CA1134236A - Process and apparatus for controlling distributing and monitoring liquids - Google Patents
Process and apparatus for controlling distributing and monitoring liquidsInfo
- Publication number
- CA1134236A CA1134236A CA341,140A CA341140A CA1134236A CA 1134236 A CA1134236 A CA 1134236A CA 341140 A CA341140 A CA 341140A CA 1134236 A CA1134236 A CA 1134236A
- Authority
- CA
- Canada
- Prior art keywords
- liquid
- applicator
- filamentary material
- tow
- band
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000007788 liquid Substances 0.000 title claims abstract description 84
- 238000000034 method Methods 0.000 title claims abstract description 21
- 238000012544 monitoring process Methods 0.000 title abstract description 3
- 238000006073 displacement reaction Methods 0.000 claims abstract description 17
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 9
- 239000000463 material Substances 0.000 claims description 24
- 239000004014 plasticizer Substances 0.000 claims description 24
- 229920002301 cellulose acetate Polymers 0.000 claims description 2
- 230000000717 retained effect Effects 0.000 claims description 2
- 239000011344 liquid material Substances 0.000 claims 2
- 238000004519 manufacturing process Methods 0.000 description 7
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 6
- URAYPUMNDPQOKB-UHFFFAOYSA-N triacetin Chemical compound CC(=O)OCC(OC(C)=O)COC(C)=O URAYPUMNDPQOKB-UHFFFAOYSA-N 0.000 description 6
- 239000000654 additive Substances 0.000 description 4
- 230000000996 additive effect Effects 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000012530 fluid Substances 0.000 description 3
- 235000013773 glyceryl triacetate Nutrition 0.000 description 3
- 229960002622 triacetin Drugs 0.000 description 3
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000001087 glyceryl triacetate Substances 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 101150094640 Siae gene Proteins 0.000 description 1
- DOOTYTYQINUNNV-UHFFFAOYSA-N Triethyl citrate Chemical compound CCOC(=O)CC(O)(C(=O)OCC)CC(=O)OCC DOOTYTYQINUNNV-UHFFFAOYSA-N 0.000 description 1
- 239000007767 bonding agent Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- AEDZKIACDBYJLQ-UHFFFAOYSA-N ethane-1,2-diol;hydrate Chemical compound O.OCCO AEDZKIACDBYJLQ-UHFFFAOYSA-N 0.000 description 1
- 239000002657 fibrous material Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 229920000669 heparin Polymers 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 229940059904 light mineral oil Drugs 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 229910001629 magnesium chloride Inorganic materials 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000001069 triethyl citrate Substances 0.000 description 1
- VMYFZRTXGLUXMZ-UHFFFAOYSA-N triethyl citrate Natural products CCOC(=O)C(O)(C(=O)OCC)C(=O)OCC VMYFZRTXGLUXMZ-UHFFFAOYSA-N 0.000 description 1
- 235000013769 triethyl citrate Nutrition 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05C—APPARATUS FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05C11/00—Component parts, details or accessories not specifically provided for in groups B05C1/00 - B05C9/00
- B05C11/10—Storage, supply or control of liquid or other fluent material; Recovery of excess liquid or other fluent material
- B05C11/1047—Apparatus or installations for supplying liquid or other fluent material comprising a buffer container or an accumulator between the supply source and the applicator
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/022—Applying additives to filter materials with liquid additives, e.g. application of plasticisers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05B—SPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
- B05B13/00—Machines or plants for applying liquids or other fluent materials to surfaces of objects or other work by spraying, not covered by groups B05B1/00 - B05B11/00
- B05B13/02—Means for supporting work; Arrangement or mounting of spray heads; Adaptation or arrangement of means for feeding work
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05B—SPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
- B05B14/00—Arrangements for collecting, re-using or eliminating excess spraying material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05B—SPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
- B05B3/00—Spraying or sprinkling apparatus with moving outlet elements or moving deflecting elements
- B05B3/02—Spraying or sprinkling apparatus with moving outlet elements or moving deflecting elements with rotating elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05C—APPARATUS FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05C11/00—Component parts, details or accessories not specifically provided for in groups B05C1/00 - B05C9/00
- B05C11/10—Storage, supply or control of liquid or other fluent material; Recovery of excess liquid or other fluent material
- B05C11/1002—Means for controlling supply, i.e. flow or pressure, of liquid or other fluent material to the applying apparatus, e.g. valves
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05C—APPARATUS FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05C11/00—Component parts, details or accessories not specifically provided for in groups B05C1/00 - B05C9/00
- B05C11/10—Storage, supply or control of liquid or other fluent material; Recovery of excess liquid or other fluent material
- B05C11/1039—Recovery of excess liquid or other fluent material; Controlling means therefor
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B5/00—Forcing liquids, gases or vapours through textile materials to effect treatment, e.g. washing, dyeing, bleaching, sizing impregnating
- D06B5/02—Forcing liquids, gases or vapours through textile materials to effect treatment, e.g. washing, dyeing, bleaching, sizing impregnating through moving materials of indefinite length
- D06B5/10—Forcing liquids, gases or vapours through textile materials to effect treatment, e.g. washing, dyeing, bleaching, sizing impregnating through moving materials of indefinite length using centrifugal force
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
- Y02P70/10—Greenhouse gas [GHG] capture, material saving, heat recovery or other energy efficient measures, e.g. motor control, characterised by manufacturing processes, e.g. for rolling metal or metal working
Abstract
PROCESS AND APPARATUS FOR CONTROLLING, DISTRIBUTING AND MONITORING LIQUIDS
ABSTRACT OF THE DISCLOSURE
A process and apparatus for controlled application of a liquid to a variable width filamentary band such as a cigarette tow band.
Liquid is fed at a constant rate by one or more positive displace-ment pumps to an applicator device which may be a disc type or a brush type applicator device. Any liquid which is not picked up from the applicator device by the tow band is returned by means of channels located in a housing member directly to the applicator device whereby variations in the width of the tow band do not sub-stantially change tow liquid pick-up from a preselected weight level.
ABSTRACT OF THE DISCLOSURE
A process and apparatus for controlled application of a liquid to a variable width filamentary band such as a cigarette tow band.
Liquid is fed at a constant rate by one or more positive displace-ment pumps to an applicator device which may be a disc type or a brush type applicator device. Any liquid which is not picked up from the applicator device by the tow band is returned by means of channels located in a housing member directly to the applicator device whereby variations in the width of the tow band do not sub-stantially change tow liquid pick-up from a preselected weight level.
Description
~3~3~5 This invention relates to the treatment of filamentary and other fibrous materials in order to impart certain desired or selected properties thereto and is more particularly con-cerned with the production of filter-rod stock for use in the manufacture of filter-tip cigarettes.
Filters for ciqarettes are commonly formed from a multi-plicity of filaments arranged in essentially longitudinal aliqn-ment with substantially all of such filaments extending continu-ously from one end of the filter to the other. In the production of such a filter, a tow or bundle of upward of several thousand substantially longitudinally aligned continuous filaments, pre-ferably already suitably crimped, is passed through one or more devices that serve essentially to open up the advancing tow. The result is that the tow assumes the appearance more or less of a continuous band or web of varyingly increased width. The many different arrangements that have been proposed to accomplish this objective range from those which ordinarily do little more than flatten, widen, and/or smooth out the tow to those which also separate the filaments as necessary to bring the same more nearly into longitudinal alignment and/or to effect deregistra-tion of the crimp in adjacent filaments.
The open tow may be treated with a selective additive material in order to impart a desired property or effect thereto.
Such additive material may be in liquid form. Illustrative types of liquid-form additive materials comprise plasticizers such as glycerol triacetate ~triacetin) and triethyl citrate, lubricants such as light mineral oil and diethylene glycol, and antistatic aqents such as mixtures of magnesium chloride in water and diethylene glycol.
o ~.~3~Z3 The resultinq opened, spr~ad and liquid treated tow may then be passed without any further treatment essentially direct-ly to the garnit~re of a filter-roa maker, wherein it is con-densed to provide a continuous filter-rod stock having a cross-S sectional area corresponding to that of the filter-tipped ciga-rettes to be produced. Customarily, the desired filter rods are obtained by appropriately cutting or severing such continuous filter-rod stock as it issues from the garniture.
A number of procedures is available for applying a liguid form material to the advancing tow. A liquid-form treating material such as a plasticizer or other filament-bonding agent, for example, is customarily discharged through appropriately arranged and designed nozzles, wicks or spray-~orming devices such as rotary brushes such as are disclosed in U.S. Defensive Pub-lS lication T ~74~005 published May 19, 1970 or rotary discs such as are disclcsed in ~.S. Patents Nos. 3,387,992 and 3,818,863. However, all of these prior art applicators pass excess liguid; that is to say, liquid not picked up by the tow to a holdinq device or tank and therefore there is no mechanism to compensate for unequal liquid pick-up.
Regardless of the method employed for applying the liquid form material to the tow band, it is necessary to monitor and control the amount of liquid form material applied to the tow.
The most common method of the prior art for determining the amount of liguid form added to the tow band i5 the so-called wet/dry weight method. In this system, a wet rod sample is taken and a weight measurement made and then liquid application is discon-tinued. When sufficient time has elapsed to assure there is no liquid application, dry rod samples are taken and a dry weight measurement is made. This method of ~onitoring is, of course, a discontinous method and is inherently wasteful. An improved prior art system for determining liquid add-on is a metering system ~ased on the use of a pneumatically eontrolled, valveless, r ~ ~ i 3~
positive-displacement pump. This pump supplies plasticizer to the plasticizer-application booth at a rate that is egual to the rate at which the plasticizer is applied to the tow. A
pneumatic system governs the pump speed and is activated by a float valve in the applicator booth~ When the aepth of plastici-ser in the booth decreases from a nominal, predetermined level, the float valve closes, creating a pressure differential across a diaphragm. The diaphragm then opens a valve that controls the supply of air to an air-ariven motor that drives the pump.
The pump speed relates to the position of the float valve and is proportional to deviations in the depth of the plasticizer in the booth. The pump is fitted with an optical sensor that detects the rotation of the pump. As the pump rotates, a series of electrical impulses is produced. The frequency of these impulses is proportional to the rate at which the pump rotates, and therefore to the flow rate of the plasticizer.
Since the pump has a positive displacement, each impulse can be equated to a known quantity of plasticizer, for example, in mg/pulse.
In theory, if the depth of plasticizer is maintained con-stant, the amount of plasticizer pumped to the applicator booth can be assumed to equal the amount applied to the tow during any particular time interval. The positive-displacement pump is then used to establish the amount of plasticizer .hat flows ~5 into the system over a period of time. With this irformation alone, an instrument can be provided that will display a reading of the amount of plasticizer flowing onto the tow, for e~ample, in mg/min.
As previously noted in all of the prior art liquid applicator processes and apparatus for the treatment of tow, liquid which ~3~Z3Ç~
is not applied to the tow is returned to a hold;ng device and- must be measured in order to determine the liquid add-on.
The disadvantages of these monitoring methods include the prob-ability of untreated cigarette filter rods entering production, loss Of production itself, as well as waste. Moreover, none of the prior art processes and apparatus have a variable control for the amount of liquid applied to the tow; that is to say, variations in tow band width will cause corresponding variations in liquid pick-up for which there is no compensation in prior art processes and apparatus.
It is therefore an object of this invention to provide a process for the preparation of cigarette filter rods wherein liquid add-on is constant in spite of tow band width variation.
It is another object of this invention to provide a liquid lS form add-on apparatus for the treatment of continuous filament tow in the preparation of cigarette filter roas wherein only one liguid flow line need be monitored.
It has been discovered that the aforementioned objectives can be achieved in a process for controlled application of a liquid to a filamentary material by feeding liquid at a con- i stant rate to an applicator device suitable for applying liquid to a running band of filamentary material and causing any liquid not picked up by the tow band to be returned directly to the applicator device. Preferably the liquid is fed at a constant rate by a positive displacement pump and the liqu;d applicator device is a rotatable brush or a rotatable disc. The apparatus of the instant invention employs a housing provided with means for draining any liquid not returned by said filamentary material back to the applicator means.
,~
_ 5 _ '~3~Z3~
This invention relates to a process for controlled application of a liquid to a filamentary material comprising, feeding said liquid at a constant rate by means of a first positive displacement pump into the center of a rotatable disc applicator device suitable for applying liquid to a running band of filamentary material, and causing any liquid not picked up by said band of filamentary material to be returned directly to said applicator device by means of a second positive displacement pump.
~ .
D `:
-5a-~3~Z3Ç~
A better understanding of the invention may be had from a discussion of the drawings wherein:
FIG. 1 is a schematic flow diagram of the controlled fluid applicator of this invention suitable for use with a brush type liquid applicator.
FIG. 2 is a cross sectional view o~ a brush type liquid applicator suitable for use in this invention.
FIG. 3 is a projected view of the bottom portion of the brush type liq~id applicator of FIG. 2 of the drawi~gs.
~IG. 4 is a schematic flow diagram of the controlled fluid applicatOr of this invention suitable for use with a disc type liquid applicator.
FIG. S is a cross sectional view of a disc type liquid applicator suitable for use in this invention.
FIG. 6 is a projected view of the bottom portion of the disc type liquid applicator o FIG. 5 of the drawings.
FIG. 7 is a graph illustrating the effect of cigarette tow band width change.
Turning to FIG. 1 of the drawings, liquid from a tank member 1 is pumped by means of a centrifugal pump 2 to a pump supply reservoir 3, pump supply resevoir being maintained at a constant level by means o an overflow pipe 4 which feeds excess liquid back to plasticizer tank 1. A positive displace-ment pump 5 then feeds liquid from the constant~pump supply re-servoir to the delivery manifold 6 of the liquid applicator device 7, delivery manifold 6 supplying liq~id to brush member 9 of liquid applicator device 7. It should be understood that a single positive displacement pump or any plurality of positive 3~231~
displacement pumps which are preferably gear pumps may also be employed for purposes of this inven~ion. By metering plasticizer into the chamber with a gear pump, t~e revolutions per minute of the pump provides the flow information required. A three-way S valve 8 is positioned intermediate gear pumps 5 and delivery manifold 6 in order that liquid feed to the delivery manifold may be diverted bac~ to the plasticizer tank in the event of a discontinuation of feed of material to the applicator chamber 7.
As can be seen in FIGS. 2 and 3 of the drawings, the brush type applicator suitable for use in conjunction with this inven--tion employs a housinq or.cabinet 21 made.of any suitable material and having detachable top and bottom spections. Preferably the bottom portion of the housing 21 consists of side walls 22 ana 23, front and rear walls 24 and 25 respectively, and a floor 26.
The housing floor 26 extends from the lowermost edges of the side walls 22 and 23 at a relatively gentle downward slope.
Positioned near the lowermost point of floor member 26 is delivery manifold member 30, delivery manifold member 30 being positioned between drain-back dam 26a and brush member 31, the peripheral portion of brush member 31 ac~uall~ contacting de- _ livery manifold mmember 30. In order to facilitate drainage and cleaning operations, a drain slot 32 is positioned through housing floor member 26 immediately beneath brush member 31.
The ceilinq 27 of the housing 21 is closed and consists o~ a pair of sections extending toward one another at an incline steep slope from the uppermost edges of the side walls. In Qperation, a constant flow of liquid is continuously supplied through the elongated slot in delivery manifold 30, liquid being L
~3~36 pic~ea up by brush member 31 and deposited on tow passing through housing member 31. Baffle members 33 and 34 are positioned on either side of-brush member 31 to insure that liquid projected by brush member 31 is properly directed~ Any liquid not picked ~p by the tow due to liquid by pass or variations in tow width is caused by the design of chamber member 21 to be returned to brush member 31 and then recycled by the brush member 31 to the advancing tow line. More specifically, liquid not applied to the tow band collects from the ceiling 27 of the housing 21 and flows downwardly into the channel sections of baffle members 27a.
Liquid then flows from baffle members 27a into side channels 29 and thence into drainback gutter 29a~ Liquid continues to flow down sidewalls 22 and 23 ana collects in drainback dam 26a. The drain-bac~ dam 26a distributes liquid uniformly back to brush member 31. Drain-back dam member 26a is also useful in facilitat-in~ cleaning of the apparatus.
The monitored fluid applicator of this invention is also suitable for use in conjunction with disc-type liquid appli-cation. A better understanding of this applicatar may be had from FIGS. 4 through 6 of the drawings:
Turning to FIG.4 of the drawings, which is a flow sheet,liquid from a tank member 41 is pumped by means of pump member 42 through a three-way solenoid valve 43 into the center of a rotat-inq disc applicator 44 which is positioned beneath a tow band ~not illustrated) passin~ through applicator chamber 45. Liquid distributed by disc member 44 and not absorbed by the tow, flows to the bottom of chamber member 45 which is~equipped with a drain 46 and flows to a three-way solenoid valve 47 which directs :, ~3~3~
liquid flow to a centrifugal pump 48. Pump member 48 in turn directs the flow of liquid back to solenoid valve 43 which in turn directs the liquid back into disc member 44. Equilibrium is achieved by the pump and valve arrangement of this invention and the liquid add-on level is controlled and equal to the pump member 42. When dry runs are desired, that is to say when it is desired to manufacture rods without any liquid addition, plasticizer is pumped from tank member 41 by positive displace-ment pump member 42 to solenoid valve member 43. Solenoid valve member 43 in turn directs liquid back to tank member 41. In addition, liquid is pumped from tank member 41 through solenoid valve member 47 by centrifugal pump member 48. Liquid from pump member 48 is directed to solenoid valve member 43 and in turn flows back to tanX member 41, thereby maintaining flow through centrifugal pump member 48 so as to prevent pump member 48 from running dry. It should be understood, however, that centrifugal pump member 48 may be replaced with other pump members such as for instance vane pumps, lob-type pumps, or other semi-positive displacement pumps.
A better understanding of the mechanism of the disc-type - ~ plasticizer applicator may be had from a discussion of FIGS. 5 and 6. As can be seen in ~IG. 5, housing member 45 consiStS of an upper housing section 49 ana a lower housing section 50, upper housing member 49 being suitably baffled for recycling of liquid not retained by the tow. More specifically, liquid not re-tained by the tow is directed by baffle members 51 to the side walls (not illustrated~ of chamber member 45, chamber member 45 having flat and substantially horizontal side walls covered by _ g ' ' " ' . ' ' ' . " I ;' ' " ` ' ' ' ' ' ' ' '. ' ' ' ~3fl~3~i a peaked roof, liquid flowing from baffle member Sl down the siae walls of chamber 45 into drain 46 positioned at the bottom of the lower section 50 of chamber member 45. The geometry of the lower section 50 of chamber membex 45 is such that the down-ward flow of liquid to drain member 46 is assured.
The lower section S0 of chamber member 45 consists of a pair of floor sections 55a and 55b extending toward one another at a relatively gentle downward slope and terminating at a pre-determined distance from one another essentially medially of the lower section 50 ! thereby leaving an elongated rectangular opening 56 extending entirely across the housing floor.
Arranged below the opening 56 is a well 57 defined by two ver-tical, trapezoidal side plates 57a and 57b depending downwardly from the facing edges of floor sections 55a and 55b, two slant- ;
ed end plates 57c and 57d secured to the downwardly converging edges of the plates 57a and 57b, and a horizontal bottom plate 57e secured to the lowermost edges of the plates 57a to 57d.
Within the well 57 of lower section 50, a liquid spraying disc 44 is arranged for rotation in a plane which is substantial- , ly parallel to and centered between the well side plates 57a and 57b. The disc 44 is essentially shaped in the manner of a narrow mouthcup-like receptacle of the type such as is disclosed in U.S. Patent No. 3,387,992 Disc mem~er 44 is driven, preferably by a motor 54 located external of the well 57. It should be understood that while a single disc member 44 has been illustrated, that a plurality of discs may also be employed in either a side-by-side or back-to-- back arrangement. Liquid is introduced to the disc through port member 58 located preferably in axial alignment with the axis of rotation of disc member 44. As previously noted, the total ~L~3~
number of discs may vary but, in any event, should be sufficient to ensure that a steady state of recycled liquid is achieved;
that is to say, when band width is reduced resulting in a high-er recycle of liquid, a suffi~ient number of recycled discs should be present to quickly restore steady-state conditions. Prefer-ably, the disc-type or brush type applicator can be equipped with pressure or flow sensing switches to prevent overfilling of the plasticizer tank should the pump drive fail or should the pump drives fail resulting in production of untreated rods, the plasticizer flow rate can be determined by means of an rpm de-tector, employed in conjunction with positive displacement pump 42. I~ so desired, information from the rpm detector may be processed through a suitable conversion device which in turn activates a digital display of the liquid flow rate~ It should be understood that suitable filtering and particle trapping systems may also be incorporated in the apparatus of this invention.
The principle of the present invention will be more fully understood from the following examples wherein data has been generated employing the brush-type applicator system. It should be understood, however, that comparable results will also be obtained when the disc type applicator of this invention is employed.
Example A cigarette tow composed of 4.0 DPF cellulose acetate fila-ments having a total denier of 39,000 is passed through an applicator chamber constructed substantially in the form as illustrated in FIGS. 2 and 3 o the drawings. The to~ is pro-cessed at a linear speed of 400 meters per minute. The brush member of the applicator device is rotated at a speed of 3400 revolutions per minute. Triacetin liquid plasticizer is pump-ed to the brush at a rate of 220 grams per minute.
1~3~Z3~
As a control, a brush applicator system 54-FA-l manu-- factured ~y Hauni-Werke ~orber ~ Co. KG of Hamburg, West Germany which employs a holding tank or booth for liquid not picked up by the tow was operated with an identical tow band S with the brush nlember rotated again at 3400 revolutions per minute and the plasticizer booth supplied with plasticizer at the rate to set initial plasticizer additives at a nominal 9% The.
band width of the tow band being passed into each applicator device is reduced by altering the air flow to the spreader box, positioned in advance of the applicator chamber. The data genera-ted is as set forth in the following table:
BAND WIDTH CHANGE
HAVNI INSTANT
INVENTION
Time Rod wgt Rod wgt (Min) gms/100 rods gms/100 rods 73.3 81.9 1/4 73.5 82.
1/2 73.7 81.9 ~ 1 0 74 0 82 20 1 1/4 73.8 82.0 25 * 2 73 8 82,0
Filters for ciqarettes are commonly formed from a multi-plicity of filaments arranged in essentially longitudinal aliqn-ment with substantially all of such filaments extending continu-ously from one end of the filter to the other. In the production of such a filter, a tow or bundle of upward of several thousand substantially longitudinally aligned continuous filaments, pre-ferably already suitably crimped, is passed through one or more devices that serve essentially to open up the advancing tow. The result is that the tow assumes the appearance more or less of a continuous band or web of varyingly increased width. The many different arrangements that have been proposed to accomplish this objective range from those which ordinarily do little more than flatten, widen, and/or smooth out the tow to those which also separate the filaments as necessary to bring the same more nearly into longitudinal alignment and/or to effect deregistra-tion of the crimp in adjacent filaments.
The open tow may be treated with a selective additive material in order to impart a desired property or effect thereto.
Such additive material may be in liquid form. Illustrative types of liquid-form additive materials comprise plasticizers such as glycerol triacetate ~triacetin) and triethyl citrate, lubricants such as light mineral oil and diethylene glycol, and antistatic aqents such as mixtures of magnesium chloride in water and diethylene glycol.
o ~.~3~Z3 The resultinq opened, spr~ad and liquid treated tow may then be passed without any further treatment essentially direct-ly to the garnit~re of a filter-roa maker, wherein it is con-densed to provide a continuous filter-rod stock having a cross-S sectional area corresponding to that of the filter-tipped ciga-rettes to be produced. Customarily, the desired filter rods are obtained by appropriately cutting or severing such continuous filter-rod stock as it issues from the garniture.
A number of procedures is available for applying a liguid form material to the advancing tow. A liquid-form treating material such as a plasticizer or other filament-bonding agent, for example, is customarily discharged through appropriately arranged and designed nozzles, wicks or spray-~orming devices such as rotary brushes such as are disclosed in U.S. Defensive Pub-lS lication T ~74~005 published May 19, 1970 or rotary discs such as are disclcsed in ~.S. Patents Nos. 3,387,992 and 3,818,863. However, all of these prior art applicators pass excess liguid; that is to say, liquid not picked up by the tow to a holdinq device or tank and therefore there is no mechanism to compensate for unequal liquid pick-up.
Regardless of the method employed for applying the liquid form material to the tow band, it is necessary to monitor and control the amount of liquid form material applied to the tow.
The most common method of the prior art for determining the amount of liguid form added to the tow band i5 the so-called wet/dry weight method. In this system, a wet rod sample is taken and a weight measurement made and then liquid application is discon-tinued. When sufficient time has elapsed to assure there is no liquid application, dry rod samples are taken and a dry weight measurement is made. This method of ~onitoring is, of course, a discontinous method and is inherently wasteful. An improved prior art system for determining liquid add-on is a metering system ~ased on the use of a pneumatically eontrolled, valveless, r ~ ~ i 3~
positive-displacement pump. This pump supplies plasticizer to the plasticizer-application booth at a rate that is egual to the rate at which the plasticizer is applied to the tow. A
pneumatic system governs the pump speed and is activated by a float valve in the applicator booth~ When the aepth of plastici-ser in the booth decreases from a nominal, predetermined level, the float valve closes, creating a pressure differential across a diaphragm. The diaphragm then opens a valve that controls the supply of air to an air-ariven motor that drives the pump.
The pump speed relates to the position of the float valve and is proportional to deviations in the depth of the plasticizer in the booth. The pump is fitted with an optical sensor that detects the rotation of the pump. As the pump rotates, a series of electrical impulses is produced. The frequency of these impulses is proportional to the rate at which the pump rotates, and therefore to the flow rate of the plasticizer.
Since the pump has a positive displacement, each impulse can be equated to a known quantity of plasticizer, for example, in mg/pulse.
In theory, if the depth of plasticizer is maintained con-stant, the amount of plasticizer pumped to the applicator booth can be assumed to equal the amount applied to the tow during any particular time interval. The positive-displacement pump is then used to establish the amount of plasticizer .hat flows ~5 into the system over a period of time. With this irformation alone, an instrument can be provided that will display a reading of the amount of plasticizer flowing onto the tow, for e~ample, in mg/min.
As previously noted in all of the prior art liquid applicator processes and apparatus for the treatment of tow, liquid which ~3~Z3Ç~
is not applied to the tow is returned to a hold;ng device and- must be measured in order to determine the liquid add-on.
The disadvantages of these monitoring methods include the prob-ability of untreated cigarette filter rods entering production, loss Of production itself, as well as waste. Moreover, none of the prior art processes and apparatus have a variable control for the amount of liquid applied to the tow; that is to say, variations in tow band width will cause corresponding variations in liquid pick-up for which there is no compensation in prior art processes and apparatus.
It is therefore an object of this invention to provide a process for the preparation of cigarette filter rods wherein liquid add-on is constant in spite of tow band width variation.
It is another object of this invention to provide a liquid lS form add-on apparatus for the treatment of continuous filament tow in the preparation of cigarette filter roas wherein only one liguid flow line need be monitored.
It has been discovered that the aforementioned objectives can be achieved in a process for controlled application of a liquid to a filamentary material by feeding liquid at a con- i stant rate to an applicator device suitable for applying liquid to a running band of filamentary material and causing any liquid not picked up by the tow band to be returned directly to the applicator device. Preferably the liquid is fed at a constant rate by a positive displacement pump and the liqu;d applicator device is a rotatable brush or a rotatable disc. The apparatus of the instant invention employs a housing provided with means for draining any liquid not returned by said filamentary material back to the applicator means.
,~
_ 5 _ '~3~Z3~
This invention relates to a process for controlled application of a liquid to a filamentary material comprising, feeding said liquid at a constant rate by means of a first positive displacement pump into the center of a rotatable disc applicator device suitable for applying liquid to a running band of filamentary material, and causing any liquid not picked up by said band of filamentary material to be returned directly to said applicator device by means of a second positive displacement pump.
~ .
D `:
-5a-~3~Z3Ç~
A better understanding of the invention may be had from a discussion of the drawings wherein:
FIG. 1 is a schematic flow diagram of the controlled fluid applicator of this invention suitable for use with a brush type liquid applicator.
FIG. 2 is a cross sectional view o~ a brush type liquid applicator suitable for use in this invention.
FIG. 3 is a projected view of the bottom portion of the brush type liq~id applicator of FIG. 2 of the drawi~gs.
~IG. 4 is a schematic flow diagram of the controlled fluid applicatOr of this invention suitable for use with a disc type liquid applicator.
FIG. S is a cross sectional view of a disc type liquid applicator suitable for use in this invention.
FIG. 6 is a projected view of the bottom portion of the disc type liquid applicator o FIG. 5 of the drawings.
FIG. 7 is a graph illustrating the effect of cigarette tow band width change.
Turning to FIG. 1 of the drawings, liquid from a tank member 1 is pumped by means of a centrifugal pump 2 to a pump supply reservoir 3, pump supply resevoir being maintained at a constant level by means o an overflow pipe 4 which feeds excess liquid back to plasticizer tank 1. A positive displace-ment pump 5 then feeds liquid from the constant~pump supply re-servoir to the delivery manifold 6 of the liquid applicator device 7, delivery manifold 6 supplying liq~id to brush member 9 of liquid applicator device 7. It should be understood that a single positive displacement pump or any plurality of positive 3~231~
displacement pumps which are preferably gear pumps may also be employed for purposes of this inven~ion. By metering plasticizer into the chamber with a gear pump, t~e revolutions per minute of the pump provides the flow information required. A three-way S valve 8 is positioned intermediate gear pumps 5 and delivery manifold 6 in order that liquid feed to the delivery manifold may be diverted bac~ to the plasticizer tank in the event of a discontinuation of feed of material to the applicator chamber 7.
As can be seen in FIGS. 2 and 3 of the drawings, the brush type applicator suitable for use in conjunction with this inven--tion employs a housinq or.cabinet 21 made.of any suitable material and having detachable top and bottom spections. Preferably the bottom portion of the housing 21 consists of side walls 22 ana 23, front and rear walls 24 and 25 respectively, and a floor 26.
The housing floor 26 extends from the lowermost edges of the side walls 22 and 23 at a relatively gentle downward slope.
Positioned near the lowermost point of floor member 26 is delivery manifold member 30, delivery manifold member 30 being positioned between drain-back dam 26a and brush member 31, the peripheral portion of brush member 31 ac~uall~ contacting de- _ livery manifold mmember 30. In order to facilitate drainage and cleaning operations, a drain slot 32 is positioned through housing floor member 26 immediately beneath brush member 31.
The ceilinq 27 of the housing 21 is closed and consists o~ a pair of sections extending toward one another at an incline steep slope from the uppermost edges of the side walls. In Qperation, a constant flow of liquid is continuously supplied through the elongated slot in delivery manifold 30, liquid being L
~3~36 pic~ea up by brush member 31 and deposited on tow passing through housing member 31. Baffle members 33 and 34 are positioned on either side of-brush member 31 to insure that liquid projected by brush member 31 is properly directed~ Any liquid not picked ~p by the tow due to liquid by pass or variations in tow width is caused by the design of chamber member 21 to be returned to brush member 31 and then recycled by the brush member 31 to the advancing tow line. More specifically, liquid not applied to the tow band collects from the ceiling 27 of the housing 21 and flows downwardly into the channel sections of baffle members 27a.
Liquid then flows from baffle members 27a into side channels 29 and thence into drainback gutter 29a~ Liquid continues to flow down sidewalls 22 and 23 ana collects in drainback dam 26a. The drain-bac~ dam 26a distributes liquid uniformly back to brush member 31. Drain-back dam member 26a is also useful in facilitat-in~ cleaning of the apparatus.
The monitored fluid applicator of this invention is also suitable for use in conjunction with disc-type liquid appli-cation. A better understanding of this applicatar may be had from FIGS. 4 through 6 of the drawings:
Turning to FIG.4 of the drawings, which is a flow sheet,liquid from a tank member 41 is pumped by means of pump member 42 through a three-way solenoid valve 43 into the center of a rotat-inq disc applicator 44 which is positioned beneath a tow band ~not illustrated) passin~ through applicator chamber 45. Liquid distributed by disc member 44 and not absorbed by the tow, flows to the bottom of chamber member 45 which is~equipped with a drain 46 and flows to a three-way solenoid valve 47 which directs :, ~3~3~
liquid flow to a centrifugal pump 48. Pump member 48 in turn directs the flow of liquid back to solenoid valve 43 which in turn directs the liquid back into disc member 44. Equilibrium is achieved by the pump and valve arrangement of this invention and the liquid add-on level is controlled and equal to the pump member 42. When dry runs are desired, that is to say when it is desired to manufacture rods without any liquid addition, plasticizer is pumped from tank member 41 by positive displace-ment pump member 42 to solenoid valve member 43. Solenoid valve member 43 in turn directs liquid back to tank member 41. In addition, liquid is pumped from tank member 41 through solenoid valve member 47 by centrifugal pump member 48. Liquid from pump member 48 is directed to solenoid valve member 43 and in turn flows back to tanX member 41, thereby maintaining flow through centrifugal pump member 48 so as to prevent pump member 48 from running dry. It should be understood, however, that centrifugal pump member 48 may be replaced with other pump members such as for instance vane pumps, lob-type pumps, or other semi-positive displacement pumps.
A better understanding of the mechanism of the disc-type - ~ plasticizer applicator may be had from a discussion of FIGS. 5 and 6. As can be seen in ~IG. 5, housing member 45 consiStS of an upper housing section 49 ana a lower housing section 50, upper housing member 49 being suitably baffled for recycling of liquid not retained by the tow. More specifically, liquid not re-tained by the tow is directed by baffle members 51 to the side walls (not illustrated~ of chamber member 45, chamber member 45 having flat and substantially horizontal side walls covered by _ g ' ' " ' . ' ' ' . " I ;' ' " ` ' ' ' ' ' ' ' '. ' ' ' ~3fl~3~i a peaked roof, liquid flowing from baffle member Sl down the siae walls of chamber 45 into drain 46 positioned at the bottom of the lower section 50 of chamber member 45. The geometry of the lower section 50 of chamber membex 45 is such that the down-ward flow of liquid to drain member 46 is assured.
The lower section S0 of chamber member 45 consists of a pair of floor sections 55a and 55b extending toward one another at a relatively gentle downward slope and terminating at a pre-determined distance from one another essentially medially of the lower section 50 ! thereby leaving an elongated rectangular opening 56 extending entirely across the housing floor.
Arranged below the opening 56 is a well 57 defined by two ver-tical, trapezoidal side plates 57a and 57b depending downwardly from the facing edges of floor sections 55a and 55b, two slant- ;
ed end plates 57c and 57d secured to the downwardly converging edges of the plates 57a and 57b, and a horizontal bottom plate 57e secured to the lowermost edges of the plates 57a to 57d.
Within the well 57 of lower section 50, a liquid spraying disc 44 is arranged for rotation in a plane which is substantial- , ly parallel to and centered between the well side plates 57a and 57b. The disc 44 is essentially shaped in the manner of a narrow mouthcup-like receptacle of the type such as is disclosed in U.S. Patent No. 3,387,992 Disc mem~er 44 is driven, preferably by a motor 54 located external of the well 57. It should be understood that while a single disc member 44 has been illustrated, that a plurality of discs may also be employed in either a side-by-side or back-to-- back arrangement. Liquid is introduced to the disc through port member 58 located preferably in axial alignment with the axis of rotation of disc member 44. As previously noted, the total ~L~3~
number of discs may vary but, in any event, should be sufficient to ensure that a steady state of recycled liquid is achieved;
that is to say, when band width is reduced resulting in a high-er recycle of liquid, a suffi~ient number of recycled discs should be present to quickly restore steady-state conditions. Prefer-ably, the disc-type or brush type applicator can be equipped with pressure or flow sensing switches to prevent overfilling of the plasticizer tank should the pump drive fail or should the pump drives fail resulting in production of untreated rods, the plasticizer flow rate can be determined by means of an rpm de-tector, employed in conjunction with positive displacement pump 42. I~ so desired, information from the rpm detector may be processed through a suitable conversion device which in turn activates a digital display of the liquid flow rate~ It should be understood that suitable filtering and particle trapping systems may also be incorporated in the apparatus of this invention.
The principle of the present invention will be more fully understood from the following examples wherein data has been generated employing the brush-type applicator system. It should be understood, however, that comparable results will also be obtained when the disc type applicator of this invention is employed.
Example A cigarette tow composed of 4.0 DPF cellulose acetate fila-ments having a total denier of 39,000 is passed through an applicator chamber constructed substantially in the form as illustrated in FIGS. 2 and 3 o the drawings. The to~ is pro-cessed at a linear speed of 400 meters per minute. The brush member of the applicator device is rotated at a speed of 3400 revolutions per minute. Triacetin liquid plasticizer is pump-ed to the brush at a rate of 220 grams per minute.
1~3~Z3~
As a control, a brush applicator system 54-FA-l manu-- factured ~y Hauni-Werke ~orber ~ Co. KG of Hamburg, West Germany which employs a holding tank or booth for liquid not picked up by the tow was operated with an identical tow band S with the brush nlember rotated again at 3400 revolutions per minute and the plasticizer booth supplied with plasticizer at the rate to set initial plasticizer additives at a nominal 9% The.
band width of the tow band being passed into each applicator device is reduced by altering the air flow to the spreader box, positioned in advance of the applicator chamber. The data genera-ted is as set forth in the following table:
BAND WIDTH CHANGE
HAVNI INSTANT
INVENTION
Time Rod wgt Rod wgt (Min) gms/100 rods gms/100 rods 73.3 81.9 1/4 73.5 82.
1/2 73.7 81.9 ~ 1 0 74 0 82 20 1 1/4 73.8 82.0 25 * 2 73 8 82,0
2-1/2 71.7 79.4 3_1/2 72 90 80 9 *At two minutes, the band width was changed from 10 inches to 7 inches.
9~3423~
As can ~e seen from the table and also from the graphic representation set forth in FI~. 7 of the drawings, which plots rod weight against time, with the prior art system, rod weight dropped when tow band width was reduced. However, when the apparatus of the instant invention is employed, rod weights are quickly restored to the preselected weight level.
9~3423~
As can ~e seen from the table and also from the graphic representation set forth in FI~. 7 of the drawings, which plots rod weight against time, with the prior art system, rod weight dropped when tow band width was reduced. However, when the apparatus of the instant invention is employed, rod weights are quickly restored to the preselected weight level.
Claims (6)
PROPERTY OR PRIVILEGE IS CLAIMED ARE DEFINED AS FOLLOWS:
1. A process for controlled application of a liquid to a filamentary material comprising, feeding said liquid at a constant rate by means of a first positive displacement pump into the center of a rotatable disc applicator device suitable for applying liquid to a running band of filamentary material, and causing any liquid not picked up by said band of filamentary material to be returned directly to said applicator device by means of a second positive displacement pump.
2. The process of claim 1 wherein a plurality of said discs are employed.
3. The process of claim 1 wherein said disc is essentially shaped in the manner of a narrow mouth cup like receptacle.
4. The process of claim 1 wherein said band of filamentary material comprises an opened cigarette filter tow, and said liquid is a plasticizer.
5. The process of claim 4 wherein said tow is comprised of continuous cellulose acetate filaments.
6. Apparatus for applying a liquid material to a filamentary material, comprising a housing, said housing being provided at two opposed locations with a pair of openings defining a generally horizontal path therebetween for said filamentary material, a rotatable disc liquid applicator means located in said housing beneath said filamentary path, a first positive displacement pump providing liquid at a constant rate to said liquid applicator means, means for adjusting the rate of advance of said filamentary material past said applicator device and the rate of feed of liquid material to said applicator whereby substantially all of said liquid is picked up by said band of filamentary material, said housing being provided with a second positive displacement pump for returning any liquid not retained by said filamentary material back to said applicator means.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US96580778A | 1978-12-04 | 1978-12-04 | |
US965,807 | 1978-12-04 |
Publications (1)
Publication Number | Publication Date |
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CA1134236A true CA1134236A (en) | 1982-10-26 |
Family
ID=25510512
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA341,140A Expired CA1134236A (en) | 1978-12-04 | 1979-12-04 | Process and apparatus for controlling distributing and monitoring liquids |
Country Status (12)
Country | Link |
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JP (1) | JPS5580570A (en) |
AT (1) | ATA753779A (en) |
AU (1) | AU5293879A (en) |
BE (1) | BE880387A (en) |
BR (1) | BR7907816A (en) |
CA (1) | CA1134236A (en) |
DE (1) | DE2947488A1 (en) |
ES (2) | ES486539A1 (en) |
FR (1) | FR2443289A1 (en) |
GB (1) | GB2042375B (en) |
IT (1) | IT1126481B (en) |
PH (1) | PH15036A (en) |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE8021131U1 (en) * | 1980-08-07 | 1981-01-29 | Automation Fuer Grafische Technik Ag, 4005 Meerbusch | DEVICE FOR PRODUCING MULTIPLE PAPER PAPERS |
US4497276A (en) * | 1981-11-16 | 1985-02-05 | Brown & Williamson Tobacco Corporation | Apparatus and method for applying plasticizers to fibrous filter material |
US4509452A (en) * | 1982-10-29 | 1985-04-09 | R. J. Reynolds Tobacco Company | Application of liquid additives to cigarette filter tow |
DE10354924B4 (en) * | 2003-11-25 | 2024-01-18 | Körber Technologies Gmbh | Device for processing filter tow material and device for producing filters |
DE102004021773B4 (en) * | 2004-04-30 | 2007-02-22 | Hauni Maschinenbau Ag | Scraper and sprayer for filter tow |
DE102005038728B3 (en) * | 2005-08-15 | 2007-03-29 | Hauni Maschinenbau Ag | Method and device for supplying an additive to a filter material web |
CN101898182B (en) * | 2010-07-13 | 2012-07-04 | 长沙湖大江远系统集成有限公司 | Method and device for adding plasticizer on loosened fiber tow belt |
ITBO20110272A1 (en) * | 2011-05-16 | 2012-11-17 | Gd Spa | DEVICE FOR THE TREATMENT OF FILTERING MATERIAL FOR SMOKE ITEMS. |
CN108754932A (en) * | 2018-06-12 | 2018-11-06 | 厦门复晟复合材料有限公司 | A kind of carbon fibre initial rinse machine gluing weight method of adjustment |
Family Cites Families (2)
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NL296607A (en) * | 1962-08-14 | 1900-01-01 | ||
GB1571281A (en) * | 1976-03-02 | 1980-07-09 | Fell E | Random dyeing of materials |
-
1979
- 1979-11-19 AU AU52938/79A patent/AU5293879A/en not_active Abandoned
- 1979-11-24 DE DE19792947488 patent/DE2947488A1/en not_active Withdrawn
- 1979-11-28 AT AT0753779A patent/ATA753779A/en not_active Application Discontinuation
- 1979-11-29 JP JP15371679A patent/JPS5580570A/en active Pending
- 1979-11-30 BR BR7907816A patent/BR7907816A/en unknown
- 1979-11-30 FR FR7929526A patent/FR2443289A1/en not_active Withdrawn
- 1979-12-03 IT IT27793/79A patent/IT1126481B/en active
- 1979-12-03 ES ES486539A patent/ES486539A1/en not_active Expired
- 1979-12-03 ES ES486551A patent/ES486551A1/en not_active Expired
- 1979-12-03 PH PH23351A patent/PH15036A/en unknown
- 1979-12-03 BE BE0/198387A patent/BE880387A/en unknown
- 1979-12-04 GB GB7941762A patent/GB2042375B/en not_active Expired
- 1979-12-04 CA CA341,140A patent/CA1134236A/en not_active Expired
Also Published As
Publication number | Publication date |
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AU5293879A (en) | 1982-05-13 |
PH15036A (en) | 1982-05-20 |
BE880387A (en) | 1980-06-03 |
ES486539A1 (en) | 1980-06-16 |
FR2443289A1 (en) | 1980-07-04 |
DE2947488A1 (en) | 1980-06-19 |
IT1126481B (en) | 1986-05-21 |
BR7907816A (en) | 1980-07-08 |
ATA753779A (en) | 1983-02-15 |
GB2042375B (en) | 1983-09-07 |
IT7927793A0 (en) | 1979-12-03 |
GB2042375A (en) | 1980-09-24 |
ES486551A1 (en) | 1980-06-16 |
JPS5580570A (en) | 1980-06-17 |
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