CA1102736A - Apparatus and process for the preparation of ammonia and heavy water - Google Patents
Apparatus and process for the preparation of ammonia and heavy waterInfo
- Publication number
- CA1102736A CA1102736A CA278,331A CA278331A CA1102736A CA 1102736 A CA1102736 A CA 1102736A CA 278331 A CA278331 A CA 278331A CA 1102736 A CA1102736 A CA 1102736A
- Authority
- CA
- Canada
- Prior art keywords
- water
- deuterium
- nitrogen
- hydrogen
- synthesis gas
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims abstract description 15
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 title claims description 88
- XLYOFNOQVPJJNP-ZSJDYOACSA-N Heavy water Chemical compound [2H]O[2H] XLYOFNOQVPJJNP-ZSJDYOACSA-N 0.000 title claims description 80
- 229910021529 ammonia Inorganic materials 0.000 title claims description 42
- 238000002360 preparation method Methods 0.000 title claims description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 104
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 80
- 230000015572 biosynthetic process Effects 0.000 claims abstract description 60
- 238000003786 synthesis reaction Methods 0.000 claims abstract description 60
- YZCKVEUIGOORGS-OUBTZVSYSA-N Deuterium Chemical compound [2H] YZCKVEUIGOORGS-OUBTZVSYSA-N 0.000 claims abstract description 57
- 229910052805 deuterium Inorganic materials 0.000 claims abstract description 57
- 239000007789 gas Substances 0.000 claims abstract description 48
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 46
- 239000001257 hydrogen Substances 0.000 claims abstract description 46
- 239000000203 mixture Substances 0.000 claims abstract description 46
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 45
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 40
- 230000002194 synthesizing effect Effects 0.000 claims abstract description 24
- 239000007788 liquid Substances 0.000 claims description 18
- 238000003860 storage Methods 0.000 claims description 15
- 238000004519 manufacturing process Methods 0.000 claims description 7
- 238000002485 combustion reaction Methods 0.000 claims description 6
- 230000005611 electricity Effects 0.000 abstract description 7
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 14
- 229910052786 argon Inorganic materials 0.000 description 7
- BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical compound NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 4
- 239000001301 oxygen Substances 0.000 description 4
- 229910052760 oxygen Inorganic materials 0.000 description 4
- 239000000567 combustion gas Substances 0.000 description 3
- 238000010276 construction Methods 0.000 description 2
- 238000010494 dissociation reaction Methods 0.000 description 2
- 230000005593 dissociations Effects 0.000 description 2
- 239000013505 freshwater Substances 0.000 description 2
- 238000005086 pumping Methods 0.000 description 2
- 241001058146 Erium Species 0.000 description 1
- 241001072332 Monia Species 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000008246 gaseous mixture Substances 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C1/00—Ammonia; Compounds thereof
- C01C1/02—Preparation, purification or separation of ammonia
- C01C1/04—Preparation of ammonia by synthesis in the gas phase
- C01C1/0405—Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst
- C01C1/0488—Processes integrated with preparations of other compounds, e.g. methanol, urea or with processes for power generation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B5/00—Water
- C01B5/02—Heavy water; Preparation by chemical reaction of hydrogen isotopes or their compounds, e.g. 4ND3 + 7O2 ---> 4NO2 + 6D2O, 2D2 + O2 ---> 2D2O
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Analytical Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Separation By Low-Temperature Treatments (AREA)
- Physical Water Treatments (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH602076A CH620176A5 (enrdf_load_stackoverflow) | 1976-05-13 | 1976-05-13 | |
| CH6020/76 | 1976-05-13 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1102736A true CA1102736A (en) | 1981-06-09 |
Family
ID=4302916
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA278,331A Expired CA1102736A (en) | 1976-05-13 | 1977-05-13 | Apparatus and process for the preparation of ammonia and heavy water |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US4213953A (enrdf_load_stackoverflow) |
| JP (1) | JPS534799A (enrdf_load_stackoverflow) |
| CA (1) | CA1102736A (enrdf_load_stackoverflow) |
| CH (1) | CH620176A5 (enrdf_load_stackoverflow) |
| DE (1) | DE2714967C3 (enrdf_load_stackoverflow) |
| FR (1) | FR2351054A1 (enrdf_load_stackoverflow) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH655081A5 (de) * | 1981-07-30 | 1986-03-27 | Sulzer Ag | Verfahren zur herstellung von mit deuterium angereichertem wasser bei der gewinnung von wasserstoff. |
| CH654489B (enrdf_load_stackoverflow) * | 1983-05-05 | 1986-02-28 | ||
| US20080311022A1 (en) * | 2007-06-14 | 2008-12-18 | Battelle Energy Alliance, Llc | Methods and apparatuses for ammonia production |
| CN103950952A (zh) * | 2014-05-20 | 2014-07-30 | 方治文 | 高纯氘氨的制备方法 |
| DE102016213360A1 (de) * | 2016-07-21 | 2018-01-25 | Thyssenkrupp Ag | Verfahren zur elektrochemischen Herstellung von Ammoniak |
| US11932951B2 (en) | 2017-10-11 | 2024-03-19 | Haldor Topsøe A/S | Method for generating synthesis gas for ammonia production |
| WO2024068198A1 (de) * | 2022-09-30 | 2024-04-04 | Siemens Energy Global GmbH & Co. KG | Anlage und verfahren zur erzeugung von ammoniak |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2180206A (en) * | 1937-12-21 | 1939-11-14 | Honnef Hermann | Wind-operated electrical power station |
| GB867736A (en) * | 1959-10-01 | 1961-05-10 | Norsk Hydro Elektrisk | Process for the concentration of heavy water |
| US3215503A (en) * | 1961-10-09 | 1965-11-02 | Zimmer Verfahrenstechnik | Apparatus for generating and storing inert gas |
| CA918382A (en) * | 1969-04-08 | 1973-01-09 | Her Majesty In Right Of Canada As Represented By Atomic Energy Of Canada Limited | Extraction of deuterium from hydrogen gas using amines in a bithermal process |
| US3705009A (en) * | 1970-06-12 | 1972-12-05 | Grace W R & Co | Heat recycling for ammonia preparation |
| US4112062A (en) * | 1971-03-22 | 1978-09-05 | Deuterium Corporation | Evaporation condensation systems |
-
1976
- 1976-05-13 CH CH602076A patent/CH620176A5/de not_active IP Right Cessation
- 1976-08-06 FR FR7624152A patent/FR2351054A1/fr active Granted
-
1977
- 1977-04-04 DE DE2714967A patent/DE2714967C3/de not_active Expired
- 1977-05-12 JP JP5482577A patent/JPS534799A/ja active Pending
- 1977-05-12 US US05/796,170 patent/US4213953A/en not_active Expired - Lifetime
- 1977-05-13 CA CA278,331A patent/CA1102736A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| FR2351054B1 (enrdf_load_stackoverflow) | 1978-11-03 |
| US4213953A (en) | 1980-07-22 |
| DE2714967C3 (de) | 1982-05-13 |
| DE2714967A1 (de) | 1977-11-17 |
| JPS534799A (en) | 1978-01-17 |
| FR2351054A1 (fr) | 1977-12-09 |
| DE2714967B2 (de) | 1981-08-13 |
| CH620176A5 (enrdf_load_stackoverflow) | 1980-11-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry |