CA1113964A - Tris(amino-5 thia-3 pentyl) amine et son procede de preparation - Google Patents
Tris(amino-5 thia-3 pentyl) amine et son procede de preparationInfo
- Publication number
- CA1113964A CA1113964A CA319,396A CA319396A CA1113964A CA 1113964 A CA1113964 A CA 1113964A CA 319396 A CA319396 A CA 319396A CA 1113964 A CA1113964 A CA 1113964A
- Authority
- CA
- Canada
- Prior art keywords
- amine
- tris
- amino
- ethanethiol
- aziridine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000001412 amines Chemical class 0.000 title claims abstract description 22
- 239000007983 Tris buffer Substances 0.000 title claims abstract description 19
- -1 5-amino-3-thia pentyl Chemical group 0.000 title claims abstract description 8
- 238000000034 method Methods 0.000 title claims 4
- 238000002360 preparation method Methods 0.000 title description 2
- DNJIEGIFACGWOD-UHFFFAOYSA-N ethanethiol Chemical compound CCS DNJIEGIFACGWOD-UHFFFAOYSA-N 0.000 claims abstract description 21
- NOWKCMXCCJGMRR-UHFFFAOYSA-N Aziridine Chemical compound C1CN1 NOWKCMXCCJGMRR-UHFFFAOYSA-N 0.000 claims abstract description 10
- 238000004519 manufacturing process Methods 0.000 claims abstract description 3
- LENZDBCJOHFCAS-UHFFFAOYSA-N tris Chemical compound OCC(N)(CO)CO LENZDBCJOHFCAS-UHFFFAOYSA-N 0.000 claims abstract description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 15
- 238000006243 chemical reaction Methods 0.000 claims description 5
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 claims description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 4
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 claims description 4
- 239000002904 solvent Substances 0.000 claims description 2
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 claims 3
- 229960001701 chloroform Drugs 0.000 claims 1
- 239000000654 additive Substances 0.000 abstract description 2
- 239000010687 lubricating oil Substances 0.000 abstract description 2
- 239000000203 mixture Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 2
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 2
- 229910052794 bromium Inorganic materials 0.000 description 2
- UMGDCJDMYOKAJW-UHFFFAOYSA-N thiourea Chemical compound NC(N)=S UMGDCJDMYOKAJW-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- LNQCUTNLHUQZLR-VNPYQEQNSA-N Iridin Natural products O(C)c1c(O)c2C(=O)C(c3cc(OC)c(OC)c(O)c3)=COc2cc1O[C@H]1[C@@H](O)[C@@H](O)[C@H](O)[C@H](CO)O1 LNQCUTNLHUQZLR-VNPYQEQNSA-N 0.000 description 1
- 241000379208 Latris Species 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Natural products NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 108010047623 iridine Proteins 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
- C07C323/23—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton
- C07C323/24—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton
- C07C323/25—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being acyclic and saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Thiazole And Isothizaole Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Plural Heterocyclic Compounds (AREA)
- Lubricants (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR78.00624 | 1978-01-11 | ||
| FR7800624A FR2414499A1 (fr) | 1978-01-11 | 1978-01-11 | Tris(amino-5 thia-3 pentyl)amine, et son procede de preparation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1113964A true CA1113964A (fr) | 1981-12-08 |
Family
ID=9203296
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA319,396A Expired CA1113964A (fr) | 1978-01-11 | 1979-01-10 | Tris(amino-5 thia-3 pentyl) amine et son procede de preparation |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US4216170A (OSRAM) |
| EP (1) | EP0003189B1 (OSRAM) |
| JP (1) | JPS54117416A (OSRAM) |
| BR (1) | BR7900132A (OSRAM) |
| CA (1) | CA1113964A (OSRAM) |
| DE (1) | DE2960002D1 (OSRAM) |
| FR (1) | FR2414499A1 (OSRAM) |
| IT (1) | IT7947582A0 (OSRAM) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4272632A (en) * | 1979-10-01 | 1981-06-09 | Polaroid Corporation | Novel silver complexing agents |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2208095A (en) * | 1937-01-05 | 1940-07-16 | Ig Farbenindustrie Ag | Process of producing insoluble condensation products containing sulphur and nitrogen |
| US2177548A (en) * | 1937-07-28 | 1939-10-24 | Goodrich Co B F | Accelerator of vulcanization |
| US2304623A (en) * | 1939-08-03 | 1942-12-08 | Du Pont | Reaction of ethylenimines with thiols and product thereof |
| US2777858A (en) * | 1950-12-12 | 1957-01-15 | Geigy Chem Corp | Diamino compounds and process for the production thereof |
| US3260718A (en) * | 1963-01-31 | 1966-07-12 | Eastman Kodak Co | Mercaptoethylating agent: 2-mercaptoethyltrichloroacetate |
| US3362996A (en) * | 1965-06-14 | 1968-01-09 | Dow Chemical Co | N-(2-(2-aminoethylthio)ethyl)ethylene-diamine and method of preparation |
| US3725481A (en) * | 1971-03-03 | 1973-04-03 | Stauffer Chemical Co | Oligomer composition from alkyl amine and sulfur chlorides |
| US3862923A (en) * | 1971-03-03 | 1975-01-28 | Stauffer Chemical Co | Oligomer composition and products made therefrom |
-
1978
- 1978-01-11 FR FR7800624A patent/FR2414499A1/fr active Granted
-
1979
- 1979-01-04 EP EP79400003A patent/EP0003189B1/fr not_active Expired
- 1979-01-04 DE DE7979400003T patent/DE2960002D1/de not_active Expired
- 1979-01-09 US US06/002,239 patent/US4216170A/en not_active Expired - Lifetime
- 1979-01-10 CA CA319,396A patent/CA1113964A/fr not_active Expired
- 1979-01-10 BR BR7900132A patent/BR7900132A/pt unknown
- 1979-01-10 IT IT7947582A patent/IT7947582A0/it unknown
- 1979-01-11 JP JP104579A patent/JPS54117416A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| FR2414499A1 (fr) | 1979-08-10 |
| JPS5735913B2 (OSRAM) | 1982-07-31 |
| EP0003189A1 (fr) | 1979-07-25 |
| FR2414499B1 (OSRAM) | 1980-06-13 |
| EP0003189B1 (fr) | 1980-07-23 |
| DE2960002D1 (en) | 1980-11-13 |
| US4216170A (en) | 1980-08-05 |
| JPS54117416A (en) | 1979-09-12 |
| IT7947582A0 (it) | 1979-01-10 |
| BR7900132A (pt) | 1979-08-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry |