BE365032A - - Google Patents
Info
- Publication number
- BE365032A BE365032A BE365032DA BE365032A BE 365032 A BE365032 A BE 365032A BE 365032D A BE365032D A BE 365032DA BE 365032 A BE365032 A BE 365032A
- Authority
- BE
- Belgium
- Prior art keywords
- alcohol
- phosphorus oxychloride
- parts
- mixture
- main patent
- Prior art date
Links
- XHXFXVLFKHQFAL-UHFFFAOYSA-N phosphoryl trichloride Chemical compound ClP(Cl)(Cl)=O XHXFXVLFKHQFAL-UHFFFAOYSA-N 0.000 claims description 16
- 238000000034 method Methods 0.000 claims description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 9
- 150000003138 primary alcohols Chemical class 0.000 claims description 4
- 239000007795 chemical reaction product Substances 0.000 claims description 2
- 150000002989 phenols Chemical class 0.000 claims description 2
- 150000002148 esters Chemical class 0.000 description 10
- 235000019441 ethanol Nutrition 0.000 description 10
- 239000000203 mixture Substances 0.000 description 9
- 230000007935 neutral effect Effects 0.000 description 8
- 238000006243 chemical reaction Methods 0.000 description 7
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- PHTQWCKDNZKARW-UHFFFAOYSA-N isoamylol Chemical compound CC(C)CCO PHTQWCKDNZKARW-UHFFFAOYSA-N 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 3
- 150000001298 alcohols Chemical class 0.000 description 3
- -1 alkyl phosphates Chemical class 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 229910019142 PO4 Inorganic materials 0.000 description 2
- 150000002170 ethers Chemical class 0.000 description 2
- 238000004508 fractional distillation Methods 0.000 description 2
- 235000021317 phosphate Nutrition 0.000 description 2
- 235000011121 sodium hydroxide Nutrition 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000032050 esterification Effects 0.000 description 1
- 238000005886 esterification reaction Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/08—Esters of oxyacids of phosphorus
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BE365032A true BE365032A (en:Method) |
Family
ID=37395
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BE365032D BE365032A (en:Method) |
Country Status (1)
| Country | Link |
|---|---|
| BE (1) | BE365032A (en:Method) |
-
0
- BE BE365032D patent/BE365032A/fr unknown
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| BE365032A (en:Method) | ||
| US2723280A (en) | 1-methyl-17-ethinyl-estradiol | |
| US2415444A (en) | Process of producing tetraethyl lead | |
| US2387203A (en) | Method of making beryllium fluoride | |
| Henriksen et al. | Dihydroxy phenylselenonium p-toluenesulfonate; Preparation and use in the recycling of selenium reagents | |
| BE365033A (en:Method) | ||
| CH401989A (fr) | Procédé de préparation de la phosphocréatine | |
| SU1341174A1 (ru) | Способ получени 2-замещенных или 2,2-замещенных 1,3-пропандиолов | |
| BE445904A (en:Method) | ||
| US2277781A (en) | Process of making and recovering tetraalkyl lead | |
| JPH0317823B2 (en:Method) | ||
| BE540017A (en:Method) | ||
| US2042630A (en) | Manufacture of 6-bromo-2,4-dini-traniline | |
| CH335525A (fr) | Procédé de préparation de la B, B-diphényl-propyl-éthylamine | |
| CN118420548A (zh) | 一种2,4-二甲氧基-5-溴嘧啶的制备方法 | |
| BE549645A (en:Method) | ||
| JPH0314012B2 (en:Method) | ||
| FR2495139A1 (fr) | Procede pour la preparation de derives de cyclopropane | |
| CH276548A (fr) | Procédé pour la fabrication de la semi-carbazone de la 5-nitro-2-furaldéhyde. | |
| JPS5976039A (ja) | （ｓ）−２，３−ジアセチル−１−ベンジルグリセロ−ル | |
| BE444578A (fr) | Procédé pour l'obtention de succédanés pour des épices poivrées | |
| BE624397A (en:Method) | ||
| CH134680A (fr) | Procédé de préparation d'alliages liquides de sodium et de potassium. | |
| JPS5821939B2 (ja) | ロジンアリルエステルの製法 | |
| CH278404A (fr) | Procédé de préparation de la vitamine A. |