BR9713260A - Composições detergente - Google Patents

Composições detergente

Info

Publication number
BR9713260A
BR9713260A BR9713260-8A BR9713260A BR9713260A BR 9713260 A BR9713260 A BR 9713260A BR 9713260 A BR9713260 A BR 9713260A BR 9713260 A BR9713260 A BR 9713260A
Authority
BR
Brazil
Prior art keywords
detergent compositions
alkyl
alkenyl
mixture
surfactants
Prior art date
Application number
BR9713260-8A
Other languages
English (en)
Inventor
Robin Gibson Hall
Original Assignee
Procter & Gamble
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from GB9621791A external-priority patent/GB2318362A/en
Priority claimed from GB9621799A external-priority patent/GB2318363A/en
Priority claimed from GB9705841A external-priority patent/GB2323385A/en
Application filed by Procter & Gamble filed Critical Procter & Gamble
Publication of BR9713260A publication Critical patent/BR9713260A/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3723—Polyamines or polyalkyleneimines
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/28—Sulfonation products derived from fatty acids or their derivatives, e.g. esters, amides
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38—Cationic compounds
    • C11D1/62—Quaternary ammonium compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38—Cationic compounds
    • C11D1/65—Mixtures of anionic with cationic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/86—Mixtures of anionic, cationic, and non-ionic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/04—Water-soluble compounds
    • C11D3/10—Carbonates ; Bicarbonates
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/12—Water-insoluble compounds
    • C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246—Silicates, e.g. diatomaceous earth
    • C11D3/1253—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
    • C11D3/1273—Crystalline layered silicates of type NaMeSixO2x+1YH2O
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/12—Water-insoluble compounds
    • C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246—Silicates, e.g. diatomaceous earth
    • C11D3/128—Aluminium silicates, e.g. zeolites
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/39—Organic or inorganic per-compounds
    • C11D3/3902—Organic or inorganic per-compounds combined with specific additives
    • C11D3/3905—Bleach activators or bleach catalysts
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/39—Organic or inorganic per-compounds
    • C11D3/3942—Inorganic per-compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/39—Organic or inorganic per-compounds
    • C11D3/3945—Organic per-compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
    • C11D1/143—Sulfonic acid esters
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
    • C11D1/146—Sulfuric acid esters
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38—Cationic compounds
    • C11D1/52—Carboxylic amides, alkylolamides or imides or their condensation products with alkylene oxides
    • C11D1/525—Carboxylic amides (R1-CO-NR2R3), where R1, R2 or R3 contain two or more hydroxy groups per alkyl group, e.g. R3 being a reducing sugar rest
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/662—Carbohydrates or derivatives
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/72—Ethers of polyoxyalkylene glycols

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Detergent Compositions (AREA)

Abstract

Patente de Invenção: <B>"COMPOSIçõES DETERGENTES"<D>. A presente invenção se refere a composições detergentes ou seus componentes contendo uma enzim celulolítica e um ou mais surfatantes catiónicos de fórmula: R^ 1^R^ 2^R^ 3^R^ 4^N^ +^X^ -^, em que R^ 1^ é um grupo hidroxialquila com no máximo 6 átomos de carbono; cada R^ 2^ e R^ 3^ é independentemente selecionado dentre C~ 1-4~ alquila ou alcenila; R^ 4^ é uma C~ 5-9~ alquila ou alcenila; e X^ -^ é um contra-íon. O surfatante catiónico pode compreender uma mistura de surfatantes em que pelo menos 10% em peso da mistura têm R^ 4^ de C~ 9~ ou menos, ou em que R^ 4^ é um grupo C~ n~ alquila de mais de 8 a 11, e um grupo C~ (n-2)~ alquila, respectivamente.
BR9713260-8A 1996-10-18 1997-10-02 Composições detergente BR9713260A (pt)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
GB9621791A GB2318362A (en) 1996-10-18 1996-10-18 Detergent compositions
GB9621799A GB2318363A (en) 1996-10-18 1996-10-18 Detergent compositions
GB9705841A GB2323385A (en) 1997-03-20 1997-03-20 Detergent compositions
PCT/US1997/017855 WO1998017758A1 (en) 1996-10-18 1997-10-02 Detergent compositions

Publications (1)

Publication Number Publication Date
BR9713260A true BR9713260A (pt) 2001-06-19

Family

ID=27268547

Family Applications (1)

Application Number Title Priority Date Filing Date
BR9713260-8A BR9713260A (pt) 1996-10-18 1997-10-02 Composições detergente

Country Status (10)

Country Link
US (1) US6103685A (pt)
EP (1) EP0934379B1 (pt)
AR (1) AR010000A1 (pt)
AT (1) ATE213765T1 (pt)
BR (1) BR9713260A (pt)
CA (1) CA2268672C (pt)
DE (1) DE69710749T2 (pt)
ES (1) ES2176708T3 (pt)
MX (1) MX206678B (pt)
WO (1) WO1998017758A1 (pt)

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE69841985D1 (de) * 1998-07-31 2010-12-16 Procter & Gamble vERWENDUNG VON OBERFLÄCHENAKTIVEN SUBSTANZEN ZUR SCUM-REDUZIERUNG IN GEWEBEPFLEGEMITTEL
US6830593B1 (en) 1998-08-03 2004-12-14 The Procter & Gamble Company Fabric care compositions
DE69828162T2 (de) * 1998-08-03 2005-12-22 The Procter & Gamble Company, Cincinnati Gewebepflegmittel
MY120271A (en) * 1999-05-19 2005-09-30 Colgate Palmolive Co Laundry detergent composition containing high level of protease enzyme
US6627591B2 (en) * 1999-12-17 2003-09-30 Unilever Home & Personal Care Usa Division Of Conopco, Inc. Dye fixing composition
GB0009029D0 (en) 2000-04-12 2000-05-31 Unilever Plc Laundry wash compositions
GB0009877D0 (en) 2000-04-20 2000-06-07 Unilever Plc Granular detergent component and process for its preparation
US6660712B2 (en) * 2000-06-02 2003-12-09 Dale Elbert Van Sickle Stabilization of amido acids with antioxidants
US20030050211A1 (en) * 2000-12-14 2003-03-13 Unilever Home & Personal Care Usa, Division Of Conopco, Inc. Enzymatic detergent compositions
ATE361356T1 (de) * 2000-12-14 2007-05-15 Unilever Nv Enzymatische waschmittelzusammensetzungen
JP4443929B2 (ja) * 2002-01-07 2010-03-31 チバ ホールディング インコーポレーテッド 染料固着剤を含む微粒子組成物
US20070212256A1 (en) * 2002-04-05 2007-09-13 Helton Danny O Mold remediation system and method
US7557076B2 (en) * 2002-06-06 2009-07-07 The Procter & Gamble Company Organic catalyst with enhanced enzyme compatibility
ES2596325T3 (es) 2002-12-04 2017-01-05 Clariant International Ltd Composición de amonio cuaternario
DE10303130A1 (de) * 2003-01-28 2004-07-29 Clariant Gmbh Wässrige Flüssigwaschmittel-Dispersionen
EP1621605B1 (en) * 2003-05-07 2008-06-25 Ciba Holding Inc. Bleach composition and bleaching detergent composition
US7381337B2 (en) * 2003-07-17 2008-06-03 Lessard Environmental, Inc. Gel-based remedial additive for remediation of environmental media and method of use
DE102004018051A1 (de) * 2004-04-08 2005-11-10 Clariant Gmbh Wasch- und Reinigungsmittel enthaltend Farbfixiermittel und Soil Release Polymere
WO2005116179A1 (de) * 2004-05-17 2005-12-08 Henkel Kommanditgesellschaft Auf Aktien Waschmittel mit gegebenenfalls in situ erzeugtem bleichverstärkendem übergangsmetallkomplex
DE102005042054A1 (de) * 2005-09-02 2007-03-08 Henkel Kgaa Parfümhaltige Teilchen mit verbesserten Dufteigenschaften
GB0523634D0 (en) * 2005-11-21 2005-12-28 Reckitt Benckiser Nv Solid cleaning formulations
US7596974B2 (en) 2006-06-19 2009-10-06 S.C. Johnson & Son, Inc. Instant stain removing device, formulation and absorbent means
PL2242830T5 (pl) * 2008-01-04 2021-08-16 The Procter & Gamble Company Kompozycje zawierające enzym i środek barwiący tkaninę
WO2013191647A1 (en) * 2012-06-18 2013-12-27 Laundry-Maid Pte Ltd Solid detergent composition
WO2014139577A1 (en) * 2013-03-14 2014-09-18 Ecolab Usa Inc. Laundry detergent composition for low temperature washing
WO2014166514A1 (en) * 2013-04-08 2014-10-16 Ecolab Usa Inc. Laundry detergent composition for low temperature washing
MX2019004601A (es) * 2016-10-18 2019-06-17 Sterilex LLC Polvo para el tratamiento de superficies activado por humedad ambiental.

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0199403B1 (en) * 1985-04-15 1993-12-15 The Procter & Gamble Company Stable liquid detergent compositions
GB9013784D0 (en) * 1990-06-20 1990-08-08 Unilever Plc Process and composition for treating fabrics
US5458809A (en) * 1992-07-15 1995-10-17 The Procter & Gamble Co. Surfactant-containing dye transfer inhibiting compositions
BR9407130A (pt) * 1993-07-19 1996-09-10 Procter & Gamble Composições detergentes que inibem transferência de corante na lavagem
DE69608546T2 (de) * 1995-03-03 2001-01-18 Procter & Gamble Waschmittelzusammensetzung enthaltend farbstofffixiermittel und cellulase
US5830843A (en) * 1996-01-31 1998-11-03 The Procter & Gamble Company Fabric care compositions including dispersible polyolefin and method for using same

Also Published As

Publication number Publication date
ES2176708T3 (es) 2002-12-01
EP0934379B1 (en) 2002-02-27
EP0934379A4 (en) 1999-12-22
MX9903685A (es) 1999-09-30
MX206678B (es) 2002-02-11
CA2268672C (en) 2004-02-17
ATE213765T1 (de) 2002-03-15
EP0934379A1 (en) 1999-08-11
CA2268672A1 (en) 1998-04-30
AR010000A1 (es) 2000-05-17
US6103685A (en) 2000-08-15
DE69710749D1 (de) 2002-04-04
DE69710749T2 (de) 2002-11-14
WO1998017758A1 (en) 1998-04-30

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Legal Events

Date Code Title Description
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 02/10/1997, OBSERVADAS AS CONDICOES LEGAIS.

B21F Lapse acc. art. 78, item iv - on non-payment of the annual fees in time

Free format text: REFERENTE A 16A ANUIDADE.

B24J Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12)

Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2258 DE 15-04-2014 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013.