AU783237B2 - Storage stable pesticide formulations containing azadirachtin - Google Patents
Storage stable pesticide formulations containing azadirachtin Download PDFInfo
- Publication number
- AU783237B2 AU783237B2 AU53553/00A AU5355300A AU783237B2 AU 783237 B2 AU783237 B2 AU 783237B2 AU 53553/00 A AU53553/00 A AU 53553/00A AU 5355300 A AU5355300 A AU 5355300A AU 783237 B2 AU783237 B2 AU 783237B2
- Authority
- AU
- Australia
- Prior art keywords
- formulation
- azadirachtin
- weight
- vegetable oil
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- FTNJWQUOZFUQQJ-IRYYUVNJSA-N azadirachtin A Natural products C([C@@H]([C@]1(C=CO[C@H]1O1)O)[C@]2(C)O3)[C@H]1[C@]23[C@]1(C)[C@H](O)[C@H](OC[C@@]2([C@@H](C[C@@H]3OC(=O)C(\C)=C/C)OC(C)=O)C(=O)OC)[C@@H]2[C@]32CO[C@@](C(=O)OC)(O)[C@@H]12 FTNJWQUOZFUQQJ-IRYYUVNJSA-N 0.000 title claims description 97
- FTNJWQUOZFUQQJ-NDAWSKJSSA-N azadirachtin A Chemical compound C([C@@H]([C@]1(C=CO[C@H]1O1)O)[C@]2(C)O3)[C@H]1[C@]23[C@]1(C)[C@H](O)[C@H](OC[C@@]2([C@@H](C[C@@H]3OC(=O)C(\C)=C\C)OC(C)=O)C(=O)OC)[C@@H]2[C@]32CO[C@@](C(=O)OC)(O)[C@@H]12 FTNJWQUOZFUQQJ-NDAWSKJSSA-N 0.000 title claims description 97
- VEHPJKVTJQSSKL-UHFFFAOYSA-N azadirachtin Natural products O1C2(C)C(C3(C=COC3O3)O)CC3C21C1(C)C(O)C(OCC2(OC(C)=O)C(CC3OC(=O)C(C)=CC)OC(C)=O)C2C32COC(C(=O)OC)(O)C12 VEHPJKVTJQSSKL-UHFFFAOYSA-N 0.000 title claims description 91
- 239000005878 Azadirachtin Substances 0.000 title claims description 84
- 239000003090 pesticide formulation Substances 0.000 title claims description 38
- 238000003860 storage Methods 0.000 title claims description 28
- 239000000203 mixture Substances 0.000 claims description 119
- 238000009472 formulation Methods 0.000 claims description 113
- 235000013500 Melia azadirachta Nutrition 0.000 claims description 30
- 239000000284 extract Substances 0.000 claims description 30
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 29
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 28
- 239000004094 surface-active agent Substances 0.000 claims description 24
- 239000008158 vegetable oil Substances 0.000 claims description 24
- 239000003960 organic solvent Substances 0.000 claims description 12
- 239000002736 nonionic surfactant Substances 0.000 claims description 8
- 229940082880 azadirachta indica flower extract Drugs 0.000 claims description 6
- 244000237986 Melia azadirachta Species 0.000 claims description 5
- 241000207961 Sesamum Species 0.000 claims description 5
- 235000003434 Sesamum indicum Nutrition 0.000 claims description 5
- KAJFOBKSQVMLSY-UHFFFAOYSA-N azadirachtin B Natural products COC(=O)C1(O)OCC23C(O)CC(OC(=O)C(=CC)C)C4(COC(C(O)C(C)(C12)C56OC5(C)C7CC6OC8OC=CC78O)C34)C(=O)OC KAJFOBKSQVMLSY-UHFFFAOYSA-N 0.000 claims description 4
- FTNJWQUOZFUQQJ-UZTPERQESA-N azadirachtin B Chemical compound C([C@@H]([C@]1(C=CO[C@H]1O1)O)[C@]2(C)O3)[C@H]1[C@]23[C@]1(C)[C@H](O)[C@H](OC[C@@]2([C@@H](C[C@H]3OC(=O)C(\C)=C\C)OC(C)=O)C(=O)OC)[C@@H]2[C@]32CO[C@@](C(=O)OC)(O)[C@@H]12 FTNJWQUOZFUQQJ-UZTPERQESA-N 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 3
- -1 polyoxyethylene trioleate Polymers 0.000 claims description 3
- JNYAEWCLZODPBN-JGWLITMVSA-N (2r,3r,4s)-2-[(1r)-1,2-dihydroxyethyl]oxolane-3,4-diol Chemical group OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O JNYAEWCLZODPBN-JGWLITMVSA-N 0.000 claims 2
- 235000009917 Crataegus X brevipes Nutrition 0.000 claims 1
- 235000013204 Crataegus X haemacarpa Nutrition 0.000 claims 1
- 235000009685 Crataegus X maligna Nutrition 0.000 claims 1
- 235000009444 Crataegus X rubrocarnea Nutrition 0.000 claims 1
- 235000009486 Crataegus bullatus Nutrition 0.000 claims 1
- 235000017181 Crataegus chrysocarpa Nutrition 0.000 claims 1
- 235000009682 Crataegus limnophila Nutrition 0.000 claims 1
- 235000004423 Crataegus monogyna Nutrition 0.000 claims 1
- 240000000171 Crataegus monogyna Species 0.000 claims 1
- 235000002313 Crataegus paludosa Nutrition 0.000 claims 1
- 235000009840 Crataegus x incaedua Nutrition 0.000 claims 1
- 235000021588 free fatty acids Nutrition 0.000 claims 1
- 240000005343 Azadirachta indica Species 0.000 description 25
- 235000011803 sesame oil Nutrition 0.000 description 20
- 239000008159 sesame oil Substances 0.000 description 20
- 230000015556 catabolic process Effects 0.000 description 11
- 238000006731 degradation reaction Methods 0.000 description 11
- 238000000034 method Methods 0.000 description 11
- 239000002904 solvent Substances 0.000 description 11
- 239000012141 concentrate Substances 0.000 description 9
- 239000007787 solid Substances 0.000 description 9
- 238000011282 treatment Methods 0.000 description 9
- 241000985245 Spodoptera litura Species 0.000 description 8
- 239000007788 liquid Substances 0.000 description 8
- 150000001533 azadirachtins Chemical class 0.000 description 7
- 230000000694 effects Effects 0.000 description 7
- 229920000136 polysorbate Polymers 0.000 description 7
- 239000004480 active ingredient Substances 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- 239000003921 oil Substances 0.000 description 5
- 235000019198 oils Nutrition 0.000 description 5
- 239000000843 powder Substances 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 241000238631 Hexapoda Species 0.000 description 4
- 239000004615 ingredient Substances 0.000 description 4
- NHOIBRJOQAYBJT-IMGVWCFESA-N nimbin Chemical compound C=1([C@@H]2C[C@H]3O[C@H]4[C@](C3=C2C)(C)[C@@H]([C@]2(C(=O)C=C[C@](C)([C@@H]2[C@H]4OC(C)=O)C(=O)OC)C)CC(=O)OC)C=COC=1 NHOIBRJOQAYBJT-IMGVWCFESA-N 0.000 description 4
- ZQIYJHBQRBBBRZ-UHFFFAOYSA-N nimbin Natural products COC(=O)CC1C2C(C(OC(=O)C)C3OC4CC(C(=C4C13C)C)c5cocc5)C(C)(C=CC2=O)C(=O)OC ZQIYJHBQRBBBRZ-UHFFFAOYSA-N 0.000 description 4
- CJHBVBNPNXOWBA-REXVOHEDSA-N salannin Chemical compound C=1([C@@H]2C[C@H]3O[C@H]4[C@](C3=C2C)(C)[C@@H]([C@]2(C)[C@@H]3[C@]([C@@H](C[C@@H]2OC(=O)C(\C)=C\C)OC(C)=O)(C)CO[C@H]34)CC(=O)OC)C=COC=1 CJHBVBNPNXOWBA-REXVOHEDSA-N 0.000 description 4
- IWERWMCSIQZTFD-UHFFFAOYSA-N salannin Natural products COC(=O)CC1C2(C)C(CC(OC(=O)C)C3(C)COC(C4OC5C(CC(=C5C14C)C)c6cocc6)C23)OC(=O)C(=CC)C IWERWMCSIQZTFD-UHFFFAOYSA-N 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 235000004443 Ricinus communis Nutrition 0.000 description 3
- 239000000654 additive Substances 0.000 description 3
- 230000001887 anti-feedant effect Effects 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 230000009036 growth inhibition Effects 0.000 description 3
- 230000001965 increasing effect Effects 0.000 description 3
- 230000000749 insecticidal effect Effects 0.000 description 3
- 239000002917 insecticide Substances 0.000 description 3
- 239000002018 neem oil Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000003981 vehicle Substances 0.000 description 3
- KWAMDQVQFVBEAU-UHFFFAOYSA-N 17-Epiazadiradione Natural products O=C1C=C2C3(C)C(OC(=O)C)CC4C(C)(C)C(=O)C=CC4(C)C3CCC2(C)C1C=1C=COC=1 KWAMDQVQFVBEAU-UHFFFAOYSA-N 0.000 description 2
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- KWAMDQVQFVBEAU-ASOIATIHSA-N Azadiradione Natural products O=C(O[C@H]1[C@]2(C)[C@@H]([C@]3(C)[C@@H](C(C)(C)C(=O)C=C3)C1)CC[C@@]1(C)[C@H](c3cocc3)C(=O)C=C21)C KWAMDQVQFVBEAU-ASOIATIHSA-N 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- PRXRUNOAOLTIEF-ADSICKODSA-N Sorbitan trioleate Chemical group CCCCCCCC\C=C/CCCCCCCC(=O)OC[C@@H](OC(=O)CCCCCCC\C=C/CCCCCCCC)[C@H]1OC[C@H](O)[C@H]1OC(=O)CCCCCCC\C=C/CCCCCCCC PRXRUNOAOLTIEF-ADSICKODSA-N 0.000 description 2
- 239000004147 Sorbitan trioleate Substances 0.000 description 2
- 239000000010 aprotic solvent Substances 0.000 description 2
- KWAMDQVQFVBEAU-HMWIRDDCSA-N azadiradione Chemical compound C=1([C@H]2[C@]3(C)CC[C@@H]4[C@@]5(C)C=CC(=O)C(C)(C)[C@@H]5C[C@H]([C@]4(C3=CC2=O)C)OC(=O)C)C=COC=1 KWAMDQVQFVBEAU-HMWIRDDCSA-N 0.000 description 2
- XXIKKMLIDXLAIK-IZSBMLLGSA-N azadirone Natural products O=C(O[C@H]1[C@]2(C)[C@@H]([C@]3(C)[C@@H](C(C)(C)C(=O)C=C3)C1)CC[C@@]1(C)[C@H](c3cocc3)CC=C21)C XXIKKMLIDXLAIK-IZSBMLLGSA-N 0.000 description 2
- 239000000969 carrier Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000001627 detrimental effect Effects 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 238000007865 diluting Methods 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 238000004128 high performance liquid chromatography Methods 0.000 description 2
- 150000002632 lipids Chemical class 0.000 description 2
- 239000012669 liquid formulation Substances 0.000 description 2
- 230000010076 replication Effects 0.000 description 2
- 235000019337 sorbitan trioleate Nutrition 0.000 description 2
- 229960000391 sorbitan trioleate Drugs 0.000 description 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 1
- 241000209495 Acorus Species 0.000 description 1
- 241000253994 Acyrthosiphon pisum Species 0.000 description 1
- 241000952611 Aphis craccivora Species 0.000 description 1
- 241001425390 Aphis fabae Species 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241001301805 Epilachna Species 0.000 description 1
- BZLVMXJERCGZMT-UHFFFAOYSA-N Methyl tert-butyl ether Chemical compound COC(C)(C)C BZLVMXJERCGZMT-UHFFFAOYSA-N 0.000 description 1
- 231100000674 Phytotoxicity Toxicity 0.000 description 1
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 1
- 229920001214 Polysorbate 60 Polymers 0.000 description 1
- 241000256248 Spodoptera Species 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000005456 alcohol based solvent Substances 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 239000003125 aqueous solvent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000012681 biocontrol agent Substances 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000004359 castor oil Substances 0.000 description 1
- 235000019438 castor oil Nutrition 0.000 description 1
- 239000013065 commercial product Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000002939 deleterious effect Effects 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000004492 dustable powder Substances 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 150000002118 epoxides Chemical class 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 125000000524 functional group Chemical group 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 1
- 239000008240 homogeneous mixture Substances 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 239000002949 juvenile hormone Substances 0.000 description 1
- 239000000787 lecithin Substances 0.000 description 1
- 235000010445 lecithin Nutrition 0.000 description 1
- 229940067606 lecithin Drugs 0.000 description 1
- 150000002630 limonoids Chemical class 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000002207 metabolite Substances 0.000 description 1
- 238000009329 organic farming Methods 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000010773 plant oil Substances 0.000 description 1
- 239000003880 polar aprotic solvent Substances 0.000 description 1
- 230000003389 potentiating effect Effects 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000011814 protection agent Substances 0.000 description 1
- 239000002728 pyrethroid Substances 0.000 description 1
- 230000000475 sunscreen effect Effects 0.000 description 1
- 239000000516 sunscreening agent Substances 0.000 description 1
- 150000003505 terpenes Chemical class 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
- 239000004563 wettable powder Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US09/536351 | 2000-03-27 | ||
| US09/536,351 US6811790B1 (en) | 2000-03-27 | 2000-03-27 | Storage stable pesticide formulations containing azadirachtin |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| AU5355300A AU5355300A (en) | 2001-10-04 |
| AU783237B2 true AU783237B2 (en) | 2005-10-06 |
Family
ID=24138155
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AU53553/00A Expired AU783237B2 (en) | 2000-03-27 | 2000-08-22 | Storage stable pesticide formulations containing azadirachtin |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US6811790B1 (https=) |
| JP (1) | JP4302905B2 (https=) |
| AR (1) | AR027722A1 (https=) |
| AU (1) | AU783237B2 (https=) |
| CA (1) | CA2316028C (https=) |
| MX (1) | MXPA01003132A (https=) |
| NZ (1) | NZ506082A (https=) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2007530665A (ja) * | 2004-03-31 | 2007-11-01 | エイド パリー （インディア） リミテッド | ニーム種子抽出物の改良された顆粒製剤化およびその方法 |
| US20080090780A1 (en) * | 2006-10-13 | 2008-04-17 | Pbi/Gordon Corporation | Storage stable azadirachtin pesticide formulation |
| WO2010046316A2 (en) * | 2008-10-24 | 2010-04-29 | Unilever Nv | A topical composition |
| CN103168783B (zh) * | 2011-12-22 | 2014-09-03 | 成都绿金高新技术股份有限公司 | 印楝素乳油组合物及其制备方法 |
| NZ727213A (en) | 2012-03-09 | 2020-03-27 | Vestaron Corp | Toxic peptide production, peptide expression in plants and combinations of cysteine rich peptides |
| JP5364819B1 (ja) * | 2012-07-10 | 2013-12-11 | 株式会社カンザイネット | 動植物の育成環境改善材および育成環境改善材の使用方法 |
| JP5973922B2 (ja) * | 2013-01-07 | 2016-08-23 | 株式会社カンザイネット | 植物の育成環境改善用混合物およびその製造方法 |
| BR102013021210B1 (pt) | 2013-01-25 | 2015-12-01 | Fundação Universidade Fed De São Carlos | processo de obtenção de nanopartículas biopoliméricas contendo óleo e extratos de azadirachta indica a. juss (neem), nanopartículas biopoliméricas e micropartículas em pó |
| MX2019001932A (es) | 2016-08-17 | 2019-11-12 | Gowan Company L L C | Formulaciones de azadiractina estables al almacenamiento y metodos de fabricacion y uso de las mismas. |
| IL297738A (en) | 2020-05-01 | 2022-12-01 | Vestaron Corp | Insecticidal combinations |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6034128A (en) * | 1998-06-09 | 2000-03-07 | Sumitomo Chemical Company, Limited | Ester compounds |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4556562A (en) | 1984-03-19 | 1985-12-03 | Vikwood, Ltd. | Stable anti-pest neem seed extract |
| US5001146A (en) | 1989-06-26 | 1991-03-19 | W. R. Grace & Co.-Conn. | Storage stable azadirachtin formulation |
| US4946681A (en) | 1989-06-26 | 1990-08-07 | W. R. Grace & Co.-Conn. | Method to prepare an improved storage stable neem seed extract |
| US5411736A (en) | 1989-12-26 | 1995-05-02 | W. R. Grace & Co.-Conn. | Hydrophic extracted neem oil-a novel insecticide |
| US5372817A (en) | 1991-01-03 | 1994-12-13 | W. R. Grace & Co.-Conn. | Insecticidal compositions derived from neem oil and neem wax fractions |
| DE4109473A1 (de) | 1991-03-22 | 1992-09-24 | Kleeberg Hubertus Dr | Verfahren zur herstellung eines lagerfaehigen azadirachtinreichen insektizids aus samenkernen des neem-baumes |
| US5352697A (en) | 1992-07-28 | 1994-10-04 | Agridyne Technologies, Inc. | Storage stable pesticide compositions comprising azadirachtin and epoxide |
| US5281618A (en) | 1992-09-21 | 1994-01-25 | W. R. Grace & Co.-Conn. | Storage stable high azadirachtin solution |
| US5397571A (en) | 1993-03-25 | 1995-03-14 | W. R. Grace & Co.-Conn. | Co-extraction of azadirachtin and neem oil |
| US5827521A (en) | 1995-03-09 | 1998-10-27 | Fortune Biotech Limited | Shelf stable insect repellent, insect growth regulator and insecticidal formulations prepared from technical azadirachtin isolated from the kernel extract of Azadirachta indica |
| US5635193A (en) | 1995-06-07 | 1997-06-03 | Thermo Trilogy Corporation | Stability of azadirachtin-containing solid |
| IN188667B (https=) | 1995-06-14 | 2002-10-26 | Council Scient Ind Res | |
| IN179008B (https=) | 1995-07-17 | 1997-08-09 | Dalmia Ct For Biotechnology | |
| IN184305B (https=) | 1995-10-19 | 2000-08-05 | Council Scient Ind Res | |
| US5885600A (en) * | 1997-04-01 | 1999-03-23 | Burlington Bio-Medical & Scientific Corp. | Natural insect repellent formula and method of making same |
-
2000
- 2000-03-27 US US09/536,351 patent/US6811790B1/en not_active Expired - Lifetime
- 2000-07-31 NZ NZ506082A patent/NZ506082A/en not_active IP Right Cessation
- 2000-08-16 CA CA002316028A patent/CA2316028C/en not_active Expired - Lifetime
- 2000-08-22 AU AU53553/00A patent/AU783237B2/en not_active Expired
-
2001
- 2001-03-26 MX MXPA01003132A patent/MXPA01003132A/es active IP Right Grant
- 2001-03-26 AR ARP010101422A patent/AR027722A1/es active IP Right Grant
- 2001-03-26 JP JP2001088861A patent/JP4302905B2/ja not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6034128A (en) * | 1998-06-09 | 2000-03-07 | Sumitomo Chemical Company, Limited | Ester compounds |
Also Published As
| Publication number | Publication date |
|---|---|
| AR027722A1 (es) | 2003-04-09 |
| NZ506082A (en) | 2001-11-30 |
| CA2316028C (en) | 2007-01-02 |
| JP2001278721A (ja) | 2001-10-10 |
| JP4302905B2 (ja) | 2009-07-29 |
| CA2316028A1 (en) | 2001-09-27 |
| US6811790B1 (en) | 2004-11-02 |
| MXPA01003132A (es) | 2004-07-30 |
| AU5355300A (en) | 2001-10-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102595885B (zh) | 作为生物化学农业产物的含蒽醌衍生物 | |
| EP1986494B1 (en) | Stable mixtures of microencapsulated and non-encapsulated pesticides | |
| Peres et al. | In natura and nanoencapsulated essential oils from Xylopia aromatica reduce oviposition of Bemisia tabaci in Phaseolus vulgaris | |
| Adel et al. | Application of new nano pesticide Geranium oil loadedsolid lipid nanoparticles for control the black cutworm Agrotis ipsilon (Hub.)(Lepi., Noctuidae). | |
| US10149476B2 (en) | Pesticidal plant extract containing loline derivatives | |
| AU783237B2 (en) | Storage stable pesticide formulations containing azadirachtin | |
| DE2936265A1 (de) | Pestizide waessrige suspension | |
| AU2015335025B2 (en) | Limonene formulation and insecticide use | |
| AU2001244451B2 (en) | Compositions containing neem seed extracts and saccharide | |
| AU2001244451A1 (en) | Compositions containing neem seed extracts and saccharide | |
| JP2003529615A5 (https=) | ||
| JP2636880B2 (ja) | 効力の増強された農業用殺虫殺ダニ剤 | |
| JP5389482B2 (ja) | キク科センダングサ属植物を用いた害虫防除剤および害虫防除方法 | |
| Genrong et al. | Research Status of Toxicity and Residue Detection of High-risk Pesticide Adjuvants | |
| WO2005039288A2 (en) | An insectidcidal composition with enhanced synergistic activity | |
| US20080255237A1 (en) | Pesticidal Composition | |
| CN105104390B (zh) | 一种含环氧虫啶和螺螨酯的杀螨组合物 | |
| Nuryanti et al. | Toxicity of nanoemulsion formulas of botanical insecticide from Pinus merkusii and Moringa oleifera essential oil using inversion phase and homogenization methods against corn planthopper | |
| Mohamed et al. | Insecticidal activity of diesel oil and synthetic plant materials against pink sugar cane mealybug Saccharicoccus sacchari (Hemiptera: Pseudococcidae). | |
| DE60031844T2 (de) | Zusammensetzungen und verfahren zur nematodenbekämpfung | |
| Li GenRong et al. | Research status of toxicity and residue detection of high-risk pesticide adjuvants. | |
| Massoud et al. | Advances in Crop Science and Technology | |
| Krall et al. | 4. Balança, G., MN. de Visscher. 1997a. Impacts on | |
| CA2269998A1 (en) | Azadirachtin formulation |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MK14 | Patent ceased section 143(a) (annual fees not paid) or expired |