BE780228A - Purifying polyoxyalkylene ether polyols - by mixing with solvents, centrifuging, and recovering polyol - Google Patents

Purifying polyoxyalkylene ether polyols - by mixing with solvents, centrifuging, and recovering polyol

Info

Publication number
BE780228A
BE780228A BE780228A BE780228A BE780228A BE 780228 A BE780228 A BE 780228A BE 780228 A BE780228 A BE 780228A BE 780228 A BE780228 A BE 780228A BE 780228 A BE780228 A BE 780228A
Authority
BE
Belgium
Prior art keywords
polyol
water
soln
solvent
polyoxyalkylene ether
Prior art date
Application number
BE780228A
Other languages
French (fr)
Original Assignee
Marles Kuhlmann Wyandotte
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US00126343A external-priority patent/US3823145A/en
Application filed by Marles Kuhlmann Wyandotte filed Critical Marles Kuhlmann Wyandotte
Publication of BE780228A publication Critical patent/BE780228A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/30Post-polymerisation treatment, e.g. recovery, purification, drying

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Polyethers (AREA)

Abstract

Polyoxyalkylene ether polyols contg. water soluble impurities derived from residual catalyst, and having a mol. wt. >=300 and a content of ethylene oxide units 65%. are purified esp. for polyurethane prepn. by (a) forming a mixt. of water, the polyol, and a solvent which has a density considerably different from that of water, dissolves the polyol and is inert relative to the polyol and water, to give a soln. of the polyol in the solvent, which is immiscible with water, (b) centrifugally sepg. the polyol soln. from the water to give streams of water contg. the impurities, and polyol soln. and (c) recovering the polyol by elimination of the solvent. Simple, efficient process giving polyols with a low impurity content e.g. =2 ppm without use of solid absorbants. Loss of polyol minimised.
BE780228A 1971-03-19 1972-03-03 Purifying polyoxyalkylene ether polyols - by mixing with solvents, centrifuging, and recovering polyol BE780228A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US00126343A US3823145A (en) 1968-07-26 1971-03-19 Removal of impurities from polyols

Publications (1)

Publication Number Publication Date
BE780228A true BE780228A (en) 1972-09-04

Family

ID=22424314

Family Applications (1)

Application Number Title Priority Date Filing Date
BE780228A BE780228A (en) 1971-03-19 1972-03-03 Purifying polyoxyalkylene ether polyols - by mixing with solvents, centrifuging, and recovering polyol

Country Status (2)

Country Link
BE (1) BE780228A (en)
IT (1) IT957525B (en)

Also Published As

Publication number Publication date
IT957525B (en) 1973-10-20

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Legal Events

Date Code Title Description
RE Patent lapsed

Owner name: PCUK PRODUITS CHIMIQUES UGINE KUHLMANN

Effective date: 19900331