AU2005309411B2 - Mesoporous metal oxide - Google Patents

Mesoporous metal oxide Download PDF

Info

Publication number
AU2005309411B2
AU2005309411B2 AU2005309411A AU2005309411A AU2005309411B2 AU 2005309411 B2 AU2005309411 B2 AU 2005309411B2 AU 2005309411 A AU2005309411 A AU 2005309411A AU 2005309411 A AU2005309411 A AU 2005309411A AU 2005309411 B2 AU2005309411 B2 AU 2005309411B2
Authority
AU
Australia
Prior art keywords
titanium
zirconium
hafnium
oxide
halide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
AU2005309411A
Other languages
English (en)
Other versions
AU2005309411A1 (en
Inventor
Carmine Torardi
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EIDP Inc
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US10/995,968 external-priority patent/US20060110316A1/en
Priority claimed from US11/170,878 external-priority patent/US7601326B2/en
Priority claimed from US11/172,099 external-priority patent/US20060110318A1/en
Priority claimed from US11/171,055 external-priority patent/US20060110317A1/en
Priority claimed from US11/170,991 external-priority patent/US7601327B2/en
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Publication of AU2005309411A1 publication Critical patent/AU2005309411A1/en
Application granted granted Critical
Publication of AU2005309411B2 publication Critical patent/AU2005309411B2/en
Ceased legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/04—Oxides; Hydroxides
    • C01G23/047—Titanium dioxide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/04—Oxides; Hydroxides
    • C01G23/047—Titanium dioxide
    • C01G23/053—Producing by wet processes, e.g. hydrolysing titanium salts
    • C01G23/0536—Producing by wet processes, e.g. hydrolysing titanium salts by hydrolysing chloride-containing salts
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00—Compounds of zirconium
    • C01G25/02—Oxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G27/00—Compounds of hafnium
    • C01G27/02—Oxides
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/36—Compounds of titanium
    • C09C1/3607—Titanium dioxide
    • C09C1/3669—Treatment with low-molecular organic compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/36—Compounds of titanium
    • C09C1/3607—Titanium dioxide
    • C09C1/3676—Treatment with macro-molecular organic compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/36—Compounds of titanium
    • C09C1/3607—Titanium dioxide
    • C09C1/3684—Treatment with organo-silicon compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/14—Pore volume
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/16—Pore diameter

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Nanotechnology (AREA)
  • Physics & Mathematics (AREA)
  • Composite Materials (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
AU2005309411A 2004-11-23 2005-11-23 Mesoporous metal oxide Ceased AU2005309411B2 (en)

Applications Claiming Priority (11)

Application Number Priority Date Filing Date Title
US10/995,968 US20060110316A1 (en) 2004-11-23 2004-11-23 Mesoporous metal oxide
US10/995,968 2004-11-23
US11/171,055 2005-06-30
US11/170,878 US7601326B2 (en) 2004-11-23 2005-06-30 Mesoporous oxide of zirconium
US11/172,099 US20060110318A1 (en) 2004-11-23 2005-06-30 Mesoporous oxide of titanium
US11/170,878 2005-06-30
US11/170,991 2005-06-30
US11/171,055 US20060110317A1 (en) 2004-11-23 2005-06-30 Mesoporous amorphous oxide of titanium
US11/172,099 2005-06-30
US11/170,991 US7601327B2 (en) 2004-11-23 2005-06-30 Mesoporous oxide of hafnium
PCT/US2005/042817 WO2006058254A1 (en) 2004-11-23 2005-11-23 Mesoporous metal oxide

Publications (2)

Publication Number Publication Date
AU2005309411A1 AU2005309411A1 (en) 2006-06-01
AU2005309411B2 true AU2005309411B2 (en) 2011-06-02

Family

ID=36498313

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2005309411A Ceased AU2005309411B2 (en) 2004-11-23 2005-11-23 Mesoporous metal oxide

Country Status (3)

Country Link
EP (1) EP1831106A4 (de)
AU (1) AU2005309411B2 (de)
WO (1) WO2006058254A1 (de)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7858066B2 (en) 2007-05-08 2010-12-28 E.I. Du Pont De Nemours And Company Method of making titanium dioxide particles
EP2207754A1 (de) * 2007-11-05 2010-07-21 E. I. du Pont de Nemours and Company Hochtemperaturstabiles anatase-titan-dioxid
AU2008343168A1 (en) * 2007-12-20 2009-07-09 E. I. Du Pont De Nemours And Company Luminescent samarium-doped titanium dioxide
CN101294928B (zh) * 2008-06-13 2011-09-07 北京化工大学 MoO3-SnO2基掺杂的纳米复合金属氧化物及其制备方法
WO2010106146A1 (en) 2009-03-20 2010-09-23 Basf Se Manufacture process for titanium dioxide materials with high surface areas and high thermal stability

Citations (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU247930A1 (ru) * 1967-07-15 1973-02-08 Т. Ф. Лимарь, С. В. лик, Л. В. Смирнов , А. И. зев Способ получения легированной полупроводниковой двуокиси титана
US4286378A (en) * 1979-03-09 1981-09-01 General Motors Corporation Process for producing a body of sintered TiO2 for resistive gas sensor
US4605631A (en) * 1984-03-19 1986-08-12 Norton Company Advanced preparation of ceramic powders
US4664894A (en) * 1984-08-07 1987-05-12 Nippon Shokubai Kagaku Kogyo Co., Ltd. Micronized zirconia and method for production thereof
US5532057A (en) * 1990-09-26 1996-07-02 The United States Of America As Represented By The Secretary Of The Navy India-stabilized ziroconia coating for composites
US5631310A (en) * 1994-02-28 1997-05-20 E. I. Du Pont De Nemours And Company Processibility and lacing resistance when silanized pigments are incorporated in polymers
US5718878A (en) * 1996-07-12 1998-02-17 Akzo Nobel N.V. Mesoporous titania and process for its preparation
US5786294A (en) * 1996-05-10 1998-07-28 Northwestern University Crystalline mesoporous zirconia catalysts having stable tetragonal pore wall structure
US5922120A (en) * 1997-12-23 1999-07-13 E. I. Du Pont De Nemours And Company Process for producing coated TiO2 pigment using cooxidation to provide hydrous oxide coatings
US6168830B1 (en) * 1999-07-28 2001-01-02 National Science Council Of Republic Of China Process for fabricating crystalline metal oxide material
JP2001031422A (ja) * 1999-07-19 2001-02-06 Agency Of Ind Science & Technol メソポーラス酸化チタン多孔体およびその製造方法
WO2001081244A2 (en) * 2000-04-26 2001-11-01 E.I. Dupont De Nemours And Company Method for producing titanium oxide particles for use in photovoltaic cells
AU2003213434A1 (en) * 2002-03-13 2003-09-22 Ishihara Sangyo Kaisha, Ltd. Process for production of titanium dioxide pigment and resin compositions containing the pigment
WO2003080514A1 (fr) * 2002-03-26 2003-10-02 Japan Science And Technology Agency Procede de production d'oxyde metallique micro-mesoporeux presentant des pores controles formes par un procede nouveau de retrait de gabarit
EP1422198A1 (de) * 2001-07-27 2004-05-26 Chiyoda Corporation Poröses oxid eines metalls der gruppe 4 und verfahren zu seiner herstellung
US7125536B2 (en) * 2004-02-06 2006-10-24 Millennium Inorganic Chemicals, Inc. Nano-structured particles with high thermal stability

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2767807B1 (fr) * 1997-08-26 1999-10-08 Oreal Procede de preparation d'oxyde de titane photochrome, compose obtenu et composition le comprenant

Patent Citations (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU247930A1 (ru) * 1967-07-15 1973-02-08 Т. Ф. Лимарь, С. В. лик, Л. В. Смирнов , А. И. зев Способ получения легированной полупроводниковой двуокиси титана
US4286378A (en) * 1979-03-09 1981-09-01 General Motors Corporation Process for producing a body of sintered TiO2 for resistive gas sensor
US4605631A (en) * 1984-03-19 1986-08-12 Norton Company Advanced preparation of ceramic powders
US4664894A (en) * 1984-08-07 1987-05-12 Nippon Shokubai Kagaku Kogyo Co., Ltd. Micronized zirconia and method for production thereof
US5532057A (en) * 1990-09-26 1996-07-02 The United States Of America As Represented By The Secretary Of The Navy India-stabilized ziroconia coating for composites
US5631310A (en) * 1994-02-28 1997-05-20 E. I. Du Pont De Nemours And Company Processibility and lacing resistance when silanized pigments are incorporated in polymers
US5786294A (en) * 1996-05-10 1998-07-28 Northwestern University Crystalline mesoporous zirconia catalysts having stable tetragonal pore wall structure
US5718878A (en) * 1996-07-12 1998-02-17 Akzo Nobel N.V. Mesoporous titania and process for its preparation
US5922120A (en) * 1997-12-23 1999-07-13 E. I. Du Pont De Nemours And Company Process for producing coated TiO2 pigment using cooxidation to provide hydrous oxide coatings
JP2001031422A (ja) * 1999-07-19 2001-02-06 Agency Of Ind Science & Technol メソポーラス酸化チタン多孔体およびその製造方法
US6168830B1 (en) * 1999-07-28 2001-01-02 National Science Council Of Republic Of China Process for fabricating crystalline metal oxide material
WO2001081244A2 (en) * 2000-04-26 2001-11-01 E.I. Dupont De Nemours And Company Method for producing titanium oxide particles for use in photovoltaic cells
EP1422198A1 (de) * 2001-07-27 2004-05-26 Chiyoda Corporation Poröses oxid eines metalls der gruppe 4 und verfahren zu seiner herstellung
AU2003213434A1 (en) * 2002-03-13 2003-09-22 Ishihara Sangyo Kaisha, Ltd. Process for production of titanium dioxide pigment and resin compositions containing the pigment
WO2003080514A1 (fr) * 2002-03-26 2003-10-02 Japan Science And Technology Agency Procede de production d'oxyde metallique micro-mesoporeux presentant des pores controles formes par un procede nouveau de retrait de gabarit
US7125536B2 (en) * 2004-02-06 2006-10-24 Millennium Inorganic Chemicals, Inc. Nano-structured particles with high thermal stability

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
ADAMSKI A ET AL, NAT. CNTR F ST&E , V51, 06, p S27-S33 *
TAKAHASHI, J Che. So., RSC, Vol. 94, No. 20, 21 Oct 1998. *

Also Published As

Publication number Publication date
AU2005309411A1 (en) 2006-06-01
WO2006058254A1 (en) 2006-06-01
EP1831106A4 (de) 2008-03-19
EP1831106A1 (de) 2007-09-12

Similar Documents

Publication Publication Date Title
US8377414B2 (en) Mesoporous amorphous oxide of titanium
US7601326B2 (en) Mesoporous oxide of zirconium
US8221655B2 (en) Mesoporous oxide of titanium
US20060110318A1 (en) Mesoporous oxide of titanium
US20060110317A1 (en) Mesoporous amorphous oxide of titanium
US7601327B2 (en) Mesoporous oxide of hafnium
US20080031806A1 (en) Continuous process for making nanocrystalline metal dioxide
Yue et al. Syntheses, Li insertion, and photoactivity of mesoporous crystalline TiO2
Kim et al. Homogeneous precipitation of TiO2 ultrafine powders from aqueous TiOCl2 solution
AU2006202179B2 (en) Lower-energy process for preparing passivated inorganic nanoparticles
EP0992456B1 (de) Verfahren zur herstellung von kompositsolen, überzugkomposition und optischem element
KR101586358B1 (ko) 하이브리드 비히클 시스템
US20060110316A1 (en) Mesoporous metal oxide
US20110259244A1 (en) Nanoparticulate Titanium Dioxide Particles with a Crystalline Core, a Metal-Oxide Shell and an Outer Skin Containing Organic Groups, and Method for the Manufacture Thereof
CA2190436A1 (en) Nanodisperse titanium dioxide, process for the production thereof and use thereof
JP5657197B2 (ja) 酸化チタン系粒子およびその製造方法
AU2005309411B2 (en) Mesoporous metal oxide
US20100266487A1 (en) High temperature stable anatase titanium dioxide
US20090117384A1 (en) Titania Nanocavities and Method of Making
US20100247413A1 (en) Luminescent samarium-doped titanium dioxide
平野正典 et al. Hydrothermal synthesis of TiO2/SiO2 composite nanoparticles and their photocatalytic performances
CN113165900B (zh) 一种在氨基酸存在下制备二氧化锆纳米颗粒的方法
Baiju et al. Aqueous sol-gel process for nanocrystalline photocatalytic titania, transparent functional coatings and ceramic membrane

Legal Events

Date Code Title Description
FGA Letters patent sealed or granted (standard patent)
MK14 Patent ceased section 143(a) (annual fees not paid) or expired