | 1991-10-10 |
| US4952225A (en) | 1990-08-28 |
| ATE66905T1 (de) | 1991-09-15 |
| JPH01141829A (ja) | 1989-06-02 |
| FR2621909A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1989-04-21 |
| EP0311942B1 (fr) | 1991-09-04 |
| GR3003169T3 (en) | 1993-02-17 |
| ES2026238T3 (es) | 1992-04-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKLA | Lapsed |