BR9913250A - Processo para a coprodução de 6-aminocapronitrila e hexametilenodiamina partindo de adiponitrila - Google Patents
Processo para a coprodução de 6-aminocapronitrila e hexametilenodiamina partindo de adiponitrilaInfo
- Publication number
- BR9913250A BR9913250A BR9913250-8A BR9913250A BR9913250A BR 9913250 A BR9913250 A BR 9913250A BR 9913250 A BR9913250 A BR 9913250A BR 9913250 A BR9913250 A BR 9913250A
- Authority
- BR
- Brazil
- Prior art keywords
- adiponitrile
- aminocapronitrile
- hexamethylenediamine
- production
- stages
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/30—Preparation of carboxylic acid nitriles by reactions not involving the formation of cyano groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
- C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
"PROCESSO PARA A COPRODUçãO DE 6-AMINOCAPRONITRILA E HEXAMETILENODIAMINA PARTINDO DE ADIPONITRILA". A invenção refere-se a um processo para a preparação simultânea de 6-aminocapronitrila e hexametilenodiamina a partir de adiponitrila, que compreende os estágios de: a) hidrogenar adiponitrila na presença de um catalisador contendo um elemento do oitavo subgrupo como um componente cataliticamente ativo para obter uma mistura contendo 6-aminocapronitrila, hexametilenodiamina, adiponitrila e produtos de alta ebulição; b) separar por destilação hexametilenodiamina a partir da mistura contendo 6-aminocapronitrila, hexametilenodiamina, adiponitrila e produtos de alta ebulição e c1) separar por destilação 6-aminocapronitrila e subseq³entemente d1) separar por destilação adipronitrila ou c2) separar simultaneamente por destilação 6-aminocapronitrila e adiponitrila em frações separadas. O processo é caracterizado pelo fato de que a temperatura do fundo nos estágios d1) ou c2) está abaixo de 185°C.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19839338A DE19839338A1 (de) | 1998-08-28 | 1998-08-28 | Verbessertes Verfahren zur gleizeitigen Herstellung von 6-Aminocapronitril und Hexamethylendiamin |
PCT/EP1999/006011 WO2000012459A1 (de) | 1998-08-28 | 1999-08-17 | Verbessertes verfahren zur gleichzeitigen herstellung von 6-aminocapronitril und hexamethylendiamin |
Publications (1)
Publication Number | Publication Date |
---|---|
BR9913250A true BR9913250A (pt) | 2001-05-22 |
Family
ID=7879114
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR9913250-8A BR9913250A (pt) | 1998-08-28 | 1999-08-17 | Processo para a coprodução de 6-aminocapronitrila e hexametilenodiamina partindo de adiponitrila |
Country Status (16)
Country | Link |
---|---|
US (1) | US6462220B1 (pt) |
EP (1) | EP1107941B1 (pt) |
JP (1) | JP2002523482A (pt) |
KR (1) | KR20010073035A (pt) |
CN (1) | CN1238334C (pt) |
AR (1) | AR020283A1 (pt) |
AT (1) | ATE220658T1 (pt) |
AU (1) | AU5622399A (pt) |
BR (1) | BR9913250A (pt) |
CA (1) | CA2342177C (pt) |
DE (2) | DE19839338A1 (pt) |
ES (1) | ES2180323T3 (pt) |
ID (1) | ID30506A (pt) |
MY (1) | MY120584A (pt) |
TW (1) | TW521068B (pt) |
WO (1) | WO2000012459A1 (pt) |
Families Citing this family (29)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10010825A1 (de) * | 2000-03-08 | 2001-09-13 | Basf Ag | Verfahren zur Abtrennung eines Azepin-Derivats aus einer Mischung enthaltend ein Amin und ein Azepin-Derivat |
DE10029187A1 (de) * | 2000-06-19 | 2001-12-20 | Basf Ag | Verfahren zur Abtrennung von 6-Aminocapronitril aus Gemischen, die 6-Aminocapronitril, Adipodinitril und Hexamethylendiamin enthalten |
US6599398B1 (en) * | 2002-07-17 | 2003-07-29 | E. I. Du Pont De Nemours And Company | Recovery of adiponitrile from a mixture of adiponitrile, aminocapronitrile and hexamethylenediamine |
US6887352B2 (en) * | 2003-03-07 | 2005-05-03 | Invista North America S.A.R.L. | Distillative method for separating hexamethylenediamine from a mixture comprising hexamethylenediamine, 6-aminocapronitrile and tetrahydroazepine |
US6924394B2 (en) | 2003-06-05 | 2005-08-02 | Invista North America S.R.L. | Low pressure process for the manufacture of 2-(aminomethyl)-1-cyclopentylamine |
US7060819B2 (en) * | 2003-09-15 | 2006-06-13 | Invista North America S.A.R.L. | Process for producing hexamethylenediamine and aminocapronitrile from adiponitrile, wherein the hexamethylenediamine contains less than 100 ppm tetrahydroazepine |
US7468119B2 (en) | 2004-09-10 | 2008-12-23 | Invista North America S.A.R.L. | Separation of 6-aminocapronitrile and hexamethylenediamine from a mixture comprising hexamethylenediamine, 6-aminocapronitrile and tetrahydroazepine |
US7208632B2 (en) | 2004-09-10 | 2007-04-24 | Invista North America S.A R.L. | Separation of 6-aminocapronitrile and hexamethylenediamine from a mixture comprising hexamethylenediamine, 6-aminocapronitrile and tetrahydroazepine |
FR2902425B1 (fr) * | 2006-06-20 | 2008-07-18 | Rhodia Recherches & Tech | Procede de fabrication de diamines primaires |
CA2763177C (en) | 2009-06-13 | 2017-08-01 | Thomas R. Boussie | Production of glutaric acid and derivatives from carbohydrate-containing materials |
AU2010259925B2 (en) | 2009-06-13 | 2016-07-07 | Archer-Daniels-Midland Company | Production of adipic acid and derivatives from carbohydrate-containing materials |
US8669397B2 (en) | 2009-06-13 | 2014-03-11 | Rennovia, Inc. | Production of adipic acid and derivatives from carbohydrate-containing materials |
EP2440515B1 (en) | 2009-06-13 | 2018-08-15 | Archer-Daniels-Midland Company | Production of adipic acid and derivatives from carbohydrate-containing materials |
US9187403B2 (en) | 2009-07-31 | 2015-11-17 | Dow Global Technologies Llc | Process for separating one or more aliphatic diamines from reductive amination reaction solvents and impurities |
US8669393B2 (en) * | 2010-03-05 | 2014-03-11 | Rennovia, Inc. | Adipic acid compositions |
BR112012022136B1 (pt) | 2010-03-05 | 2018-10-09 | Rennovia Inc | composição de ácido adípico |
US9770705B2 (en) | 2010-06-11 | 2017-09-26 | Rennovia Inc. | Oxidation catalysts |
WO2013090031A2 (en) | 2011-12-14 | 2013-06-20 | Rennovia, Inc. | Water concentration reduction process |
US8981130B2 (en) | 2011-12-30 | 2015-03-17 | E I Du Pont De Nemours And Company | Process for the production of hexanediols |
WO2013101980A1 (en) | 2011-12-30 | 2013-07-04 | E. I. Du Pont De Nemours And Company | Process for preparing 1, 6-hexanediol |
WO2013101970A1 (en) | 2011-12-30 | 2013-07-04 | E. I. Du Pont De Nemours And Company | Production of 5-hydroxymethyl-2-furfural from levoglucosenone |
US8884035B2 (en) | 2011-12-30 | 2014-11-11 | E I Du Pont De Nemours And Company | Production of tetrahydrofuran-2, 5-dimethanol from isosorbide |
US8889912B2 (en) | 2011-12-30 | 2014-11-18 | E I Du Pont De Nemours And Company | Process for preparing 1,6-hexanediol |
US8865940B2 (en) | 2011-12-30 | 2014-10-21 | E I Du Pont De Nemours And Company | Process for preparing 1,6-hexanediol |
DE102012006946A1 (de) | 2012-04-10 | 2013-10-10 | Stratley Ag | Verfahren zur Herstellung von Caprolactam |
US8846985B2 (en) | 2012-04-27 | 2014-09-30 | E I Du Pont De Nemours And Company | Production of alpha, omega-diols |
US9018423B2 (en) | 2012-04-27 | 2015-04-28 | E I Du Pont De Nemours And Company | Production of alpha, omega-diols |
US8859826B2 (en) | 2012-04-27 | 2014-10-14 | E I Du Pont De Nemours And Company | Production of alpha, omega-diols |
US9822067B2 (en) | 2014-02-07 | 2017-11-21 | BASF SE (Ellwanger & Baier Patentanwälte) | Method for purifying adipodinitrile (ADN) |
Family Cites Families (22)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE848654C (de) | 1950-08-19 | 1952-09-08 | Basf Ag | Verfahren zur Herstellung von partiellen Hydrierungsprodukten des Adipinsaeuredinitrils |
DE954416C (de) | 1952-11-04 | 1956-12-20 | Basf Ag | Verfahren zur Herstellung von Aminonitrilen und Diaminen |
US2762835A (en) | 1953-03-12 | 1956-09-11 | Celanese Corp | Preparation of amino nitriles |
US3322815A (en) | 1964-07-27 | 1967-05-30 | Nat Distillers Chem Corp | Aminoalkanenitriles and process for preparing the same |
CA915707A (en) | 1969-07-11 | 1972-11-28 | J. Kershaw Bernard | Hydrogenation of adiponitrile |
US4601859A (en) | 1984-05-04 | 1986-07-22 | Allied Corporation | Selective hydrogenation of aliphatic dinitriles to omega-aminonitriles in ammonia with supported, finely dispersed rhodium-containing catalyst |
DE4235466A1 (de) | 1992-10-21 | 1994-04-28 | Bayer Ag | Verfahren zur Herstellung von (cyclo)aliphatischen Aminonitrilen |
DE4339648A1 (de) | 1993-11-20 | 1995-05-24 | Basf Ag | Verfahren zur Herstellung von Caprolactam |
FR2728259B1 (fr) | 1994-12-14 | 1997-03-14 | Rhone Poulenc Chimie | Procede d'hemihydrogenation de dinitriles en aminonitriles |
DE4446907A1 (de) | 1994-12-27 | 1996-07-04 | Basf Ag | Verfahren zur Herstellung eines Hydrierkatalysators |
DE4446893A1 (de) | 1994-12-27 | 1996-07-04 | Basf Ag | Verfahren zur Herstellung von aliphatischen alpha,omega-Aminonitrilen |
US5599962A (en) | 1995-01-31 | 1997-02-04 | E. I. Du Pont De Nemours And Company | Process for the preparation of ruthenium hydrogenation catalysts and products thereof |
US5559262A (en) | 1995-01-31 | 1996-09-24 | E. I. Du Pont De Nemours And Company | Process for the preparation of ruthenium complexes and their in situ use as hydrogenation catalysts |
FR2738757B1 (fr) | 1995-09-15 | 1997-10-31 | Rhone Poulenc Fibres | Nouveaux composes metalliques utilisables comme catalyseurs |
DE19548289A1 (de) * | 1995-12-22 | 1997-06-26 | Basf Ag | Verfahren zur gleichzeitigen Herstellung von Caprolactam und Hexamethylendiamin |
DE19614154C1 (de) | 1996-04-10 | 1997-09-25 | Basf Ag | Verfahren zur gleichzeitigen Herstellung von 6-Aminocapronitril und Hexamethylendiamin |
DE19636766A1 (de) * | 1996-09-10 | 1998-03-12 | Basf Ag | Verfahren zur gleichzeitigen Herstellung von 6-Aminocapronitril und Hexamethylendiamin |
DE19636765A1 (de) | 1996-09-10 | 1998-03-12 | Basf Ag | Verfahren zur gleichzeitigen Herstellung von 6-Aminocapronitril und Hexamethylendiamin |
DE19636767A1 (de) | 1996-09-10 | 1998-03-12 | Basf Ag | Verfahren zur Herstellung von aliphatischen alpha, omega-Aminonitrilen |
DE19704614A1 (de) | 1997-02-07 | 1998-08-13 | Basf Ag | Verfahren zur Abtrennnung eines Imins aus einer Mischung enthaltend ein Amin und ein Imin |
DE19704612A1 (de) | 1997-02-07 | 1998-08-13 | Basf Ag | Verfahren zur Gewinnung von Hexamethylendiamin aus Hexamethylendiamin enthaltenden Mischungen |
DE19832529A1 (de) | 1998-07-20 | 2000-01-27 | Basf Ag | Verbessertes Verfahren zur gleichzeitigen Herstellung von 6-Aminocapronitril und Hexamethylendiamin |
-
1998
- 1998-08-28 DE DE19839338A patent/DE19839338A1/de not_active Withdrawn
-
1999
- 1999-08-17 AT AT99942875T patent/ATE220658T1/de not_active IP Right Cessation
- 1999-08-17 ID IDW20010419A patent/ID30506A/id unknown
- 1999-08-17 CA CA002342177A patent/CA2342177C/en not_active Expired - Fee Related
- 1999-08-17 WO PCT/EP1999/006011 patent/WO2000012459A1/de not_active Application Discontinuation
- 1999-08-17 EP EP99942875A patent/EP1107941B1/de not_active Revoked
- 1999-08-17 KR KR1020017002523A patent/KR20010073035A/ko not_active Application Discontinuation
- 1999-08-17 CN CNB998103764A patent/CN1238334C/zh not_active Expired - Lifetime
- 1999-08-17 DE DE59902062T patent/DE59902062D1/de not_active Revoked
- 1999-08-17 AU AU56223/99A patent/AU5622399A/en not_active Abandoned
- 1999-08-17 ES ES99942875T patent/ES2180323T3/es not_active Expired - Lifetime
- 1999-08-17 JP JP2000567494A patent/JP2002523482A/ja not_active Withdrawn
- 1999-08-17 US US09/763,710 patent/US6462220B1/en not_active Expired - Lifetime
- 1999-08-17 BR BR9913250-8A patent/BR9913250A/pt not_active IP Right Cessation
- 1999-08-26 TW TW088114617A patent/TW521068B/zh not_active IP Right Cessation
- 1999-08-27 MY MYPI99003707A patent/MY120584A/en unknown
- 1999-08-27 AR ARP990104306A patent/AR020283A1/es unknown
Also Published As
Publication number | Publication date |
---|---|
CA2342177C (en) | 2008-12-23 |
AR020283A1 (es) | 2002-05-02 |
ID30506A (id) | 2001-12-13 |
US6462220B1 (en) | 2002-10-08 |
CN1238334C (zh) | 2006-01-25 |
CN1315935A (zh) | 2001-10-03 |
ES2180323T3 (es) | 2003-02-01 |
ATE220658T1 (de) | 2002-08-15 |
AU5622399A (en) | 2000-03-21 |
EP1107941A1 (de) | 2001-06-20 |
KR20010073035A (ko) | 2001-07-31 |
TW521068B (en) | 2003-02-21 |
DE59902062D1 (de) | 2002-08-22 |
DE19839338A1 (de) | 2000-03-02 |
CA2342177A1 (en) | 2000-03-09 |
EP1107941B1 (de) | 2002-07-17 |
JP2002523482A (ja) | 2002-07-30 |
WO2000012459A1 (de) | 2000-03-09 |
MY120584A (en) | 2005-11-30 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B08F | Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette] |
Free format text: REFERENTE A 9O ANUIDADE. |
|
B08K | Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette] |
Free format text: REFERENTE AO DESPACHO 8.6 DA RPI 1999 DE 28/04/2009. |