BR112013021461A2 - processo para a determinação do teor de sulfeto de hidrogênio em óleos bruto e residual - Google Patents

processo para a determinação do teor de sulfeto de hidrogênio em óleos bruto e residual

Info

Publication number
BR112013021461A2
BR112013021461A2 BR112013021461A BR112013021461A BR112013021461A2 BR 112013021461 A2 BR112013021461 A2 BR 112013021461A2 BR 112013021461 A BR112013021461 A BR 112013021461A BR 112013021461 A BR112013021461 A BR 112013021461A BR 112013021461 A2 BR112013021461 A2 BR 112013021461A2
Authority
BR
Brazil
Prior art keywords
crude
hydrogen sulfide
sulfur
oils
residual oils
Prior art date
Application number
BR112013021461A
Other languages
English (en)
Inventor
Dominko Adrin
Matthias Krull
Michael Brauchle
Michael Feustel
Original Assignee
Clariant Finance Bvi Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=45688423&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=BR112013021461(A2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Priority claimed from DE201110012445 external-priority patent/DE102011012445A1/de
Priority claimed from DE201110113943 external-priority patent/DE102011113943A1/de
Application filed by Clariant Finance Bvi Ltd filed Critical Clariant Finance Bvi Ltd
Publication of BR112013021461A2 publication Critical patent/BR112013021461A2/pt

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/26—Oils; Viscous liquids; Paints; Inks
    • G01N33/28—Oils, i.e. hydrocarbon liquids
    • G01N33/2835—Specific substances contained in the oils or fuels
    • G01N33/287—Sulfur content
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G21/00—Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents
    • C10G21/06—Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents characterised by the solvent used
    • C10G21/12—Organic compounds only
    • C10G21/14—Hydrocarbons
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/22—Fuels; Explosives
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/26—Oils; Viscous liquids; Paints; Inks
    • G01N33/28—Oils, i.e. hydrocarbon liquids
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1033—Oil well production fluids
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1037—Hydrocarbon fractions
    • C10G2300/1048—Middle distillates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/201—Impurities
    • C10G2300/202—Heteroatoms content, i.e. S, N, O, P
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/201—Impurities
    • C10G2300/207—Acid gases, e.g. H2S, COS, SO2, HCN
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/40—Characteristics of the process deviating from typical ways of processing
    • C10G2300/4006—Temperature
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/40—Characteristics of the process deviating from typical ways of processing
    • C10G2300/44—Solvents
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/18—Sulfur containing
    • Y10T436/182—Organic or sulfhydryl containing [e.g., mercaptan, hydrogen, sulfide, etc.]
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/18—Sulfur containing
    • Y10T436/182—Organic or sulfhydryl containing [e.g., mercaptan, hydrogen, sulfide, etc.]
    • Y10T436/184—Only hydrogen sulfide

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Medicinal Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Food Science & Technology (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Organic Chemistry (AREA)
  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Abstract

processo para a determinação do teor de sulfeto de hidrogênio em óleos bruto e residual a presente invenção refere-se a um processo para determinar o teor de h~ 2~s que se ajusta durante o armazenamento sob calor de óleos bruto e residual contendo enxofre, bem como de destilados de óleos minerais contendo óleos brutos e/ou residuais contendo enxofre, no qual uma amostra do óleo mineral contendo enxofre é dissolvida em um solvente ou mistura de solventes que ferve acima de 200°c e a solução do óleo mineral contendo enxofre é percorrida a temperaturas acima de 80ºc por um gás portador e a quantidade de sulfeto de hidrogênio transportada com o gás portador é quantitativamente analisada.
BR112013021461A 2011-02-25 2012-02-14 processo para a determinação do teor de sulfeto de hidrogênio em óleos bruto e residual BR112013021461A2 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE201110012445 DE102011012445A1 (de) 2011-02-25 2011-02-25 Verfahren zur Bestimmung des Gehalts an Schwefelwasserstoff in Roh- und Rückstandsölen
DE201110113943 DE102011113943A1 (de) 2011-09-20 2011-09-20 Verfahren zur Bestimmung des Gehalts an Schwefelwasserstoff in Roh- und Rückstandsölen
PCT/EP2012/000651 WO2012113519A1 (de) 2011-02-25 2012-02-14 Verfahren zur bestimmung des gehalts an schwefelwasserstoff in roh- und rückstandsölen

Publications (1)

Publication Number Publication Date
BR112013021461A2 true BR112013021461A2 (pt) 2016-10-25

Family

ID=45688423

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112013021461A BR112013021461A2 (pt) 2011-02-25 2012-02-14 processo para a determinação do teor de sulfeto de hidrogênio em óleos bruto e residual

Country Status (8)

Country Link
US (1) US9029160B2 (pt)
EP (1) EP2678674B2 (pt)
JP (1) JP2014507660A (pt)
KR (1) KR20140006813A (pt)
BR (1) BR112013021461A2 (pt)
CA (1) CA2828127C (pt)
EA (1) EA023063B1 (pt)
WO (1) WO2012113519A1 (pt)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8914857B2 (en) * 2012-11-21 2014-12-16 Wal-Mart Stores, Inc. Security bypass environment for circumventing a security application in a computing environment
EP3704480B1 (en) * 2017-04-04 2021-03-03 Total Se Screening method for assessing the h2s release capacity of a sulfur containing sample
US10564142B2 (en) * 2017-09-29 2020-02-18 Saudi Arabian Oil Company Quantifying organic and inorganic sulfur components
CN109765275B (zh) * 2019-01-17 2024-01-09 中国石油化工股份有限公司 一种室外快速在线检测原油硫化氢含量的方法、装置
CN113514602A (zh) * 2021-03-25 2021-10-19 长沙矿冶研究院有限责任公司 一种含硫矿物中亚铁的测定方法
US11821823B2 (en) * 2021-08-02 2023-11-21 Saudi Arabian Oil Company Creating a hydrogen sulfide crude oil reference standard

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Publication number Priority date Publication date Assignee Title
US3660035A (en) * 1969-03-26 1972-05-02 Robin S Marsh Method and apparatus for determination of hydrogen sulfide in hydrogen sulfide petroleum products
FR2581759B1 (fr) * 1985-05-07 1987-06-26 Elf Aquitaine Procede de preparation en continu des echantillons de gaz dissous dans un liquide pour l'analyse de ces gaz
FR2607255B1 (fr) 1986-11-25 1989-09-29 Inst Francais Du Petrole Procede et dispositif de determination de la quantite d'au moins un element choisi parmi le carbone, l'hydrogene, le soufre et l'azote d'au moins deux fractions d'un echantillon de matiere organique
US5379654A (en) 1993-04-14 1995-01-10 Intevep, S.A. Method and apparatus for the analysis of gas in a medium
RU2155960C2 (ru) 1998-11-23 2000-09-10 Предприятие "Астраханьгазпром" РАО "Газпром" Способ определения содержания сероводорода в мазуте
RU2285917C1 (ru) 2005-07-20 2006-10-20 Открытое акционерное общество "Татнефть" им. В.Д. Шашина Способ определения содержания сероводорода и легких меркаптанов в нефти, нефтепродуктах и газовом конденсате
US20080165361A1 (en) * 2007-01-05 2008-07-10 Kauffman Robert E Method of analyzing sulfur content in fuels
CN101737040A (zh) 2008-11-18 2010-06-16 长春吉大·小天鹅仪器有限公司 石油钻探现场硫化氢检测装置及检测方法
JP5323743B2 (ja) 2010-02-19 2013-10-23 Ｊｘ日鉱日石エネルギー株式会社 硫化水素の検出方法

Also Published As

Publication number Publication date
EP2678674B2 (de) 2019-07-10
EP2678674A1 (de) 2014-01-01
EA201300948A1 (ru) 2014-01-30
US9029160B2 (en) 2015-05-12
CA2828127A1 (en) 2012-08-30
KR20140006813A (ko) 2014-01-16
US20140004611A1 (en) 2014-01-02
JP2014507660A (ja) 2014-03-27
WO2012113519A1 (de) 2012-08-30
EA023063B1 (ru) 2016-04-29
EP2678674B1 (de) 2016-12-14
CA2828127C (en) 2019-09-10

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Legal Events

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B08F Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette]
B08K Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette]