BE639027A - - Google Patents

Info

Publication number

BE639027A

BE639027A BE639027DA BE639027A BE 639027 A BE639027 A BE 639027A BE 639027D A BE639027D A BE 639027DA BE 639027 A BE639027 A BE 639027A

Authority

BE

Belgium

Prior art keywords

cyclohexylamine

boric

acid

biborate

amount

Prior art date

Links

• Espacenet
• Global Dossier
• Discuss

• PAFZNILMFXTMIY-UHFFFAOYSA-N cyclohexylamine Chemical compound NC1CCCCC1 PAFZNILMFXTMIY-UHFFFAOYSA-N 0.000 claims description 28
• 229910011255 B2O3 Inorganic materials 0.000 claims description 12
• JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 claims description 12
• KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims description 7
• 239000004327 boric acid Substances 0.000 claims description 7
• 239000000203 mixture Substances 0.000 claims description 7
• VGTPKLINSHNZRD-UHFFFAOYSA-N oxoborinic acid Chemical compound OB=O VGTPKLINSHNZRD-UHFFFAOYSA-N 0.000 claims description 7
• 238000000034 method Methods 0.000 claims description 5
• 239000007788 liquid Substances 0.000 claims description 4
• 239000012429 reaction media Substances 0.000 claims description 4
• 150000001338 aliphatic hydrocarbons Chemical class 0.000 claims description 2
• 150000004945 aromatic hydrocarbons Chemical class 0.000 claims description 2
• 150000008280 chlorinated hydrocarbons Chemical class 0.000 claims description 2
• 238000004519 manufacturing process Methods 0.000 claims description 2
• 239000000047 product Substances 0.000 description 10
• 238000006243 chemical reaction Methods 0.000 description 9
• RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 8
• 229910001868 water Inorganic materials 0.000 description 8
• 150000001412 amines Chemical class 0.000 description 7
• 239000002253 acid Substances 0.000 description 5
• 239000003208 petroleum Substances 0.000 description 5
• 238000003756 stirring Methods 0.000 description 5
• 239000000725 suspension Substances 0.000 description 5
• 238000010992 reflux Methods 0.000 description 4
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
• YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
• 150000001639 boron compounds Chemical class 0.000 description 3
• 239000011541 reaction mixture Substances 0.000 description 3
• 238000009835 boiling Methods 0.000 description 2
• 239000003153 chemical reaction reagent Substances 0.000 description 2
• 238000004821 distillation Methods 0.000 description 2
• 238000010438 heat treatment Methods 0.000 description 2
• 239000007787 solid Substances 0.000 description 2
• 239000002904 solvent Substances 0.000 description 2
• 239000003039 volatile agent Substances 0.000 description 2
• PQMFVUNERGGBPG-UHFFFAOYSA-N (6-bromopyridin-2-yl)hydrazine Chemical class NNC1=CC=CC(Br)=N1 PQMFVUNERGGBPG-UHFFFAOYSA-N 0.000 description 1
• XHRCFGDFESIFRG-UHFFFAOYSA-N 2-chloro-n-ethyl-n-[(2-methylphenyl)methyl]ethanamine Chemical compound ClCCN(CC)CC1=CC=CC=C1C XHRCFGDFESIFRG-UHFFFAOYSA-N 0.000 description 1
• 125000000217 alkyl group Chemical group 0.000 description 1
• 125000004429 atom Chemical group 0.000 description 1
• CREXVNNSNOKDHW-UHFFFAOYSA-N azaniumylideneazanide Chemical group N[N] CREXVNNSNOKDHW-UHFFFAOYSA-N 0.000 description 1
• 150000001642 boronic acid derivatives Chemical class 0.000 description 1
• 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
• 238000009833 condensation Methods 0.000 description 1
• 230000005494 condensation Effects 0.000 description 1
• 239000000470 constituent Substances 0.000 description 1
• 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 description 1
• 239000003085 diluting agent Substances 0.000 description 1
• 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
• 239000000706 filtrate Substances 0.000 description 1
• 238000001914 filtration Methods 0.000 description 1
• 229940083124 ganglion-blocking antiadrenergic secondary and tertiary amines Drugs 0.000 description 1
• 230000002503 metabolic effect Effects 0.000 description 1
• 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
• 238000002156 mixing Methods 0.000 description 1
• 238000002360 preparation method Methods 0.000 description 1
• 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
• 238000000926 separation method Methods 0.000 description 1