BR0318682A - process for producing glycine enriched with improved flow sodium chloride crystals - Google Patents
process for producing glycine enriched with improved flow sodium chloride crystalsInfo
- Publication number
- BR0318682A BR0318682A BRPI0318682-2A BR0318682A BR0318682A BR 0318682 A BR0318682 A BR 0318682A BR 0318682 A BR0318682 A BR 0318682A BR 0318682 A BR0318682 A BR 0318682A
- Authority
- BR
- Brazil
- Prior art keywords
- glycine
- brine
- enriched
- crystals
- sodium chloride
- Prior art date
Links
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 title abstract 18
- 239000004471 Glycine Substances 0.000 title abstract 9
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 title abstract 7
- 239000011780 sodium chloride Substances 0.000 title abstract 5
- 239000013078 crystal Substances 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 4
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 abstract 9
- 239000012267 brine Substances 0.000 abstract 7
- 235000002639 sodium chloride Nutrition 0.000 abstract 5
- QNRATNLHPGXHMA-XZHTYLCXSA-N (r)-(6-ethoxyquinolin-4-yl)-[(2s,4s,5r)-5-ethyl-1-azabicyclo[2.2.2]octan-2-yl]methanol;hydrochloride Chemical compound Cl.C([C@H]([C@H](C1)CC)C2)CN1[C@@H]2[C@H](O)C1=CC=NC2=CC=C(OCC)C=C21 QNRATNLHPGXHMA-XZHTYLCXSA-N 0.000 abstract 3
- 238000001704 evaporation Methods 0.000 abstract 2
- 230000008020 evaporation Effects 0.000 abstract 2
- 239000012452 mother liquor Substances 0.000 abstract 2
- 125000004122 cyclic group Chemical group 0.000 abstract 1
- 150000002333 glycines Chemical class 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 238000005406 washing Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D3/00—Halides of sodium, potassium or alkali metals in general
- C01D3/04—Chlorides
- C01D3/06—Preparation by working up brines; seawater or spent lyes
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D3/00—Halides of sodium, potassium or alkali metals in general
- C01D3/26—Preventing the absorption of moisture or caking of the crystals
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Seasonings (AREA)
- Food Preservation Except Freezing, Refrigeration, And Drying (AREA)
Abstract
"PROCESSO PARA PRODUçãO DE GLICINA ENRIQUECIDA COM CRISTAIS DE CLORETO DE SóDIO COM FLUXO MELHORADO". A presente invenção se relaciona a um processo cíclico simples, económico e eficiente para produção de glicina enriquecida no formato dodecaédrico rómbico, fluxo livre de sal comum da salmoura, dito processo compreendendo etapas de adição de glicina de concentração variando entre 10 á 25% para a salmoura saturada, evaporação da salmoura saturada contendo glicina para obter cristais tendo alto índice de glicina, com mother líquor, lavagem dos cristais com salmoura saturada para obter sal comum enriquecido com glicina no formato dodecaédrico rómbico tendo glicina índice variando entre 05 à 1.0% e salmoura lavada, combinando o mother liquor e a salmoura lavada para obter a salmoura resultante, sujeitando a salmoura resultante à evaporação solar, e repetindo as etapas de (iii) à (v) para obter sal comum enriquecido com glicina no formato dodecaédrico rómbico da salmoura com concentração de glicina variando entre 0.5 à 1.0%."Process for Producing Enriched Glycine with Enhanced Flow Sodium Chloride Crystals". The present invention relates to a simple, economical and efficient cyclic process for producing rhombic dodecahedral-shaped glycine-enriched common salt free salt brine, said process comprising glycine addition steps of concentration ranging from 10 to 25% for saturated brine, evaporation of saturated glycine containing brine to obtain high glycine index crystals, with mother liquor, washing of crystals with saturated brine to obtain rhombic dodecahedral glycine-enriched common salt having glycine index ranging from 05 to 1.0% and brine washed, combining the mother liquor and the washed brine to obtain the resulting brine, subjecting the resulting brine to solar evaporation, and repeating steps (iii) to (v) to obtain the glycine-enriched common salt in the rhombic dodecahedral format of brine with glycine concentration ranging from 0.5 to 1.0%.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PCT/IB2003/006237 WO2005066075A1 (en) | 2003-12-24 | 2003-12-24 | Process for production of glycine enriched sodium chloride crystals with improved flow |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| BR0318682A true BR0318682A (en) | 2006-12-12 |
| BR0318682B1 BR0318682B1 (en) | 2013-07-16 |
Family
ID=34746632
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BRPI0318682-2B1A BR0318682B1 (en) | 2003-12-24 | 2003-12-24 | process for producing improved flow glycine enriched naci crystals. |
Country Status (9)
| Country | Link |
|---|---|
| JP (1) | JP4805677B2 (en) |
| CN (1) | CN1972869B (en) |
| BR (1) | BR0318682B1 (en) |
| CA (1) | CA2551051C (en) |
| DE (1) | DE10394353B4 (en) |
| GB (1) | GB2440138B (en) |
| IL (1) | IL176542A (en) |
| MX (1) | MXPA06007390A (en) |
| WO (1) | WO2005066075A1 (en) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU2008346088B2 (en) | 2008-01-07 | 2013-09-19 | Council Of Scientific & Industrial Research | Free flowing 100 - 500 mm size spherical crystals of common salt and process for preparation thereof |
| GB0807919D0 (en) | 2008-05-01 | 2008-06-04 | Moorlodge Biotech Ventures Ltd | |
| WO2010002712A2 (en) | 2008-06-30 | 2010-01-07 | 3M Innovative Properties Company | Method of crystallization |
| MX350838B (en) | 2011-02-11 | 2017-09-18 | Grain Proc Corporation * | Salt composition. |
| CN103373735A (en) * | 2012-04-27 | 2013-10-30 | 北京美华盛工程技术有限公司 | Method for producing food-grade sodium chloride and potassium chloride salt with anti-blocking property |
| WO2014167185A1 (en) * | 2013-04-10 | 2014-10-16 | Smart Salt Oy | Food salt product |
| US10881123B2 (en) * | 2017-10-27 | 2021-01-05 | Frito-Lay North America, Inc. | Crystal morphology for sodium reduction |
| CN111302362B (en) * | 2020-04-03 | 2021-05-07 | 天津科技大学 | Large-particle spherical salt and preparation method thereof |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3856922A (en) * | 1973-11-06 | 1974-12-24 | R Bragdon | Process for preparing substantially non-caking sodium chloride |
| JPH1142064A (en) * | 1997-07-28 | 1999-02-16 | Akou Kasei Kk | Common salt composition having high mineral content |
| FI110474B (en) * | 1999-01-27 | 2003-02-14 | Modulpo Salts Oy | Nutritional physiological salt product, its use and process for its preparation |
| JP2001061417A (en) * | 1999-08-25 | 2001-03-13 | Sanei Gen Ffi Inc | Powdery substance-containing composition |
| KR100427012B1 (en) * | 2000-01-12 | 2004-04-30 | 오성은 | a manufacturing process of a pure salt |
| WO2002013631A1 (en) * | 2000-08-14 | 2002-02-21 | Unilever N.V. | Granulation process |
| JP4246407B2 (en) * | 2001-04-27 | 2009-04-02 | キッセイ薬品工業株式会社 | Liquid seasoning |
-
2003
- 2003-12-24 BR BRPI0318682-2B1A patent/BR0318682B1/en active IP Right Grant
- 2003-12-24 CA CA2551051A patent/CA2551051C/en not_active Expired - Fee Related
- 2003-12-24 CN CN2003801109228A patent/CN1972869B/en not_active Expired - Fee Related
- 2003-12-24 WO PCT/IB2003/006237 patent/WO2005066075A1/en active Application Filing
- 2003-12-24 DE DE10394353.6T patent/DE10394353B4/en not_active Expired - Fee Related
- 2003-12-24 GB GB0612958A patent/GB2440138B/en not_active Expired - Fee Related
- 2003-12-24 JP JP2005513078A patent/JP4805677B2/en not_active Expired - Fee Related
- 2003-12-24 MX MXPA06007390A patent/MXPA06007390A/en active IP Right Grant
-
2006
- 2006-06-25 IL IL176542A patent/IL176542A/en not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| JP4805677B2 (en) | 2011-11-02 |
| GB2440138B (en) | 2009-04-08 |
| IL176542A (en) | 2010-12-30 |
| AU2003288642A1 (en) | 2005-08-12 |
| JP2007527834A (en) | 2007-10-04 |
| GB2440138A (en) | 2008-01-23 |
| CN1972869A (en) | 2007-05-30 |
| BR0318682B1 (en) | 2013-07-16 |
| CN1972869B (en) | 2011-03-30 |
| DE10394353T5 (en) | 2006-11-23 |
| WO2005066075A1 (en) | 2005-07-21 |
| DE10394353B4 (en) | 2014-09-11 |
| IL176542A0 (en) | 2006-10-05 |
| CA2551051C (en) | 2011-08-02 |
| CA2551051A1 (en) | 2005-07-21 |
| MXPA06007390A (en) | 2007-03-23 |
| GB0612958D0 (en) | 2006-08-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
| B06A | Patent application procedure suspended [chapter 6.1 patent gazette] | ||
| B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
| B09X | Republication of the decision to grant [chapter 9.1.3 patent gazette] | ||
| B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 24/12/2003, OBSERVADAS AS CONDICOES LEGAIS. |