AU2010329807A8 - Method and apparatus to create uniform mixing in connection with a hydrometallurgical process - Google Patents

Method and apparatus to create uniform mixing in connection with a hydrometallurgical process

Info

Publication number
AU2010329807A8
AU2010329807A8 AU2010329807A AU2010329807A AU2010329807A8 AU 2010329807 A8 AU2010329807 A8 AU 2010329807A8 AU 2010329807 A AU2010329807 A AU 2010329807A AU 2010329807 A AU2010329807 A AU 2010329807A AU 2010329807 A8 AU2010329807 A8 AU 2010329807A8
Authority
AU
Australia
Prior art keywords
mixing
reactor
hydrometallurgical process
connection
uniform mixing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
AU2010329807A
Other versions
AU2010329807A1 (en
Inventor
Launo Lilja
Juhani Lyyra
Bror Nyman
Pertti Pekkala
Teemu Ritasalao
Jussi Vaarno
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Metso Corp
Original Assignee
Outotec Oyj
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Outotec Oyj filed Critical Outotec Oyj
Publication of AU2010329807A1 publication Critical patent/AU2010329807A1/en
Publication of AU2010329807A8 publication Critical patent/AU2010329807A8/en
Abandoned legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/92Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with helices or screws
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D21/00Separation of suspended solid particles from liquids by sedimentation
    • B01D21/01Separation of suspended solid particles from liquids by sedimentation using flocculating agents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D21/00Separation of suspended solid particles from liquids by sedimentation
    • B01D21/02Settling tanks with single outlets for the separated liquid
    • B01D21/08Settling tanks with single outlets for the separated liquid provided with flocculating compartments
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D21/00Separation of suspended solid particles from liquids by sedimentation
    • B01D21/28Mechanical auxiliary equipment for acceleration of sedimentation, e.g. by vibrators or the like
    • B01D21/286Means for gentle agitation for enhancing flocculation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/50Mixing liquids with solids
    • B01F23/53Mixing liquids with solids using driven stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05Stirrers
    • B01F27/11Stirrers characterised by the configuration of the stirrers
    • B01F27/114Helically shaped stirrers, i.e. stirrers comprising a helically shaped band or helically shaped band sections
    • B01F27/1145Helically shaped stirrers, i.e. stirrers comprising a helically shaped band or helically shaped band sections ribbon shaped with an open space between the helical ribbon flight and the rotating axis
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05Stirrers
    • B01F27/11Stirrers characterised by the configuration of the stirrers
    • B01F27/114Helically shaped stirrers, i.e. stirrers comprising a helically shaped band or helically shaped band sections
    • B01F27/1145Helically shaped stirrers, i.e. stirrers comprising a helically shaped band or helically shaped band sections ribbon shaped with an open space between the helical ribbon flight and the rotating axis
    • B01F27/11451Helically shaped stirrers, i.e. stirrers comprising a helically shaped band or helically shaped band sections ribbon shaped with an open space between the helical ribbon flight and the rotating axis forming open frameworks or cages
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/86Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis co-operating with deflectors or baffles fixed to the receptacle
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/92Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with helices or screws
    • B01F27/922Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with helices or screws with two or more helices, e.g. with intermeshing helices
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F11/00Treatment of sludge; Devices therefor
    • C02F11/12Treatment of sludge; Devices therefor by de-watering, drying or thickening
    • C02F11/14Treatment of sludge; Devices therefor by de-watering, drying or thickening with addition of chemical agents
    • C02F11/147Treatment of sludge; Devices therefor by de-watering, drying or thickening with addition of chemical agents using organic substances
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/34Treatment of water, waste water, or sewage with mechanical oscillations
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/52Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2301/00General aspects of water treatment
    • C02F2301/02Fluid flow conditions
    • C02F2301/024Turbulent

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Water Supply & Treatment (AREA)
  • Hydrology & Water Resources (AREA)
  • Environmental & Geological Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Dispersion Chemistry (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Separation Of Suspended Particles By Flocculating Agents (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

The invention relates to a method and apparatus for mixing one or several solutions in a reactor (3) in conjunction with a hydrometallurgical process, such as precipitation, crystallisation or forming a suspension in solvent extraction. Mixing with a vertical circulation flow is created in the reactor by means of a multi-part mixer (1), so that the primary mixing zone in which the mixer rotates is over 70 % of the effective volume of the reactor, whereby the homogenous, low-intensity mixing needed for precipitation, crystallisation and/or the mixing stage of solvent extraction is achieved.
AU2010329807A 2009-12-08 2010-12-08 Method and apparatus to create uniform mixing in connection with a hydrometallurgical process Abandoned AU2010329807A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FI20096296A FI123597B (en) 2009-12-08 2009-12-08 Method and apparatus for separating solids from slurry and use of the method and / or apparatus
FI20096296 2009-12-08
PCT/FI2010/000074 WO2011070219A1 (en) 2009-12-08 2010-12-08 Method and apparatus to create uniform mixing in connection with a hydrometalurgical process

Publications (2)

Publication Number Publication Date
AU2010329807A1 AU2010329807A1 (en) 2012-06-21
AU2010329807A8 true AU2010329807A8 (en) 2012-07-19

Family

ID=41462762

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2010329807A Abandoned AU2010329807A1 (en) 2009-12-08 2010-12-08 Method and apparatus to create uniform mixing in connection with a hydrometallurgical process

Country Status (11)

Country Link
EP (1) EP2509709A4 (en)
CN (1) CN102665887B (en)
AU (1) AU2010329807A1 (en)
BR (1) BR112012013894A2 (en)
CA (1) CA2780852A1 (en)
CL (1) CL2012001477A1 (en)
EA (1) EA022724B1 (en)
FI (2) FI123597B (en)
PE (1) PE20130300A1 (en)
WO (2) WO2011070218A1 (en)
ZA (1) ZA201203911B (en)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10899969B2 (en) * 2012-06-21 2021-01-26 Suncor Energy Inc. Enhanced techniques for dewatering thick fine tailings
CN103936042A (en) * 2013-01-22 2014-07-23 贵阳铝镁设计研究院有限公司 Three-shaft stirring decomposing tank
CA2823459C (en) 2013-08-09 2015-06-23 Imperial Oil Resources Limited Method of using a silicate-containing stream from a hydrocarbon operation or from a geothermal source to treat fluid tailings by chemically-induced micro-agglomeration
CA2946162A1 (en) 2014-04-30 2015-11-05 Dow Global Technologies Llc Treatment of aqueous mineral suspensions with polymeric flocculants
WO2015168378A1 (en) 2014-04-30 2015-11-05 Dow Global Technologies Llc Polymeric flocculants for treating aqueous mineral suspensions
CA2956460A1 (en) 2014-07-31 2016-02-04 Dow Global Technologies Llc In-line dynamic mixing apparatus for flocculating and dewatering oil sands fine tailings
CN104226147B (en) * 2014-10-15 2016-08-17 浙江辰鸿纺织品科技有限公司 A kind of for window cloth slurry high efficiency dispersion mixing arrangement
WO2017034790A1 (en) 2015-08-25 2017-03-02 Dow Global Technologies Llc Flocculation of high-solids mineral slurries
AR108480A1 (en) 2016-05-27 2018-08-22 Dow Global Technologies Llc METHOD OF TREATMENT OF MINERAL SUSPENSIONS WITH HIGH CONTENT OF SOLIDS WITH POLYMER FLOCULANTS
US20190233310A1 (en) 2016-07-25 2019-08-01 Dow Global Technologies Llc Acoustic mixing for flocculant addition to mineral suspensions
CA3038070A1 (en) 2016-09-23 2018-03-29 Dow Global Technologies Llc Process for tailings remediation
WO2018063810A1 (en) 2016-09-27 2018-04-05 Dow Global Technologies Llc Process for dewatering an aqueous process stream
CN106861501A (en) * 2017-03-20 2017-06-20 无锡科技职业学院 A kind of high-shear emulsifying dissolves mixing kettle
WO2019172223A1 (en) * 2018-03-05 2019-09-12 日本ソセー工業株式会社 Rotary mixer in two-liquid mixture injection machine
CN109529703A (en) * 2018-11-28 2019-03-29 河南易成新能源股份有限公司 Graphite product ingredient mixing arrangement
CN112456672A (en) * 2019-09-09 2021-03-09 国家能源投资集团有限责任公司 Mine water treatment method and system
US20230201778A1 (en) * 2020-04-20 2023-06-29 Metso Outotec Finland Oy Mixing arrangement, mixer settler unit and use

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR615110A (en) * 1926-04-26 1926-12-30 Mixer
NL52125C (en) * 1939-03-31 1942-03-16
DE1225951B (en) * 1961-08-10 1966-09-29 Wilhelm Heinrich Schmidt Mixing device
US4198376A (en) * 1974-02-14 1980-04-15 Rhone-Progil Vertical autoclave for bulk polymerization of vinyl chloride based polymers and copolymers
US5248485A (en) * 1990-04-04 1993-09-28 Outokumpu Oy Method for mixing liquid, solids and gas and for simultaneously separating gas or gas and solids from the liquid
CN2158301Y (en) * 1993-03-26 1994-03-09 郭洪臣 Double-shaft helice mixer
DE19901267B4 (en) * 1999-01-15 2006-08-10 Löhr, Anke, Dr. Mixing and treatment device
FI114783B (en) * 2001-06-25 2004-12-31 Outokumpu Oy Method and apparatus for clarifying sludge
FI123662B (en) * 2006-02-17 2013-08-30 Outotec Oyj Method and agitator apparatus for mixing gas in slurry in a closed reactor
CA2673982A1 (en) * 2008-07-28 2010-01-28 Hunton Energy Holdings, LLC Basic filtration of bitumen fines

Also Published As

Publication number Publication date
FI20096296A (en) 2011-06-09
ZA201203911B (en) 2013-04-24
EA201290405A1 (en) 2013-01-30
CN102665887A (en) 2012-09-12
EP2509709A4 (en) 2016-01-06
WO2011070218A1 (en) 2011-06-16
FI20100318A (en) 2011-06-09
WO2011070219A1 (en) 2011-06-16
FI20100318A0 (en) 2010-09-16
EP2509709A1 (en) 2012-10-17
FI123597B (en) 2013-07-31
PE20130300A1 (en) 2013-03-22
CL2012001477A1 (en) 2012-11-16
WO2011070219A8 (en) 2011-11-17
FI20096296A0 (en) 2009-12-08
EA022724B1 (en) 2016-02-29
AU2010329807A1 (en) 2012-06-21
CA2780852A1 (en) 2011-06-16
FI124092B (en) 2014-03-14
BR112012013894A2 (en) 2016-05-03
CN102665887B (en) 2015-06-24

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Legal Events

Date Code Title Description
TH Corrigenda

Free format text: IN VOL 26 , NO 23 , PAGE(S) 3149 UNDER THE HEADING PCT APPLICATIONS THAT HAVE ENTERED THE NATIONAL PHASE - NAME INDEX UNDER THE NAME OUTOTEC OYJ, APPLICATION NO. 2010329807, UNDER INID (72) CORRECT THE CO-INTENTOR TO PEKKALA, PERTTI.

DA3 Amendments made section 104

Free format text: THE NATURE OF THE AMENDMENT IS: AMEND THE INVENTION TITLE TO READ METHOD AND APPARATUS TO CREATE UNIFORM MIXING IN CONNECTION WITH A HYDROMETALLURGICAL PROCESS

MK5 Application lapsed section 142(2)(e) - patent request and compl. specification not accepted