BR9708427A - Processo para incluir um enchimento particulado fino em papel de seda utilizando um polieletrólito aniônico - Google Patents
Processo para incluir um enchimento particulado fino em papel de seda utilizando um polieletrólito aniônicoInfo
- Publication number
- BR9708427A BR9708427A BR9708427A BR9708427A BR9708427A BR 9708427 A BR9708427 A BR 9708427A BR 9708427 A BR9708427 A BR 9708427A BR 9708427 A BR9708427 A BR 9708427A BR 9708427 A BR9708427 A BR 9708427A
- Authority
- BR
- Brazil
- Prior art keywords
- tissue paper
- fine particulate
- anionic polyelectrolyte
- particulate filling
- tissue
- Prior art date
Links
Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21F—PAPER-MAKING MACHINES; METHODS OF PRODUCING PAPER THEREON
- D21F11/00—Processes for making continuous lengths of paper, or of cardboard, or of wet web for fibre board production, on paper-making machines
- D21F11/14—Making cellulose wadding, filter or blotting paper
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H23/00—Processes or apparatus for adding material to the pulp or to the paper
- D21H23/02—Processes or apparatus for adding material to the pulp or to the paper characterised by the manner in which substances are added
- D21H23/04—Addition to the pulp; After-treatment of added substances in the pulp
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/20—Macromolecular organic compounds
- D21H17/21—Macromolecular organic compounds of natural origin; Derivatives thereof
- D21H17/24—Polysaccharides
- D21H17/28—Starch
- D21H17/29—Starch cationic
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/20—Macromolecular organic compounds
- D21H17/33—Synthetic macromolecular compounds
- D21H17/34—Synthetic macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D21H17/37—Polymers of unsaturated acids or derivatives thereof, e.g. polyacrylates
- D21H17/375—Poly(meth)acrylamide
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/20—Macromolecular organic compounds
- D21H17/33—Synthetic macromolecular compounds
- D21H17/34—Synthetic macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D21H17/41—Synthetic macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds containing ionic groups
- D21H17/42—Synthetic macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds containing ionic groups anionic
- D21H17/43—Carboxyl groups or derivatives thereof
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/63—Inorganic compounds
- D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
- D21H17/68—Water-insoluble compounds, e.g. fillers, pigments siliceous, e.g. clays
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/63—Inorganic compounds
- D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
- D21H17/69—Water-insoluble compounds, e.g. fillers, pigments modified, e.g. by association with other compositions prior to incorporation in the pulp or paper
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/50—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by form
- D21H21/52—Additives of definite length or shape
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
- D21H27/30—Multi-ply
- D21H27/38—Multi-ply at least one of the sheets having a fibrous composition differing from that of other sheets
Landscapes
- Paper (AREA)
- Materials For Medical Uses (AREA)
- Sanitary Thin Papers (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/627,855 US5700352A (en) | 1996-04-03 | 1996-04-03 | Process for including a fine particulate filler into tissue paper using an anionic polyelectrolyte |
PCT/US1997/006018 WO1997037081A1 (en) | 1996-04-03 | 1997-04-03 | A process for including a fine particulate filler into tissue paper using an anionic polyelectrolyte |
Publications (1)
Publication Number | Publication Date |
---|---|
BR9708427A true BR9708427A (pt) | 1999-08-03 |
Family
ID=24516425
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR9708427A BR9708427A (pt) | 1996-04-03 | 1997-04-03 | Processo para incluir um enchimento particulado fino em papel de seda utilizando um polieletrólito aniônico |
Country Status (10)
Country | Link |
---|---|
US (1) | US5700352A (pt) |
EP (1) | EP0891444B1 (pt) |
JP (1) | JP3194233B2 (pt) |
KR (1) | KR100315335B1 (pt) |
AT (1) | ATE269442T1 (pt) |
AU (1) | AU2455097A (pt) |
BR (1) | BR9708427A (pt) |
CA (1) | CA2250842A1 (pt) |
DE (1) | DE69729561D1 (pt) |
WO (1) | WO1997037081A1 (pt) |
Families Citing this family (33)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5830317A (en) * | 1995-04-07 | 1998-11-03 | The Procter & Gamble Company | Soft tissue paper with biased surface properties containing fine particulate fillers |
US5672249A (en) * | 1996-04-03 | 1997-09-30 | The Procter & Gamble Company | Process for including a fine particulate filler into tissue paper using starch |
AU2708799A (en) * | 1998-03-23 | 1999-10-18 | Pulp And Paper Research Institute Of Canada | Method for producing pulp and paper with calcium carbonate filler |
CA2676732C (en) | 1998-06-12 | 2014-04-15 | Georgia-Pacific Consumer Products Lp | Method of making a paper web having a high internal void volume of secondary fibers and a product made by the process |
CO5150202A1 (es) | 1998-12-31 | 2002-04-29 | Kimberly Clark Co | Composicion de tisu facial y metodo para usarla para el secuestro de irritantes de la piel de la secrecion nasal |
US6241850B1 (en) | 1999-06-16 | 2001-06-05 | The Procter & Gamble Company | Soft tissue product exhibiting improved lint resistance and process for making |
US6383336B1 (en) | 1999-12-14 | 2002-05-07 | Kimberly-Clark Worldwide, Inc. | Strong, soft non-compressively dried tissue products containing particulate fillers |
US6358365B1 (en) | 1999-12-14 | 2002-03-19 | Hercules Incorporated | Metal silicates, cellulose products, and processes thereof |
US6425981B1 (en) * | 1999-12-16 | 2002-07-30 | Metso Paper Karlstad Aktiebolg (Ab) | Apparatus and associated method for drying a wet web of paper |
US6464830B1 (en) * | 2000-11-07 | 2002-10-15 | Kimberly-Clark Worldwide, Inc. | Method for forming a multi-layered paper web |
US6837970B2 (en) * | 2001-12-18 | 2005-01-04 | Kimberly-Clark Worldwide, Inc. | Wood pulp fiber morphology modifications through thermal drying |
US6939443B2 (en) * | 2002-06-19 | 2005-09-06 | Lanxess Corporation | Anionic functional promoter and charge control agent |
US20040203308A1 (en) * | 2003-04-09 | 2004-10-14 | Ko Young Chan | Process for making absorbent material |
US7976679B2 (en) | 2004-12-02 | 2011-07-12 | The Procter & Gamble Company | Fibrous structures comprising a low surface energy additive |
US7208429B2 (en) * | 2004-12-02 | 2007-04-24 | The Procter + Gamble Company | Fibrous structures comprising a nonoparticle additive |
US7459179B2 (en) * | 2004-12-02 | 2008-12-02 | The Procter & Gamble Company | Process for making a fibrous structure comprising an additive |
US20060260509A1 (en) * | 2005-04-22 | 2006-11-23 | Evers Glenn R | Compositions for enhanced paper brightness and whiteness |
US20080163995A1 (en) * | 2005-04-27 | 2008-07-10 | Joy Kogias | Paper Product Containing Mineral Material Which Stimulates Micro-Organism Activity In Naturally Occurring Environmental Conditions |
US20070133346A1 (en) * | 2005-12-14 | 2007-06-14 | Tommy Jacobson | Mixing of chemicals into a thin stock pipe |
US20090162642A1 (en) * | 2006-01-26 | 2009-06-25 | Katsumasa Ono | Paper containing preggregated filler and process for producing the same |
JP4287438B2 (ja) * | 2006-01-31 | 2009-07-01 | 大王製紙株式会社 | 薬液含有薄葉紙 |
EP1918456A1 (en) * | 2006-10-31 | 2008-05-07 | M-real Oyj | Method of producing a fibrous web containing fillers |
US20080178489A1 (en) * | 2007-01-15 | 2008-07-31 | Roger Dionne | Shaver saver |
US8172983B2 (en) * | 2007-09-12 | 2012-05-08 | Nalco Company | Controllable filler prefloculation using a dual polymer system |
PT2093261E (pt) | 2007-11-02 | 2013-11-26 | Omya Int Ag | Utilização de um carbonato de cálcio reagido à superfície em papel de tecido, o processo para preparar um produto de papel de tecido de macieza melhorada e resultando em produtos de papel de tecido de macieza melhorada |
US20090275699A1 (en) * | 2008-05-05 | 2009-11-05 | Mingfu Zhang | Starch containing formaldehyde-free thermoset binders for fiber products |
CA2736512C (en) * | 2008-09-22 | 2017-11-14 | Hercules Incorporated | Copolymer blend compositions for use to increase paper filler content |
US8758567B2 (en) * | 2009-06-03 | 2014-06-24 | Hercules Incorporated | Cationic wet strength resin modified pigments in barrier coating applications |
US8916012B2 (en) | 2010-12-28 | 2014-12-23 | Kimberly-Clark Worldwide, Inc. | Method of making substrates comprising frothed benefit agents |
PT106170A (pt) * | 2012-02-20 | 2013-08-20 | Fapajal Fabrica De Papel Do Tojal S A | Processo de fixação de cargas de carbonato de cálcio em papéis leves crepados (tissu) sem impacto negativo nas características do papel |
US10618248B2 (en) * | 2017-06-19 | 2020-04-14 | Johns Manville | Multilayer facer manufacturing system |
CN109606789B (zh) * | 2018-12-29 | 2024-06-28 | 成都三可实业有限公司 | 一种用于条形软糖包装的转向机构 |
CN115646647B (zh) * | 2022-11-21 | 2023-03-10 | 太原陆森矿业机械有限公司 | 一种适用于湿式重介混合物的磁选机 |
Family Cites Families (48)
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US2216143A (en) * | 1936-05-11 | 1940-10-01 | Cons Water Power & Paper Co | Process of coating paper |
BE661981A (pt) * | 1964-04-03 | |||
US3301746A (en) * | 1964-04-13 | 1967-01-31 | Procter & Gamble | Process for forming absorbent paper by imprinting a fabric knuckle pattern thereon prior to drying and paper thereof |
US3823062A (en) * | 1972-02-28 | 1974-07-09 | Int Paper Co | Twin-wire papermaking employing stabilized stock flow and water filled seal(drainage)boxes |
US3821068A (en) * | 1972-10-17 | 1974-06-28 | Scott Paper Co | Soft,absorbent,fibrous,sheet material formed by avoiding mechanical compression of the fiber furnish until the sheet is at least 80% dry |
US3974025A (en) * | 1974-04-01 | 1976-08-10 | The Procter & Gamble Company | Absorbent paper having imprinted thereon a semi-twill, fabric knuckle pattern prior to final drying |
GB1505641A (en) * | 1974-04-19 | 1978-03-30 | Grace W R & Co | Process of preparing a filler composition for paper |
US4166001A (en) * | 1974-06-21 | 1979-08-28 | Kimberly-Clark Corporation | Multiple layer formation process for creped tissue |
GB1497280A (en) * | 1974-12-10 | 1978-01-05 | Ass Portland Cement | Agglomerating suspended particulate material in aqueous systems |
US3994771A (en) * | 1975-05-30 | 1976-11-30 | The Procter & Gamble Company | Process for forming a layered paper web having improved bulk, tactile impression and absorbency and paper thereof |
US4308092A (en) * | 1975-12-15 | 1981-12-29 | Rohm And Haas Company | Creping paper using cationic water soluble addition |
US4406737A (en) * | 1976-05-07 | 1983-09-27 | Rohm And Haas Company | Creping paper using cationic water soluble addition polymer |
SE7708115L (sv) * | 1976-07-14 | 1978-01-15 | English Clays Lovering Pochin | Forfarande for framstellning av papper eller papp |
IE47019B1 (en) * | 1977-07-12 | 1983-11-30 | Blue Circle Ind Ltd | Producing dispersions of polymeric material and preflocculated fillers for use in papermaking |
US4191609A (en) * | 1979-03-09 | 1980-03-04 | The Procter & Gamble Company | Soft absorbent imprinted paper sheet and method of manufacture thereof |
US4300981A (en) * | 1979-11-13 | 1981-11-17 | The Procter & Gamble Company | Layered paper having a soft and smooth velutinous surface, and method of making such paper |
FR2492425A1 (fr) * | 1980-10-21 | 1982-04-23 | Gascogne Papeteries | Procede de preparation par des techniques papetieres d'un materiau en feuille avec une retention sur machine amelioree, materiau en feuille ainsi obtenu et son application notamment dans le domaine de l'impression-ecriture, de l'emballage et des revetements |
US4637859A (en) * | 1983-08-23 | 1987-01-20 | The Procter & Gamble Company | Tissue paper |
US4529480A (en) * | 1983-08-23 | 1985-07-16 | The Procter & Gamble Company | Tissue paper |
SE453206B (sv) * | 1983-10-21 | 1988-01-18 | Valmet Paper Machinery Inc | Hygienpappersbana, forfarande for framstellning derav samt anvendning av expanderbara mikrosferer av termoplast vid framstellning av hygienpappersbana |
FR2578870B1 (fr) * | 1985-03-18 | 1988-07-29 | Gascogne Papeteries | Procede de preparation d'une feuille fibreuse par voie papetiere pour ameliorer la retention et en particulier l'opacite. |
US4795530A (en) * | 1985-11-05 | 1989-01-03 | Kimberly-Clark Corporation | Process for making soft, strong cellulosic sheet and products made thereby |
GB8531558D0 (en) * | 1985-12-21 | 1986-02-05 | Wiggins Teape Group Ltd | Loaded paper |
GB8602121D0 (en) * | 1986-01-29 | 1986-03-05 | Allied Colloids Ltd | Paper & paper board |
JPH0670317B2 (ja) * | 1986-02-07 | 1994-09-07 | 三菱製紙株式会社 | 填料内添紙の製造方法 |
GB8621680D0 (en) * | 1986-09-09 | 1986-10-15 | Du Pont | Filler compositions |
US4772332A (en) * | 1987-04-21 | 1988-09-20 | Engelhard Corporation | Use of mixture of high molecular weight sulfonates as auxiliary dispersant for structured kaolins |
US4927498A (en) * | 1988-01-13 | 1990-05-22 | E. I. Du Pont De Nemours And Company | Retention and drainage aid for papermaking |
US5266622A (en) * | 1988-05-05 | 1993-11-30 | Bayer Aktiengesellschaft | Aqueous dispersions containing a synergistic dispersant combination |
SE461156B (sv) * | 1988-05-25 | 1990-01-15 | Eka Nobel Ab | Saett foer framstaellning av papper varvid formning och avvattning aeger rum i naervaro av en aluminiumfoerening, ett katjoniskt retentionsmedel och en polymer kiselsyra |
US4940513A (en) * | 1988-12-05 | 1990-07-10 | The Procter & Gamble Company | Process for preparing soft tissue paper treated with noncationic surfactant |
US4959125A (en) * | 1988-12-05 | 1990-09-25 | The Procter & Gamble Company | Soft tissue paper containing noncationic surfactant |
US5185206A (en) * | 1988-09-16 | 1993-02-09 | E. I. Du Pont De Nemours And Company | Polysilicate microgels as retention/drainage aids in papermaking |
US4954220A (en) * | 1988-09-16 | 1990-09-04 | E. I. Du Pont De Nemours And Company | Polysilicate microgels as retention/drainage aids in papermaking |
US5164046A (en) * | 1989-01-19 | 1992-11-17 | The Procter & Gamble Company | Method for making soft tissue paper using polysiloxane compound |
US4978396A (en) * | 1989-05-12 | 1990-12-18 | Kerr-Mcgee Chemical Corporation | Process for preparing high solids slurries |
US5068276A (en) * | 1989-12-29 | 1991-11-26 | E.C.C. America Inc. | Chemically aggregated mineral pigments |
US5164045A (en) * | 1991-03-04 | 1992-11-17 | James River Corporation Of Virginia | Soft, high bulk foam-formed stratified tissue and method for making same |
US5415740A (en) * | 1991-04-25 | 1995-05-16 | Betz Paperchem, Inc. | Method for improving retention and drainage characteristics in alkaline papermaking |
US5228954A (en) * | 1991-05-28 | 1993-07-20 | The Procter & Gamble Cellulose Company | Cellulose pulps of selected morphology for improved paper strength potential |
US5227023A (en) * | 1991-08-26 | 1993-07-13 | James River Corporation Of Virginia | Multi-layer papers and tissues |
US5221435A (en) * | 1991-09-27 | 1993-06-22 | Nalco Chemical Company | Papermaking process |
US5405499A (en) * | 1993-06-24 | 1995-04-11 | The Procter & Gamble Company | Cellulose pulps having improved softness potential |
IL113721A (en) * | 1994-05-20 | 1999-04-11 | Minerals Tech Inc | Dual surface treated filler material method for its preparation and use in papermaking |
JP3647909B2 (ja) * | 1994-08-24 | 2005-05-18 | リンテック株式会社 | 化粧用脂取り紙 |
JP3512481B2 (ja) * | 1994-08-25 | 2004-03-29 | 泉製紙株式会社 | 洗浄装置付き水洗トイレ用トイレットペーパー |
US5487813A (en) * | 1994-12-02 | 1996-01-30 | The Procter & Gamble Company | Strong and soft creped tissue paper and process for making the same by use of biodegradable crepe facilitating compositions |
US5611890A (en) * | 1995-04-07 | 1997-03-18 | The Proctor & Gamble Company | Tissue paper containing a fine particulate filler |
-
1996
- 1996-04-03 US US08/627,855 patent/US5700352A/en not_active Expired - Fee Related
-
1997
- 1997-04-03 WO PCT/US1997/006018 patent/WO1997037081A1/en active IP Right Grant
- 1997-04-03 AT AT97920329T patent/ATE269442T1/de not_active IP Right Cessation
- 1997-04-03 BR BR9708427A patent/BR9708427A/pt not_active Application Discontinuation
- 1997-04-03 KR KR1019980707929A patent/KR100315335B1/ko not_active IP Right Cessation
- 1997-04-03 AU AU24550/97A patent/AU2455097A/en not_active Abandoned
- 1997-04-03 EP EP97920329A patent/EP0891444B1/en not_active Expired - Lifetime
- 1997-04-03 DE DE69729561T patent/DE69729561D1/de not_active Expired - Lifetime
- 1997-04-03 CA CA002250842A patent/CA2250842A1/en not_active Abandoned
- 1997-04-03 JP JP53562797A patent/JP3194233B2/ja not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
EP0891444B1 (en) | 2004-06-16 |
JP3194233B2 (ja) | 2001-07-30 |
ATE269442T1 (de) | 2004-07-15 |
KR20000005242A (ko) | 2000-01-25 |
JP2000507656A (ja) | 2000-06-20 |
KR100315335B1 (ko) | 2002-04-06 |
DE69729561D1 (de) | 2004-07-22 |
EP0891444A1 (en) | 1999-01-20 |
US5700352A (en) | 1997-12-23 |
AU2455097A (en) | 1997-10-22 |
WO1997037081A1 (en) | 1997-10-09 |
CA2250842A1 (en) | 1997-10-09 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PC | Transfer |
Free format text: INSTITUTE OF PAPER SCIENCE AND TECHNOLOGY (US) |
|
B06A | Patent application procedure suspended [chapter 6.1 patent gazette] | ||
B11B | Dismissal acc. art. 36, par 1 of ipl - no reply within 90 days to fullfil the necessary requirements |