AU2003295736B2 - Tissue web product having both fugitive wet strength and a fiber flexibilizing compound - Google Patents
Tissue web product having both fugitive wet strength and a fiber flexibilizing compound Download PDFInfo
- Publication number
- AU2003295736B2 AU2003295736B2 AU2003295736A AU2003295736A AU2003295736B2 AU 2003295736 B2 AU2003295736 B2 AU 2003295736B2 AU 2003295736 A AU2003295736 A AU 2003295736A AU 2003295736 A AU2003295736 A AU 2003295736A AU 2003295736 B2 AU2003295736 B2 AU 2003295736B2
- Authority
- AU
- Australia
- Prior art keywords
- web
- fiber
- tissue product
- tissue
- fibers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/71—Mixtures of material ; Pulp or paper comprising several different materials not incorporated by special processes
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H23/00—Processes or apparatus for adding material to the pulp or to the paper
- D21H23/76—Processes or apparatus for adding material to the pulp or to the paper characterised by choice of auxiliary compounds which are added separately from at least one other compound, e.g. to improve the incorporation of the latter or to obtain an enhanced combined effect
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/20—Macromolecular organic compounds
- D21H17/33—Synthetic macromolecular compounds
- D21H17/34—Synthetic macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D21H17/36—Polyalkenyalcohols; Polyalkenylethers; Polyalkenylesters
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/20—Macromolecular organic compounds
- D21H17/33—Synthetic macromolecular compounds
- D21H17/46—Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D21H17/53—Polyethers; Polyesters
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/63—Inorganic compounds
- D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/71—Mixtures of material ; Pulp or paper comprising several different materials not incorporated by special processes
- D21H17/74—Mixtures of material ; Pulp or paper comprising several different materials not incorporated by special processes of organic and inorganic material
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/36—Coatings with pigments
- D21H19/44—Coatings with pigments characterised by the other ingredients, e.g. the binder or dispersing agent
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
- D21H21/18—Reinforcing agents
- D21H21/20—Wet strength agents
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
- D21H21/22—Agents rendering paper porous, absorbent or bulky
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/24—Structurally defined web or sheet [e.g., overall dimension, etc.]
- Y10T428/24355—Continuous and nonuniform or irregular surface on layer or component [e.g., roofing, etc.]
- Y10T428/24446—Wrinkled, creased, crinkled or creped
- Y10T428/24455—Paper
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/24—Structurally defined web or sheet [e.g., overall dimension, etc.]
- Y10T428/24355—Continuous and nonuniform or irregular surface on layer or component [e.g., roofing, etc.]
- Y10T428/24446—Wrinkled, creased, crinkled or creped
- Y10T428/24455—Paper
- Y10T428/24463—Plural paper components
Landscapes
- Paper (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/302,228 US6818101B2 (en) | 2002-11-22 | 2002-11-22 | Tissue web product having both fugitive wet strength and a fiber flexibilizing compound |
US10/302,228 | 2002-11-22 | ||
PCT/US2003/037217 WO2004048694A2 (en) | 2002-11-22 | 2003-11-20 | Tissue web product having both fugitive wet strength and a fiber flexibilizing compound |
Publications (2)
Publication Number | Publication Date |
---|---|
AU2003295736A1 AU2003295736A1 (en) | 2004-06-18 |
AU2003295736B2 true AU2003295736B2 (en) | 2006-12-07 |
Family
ID=32324713
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AU2003295736A Ceased AU2003295736B2 (en) | 2002-11-22 | 2003-11-20 | Tissue web product having both fugitive wet strength and a fiber flexibilizing compound |
Country Status (9)
Country | Link |
---|---|
US (1) | US6818101B2 (ja) |
EP (1) | EP1563142A2 (ja) |
JP (1) | JP2006506556A (ja) |
CN (2) | CN100402749C (ja) |
AU (1) | AU2003295736B2 (ja) |
BR (1) | BR0316513A (ja) |
CA (1) | CA2506939C (ja) |
MX (1) | MXPA05004551A (ja) |
WO (1) | WO2004048694A2 (ja) |
Families Citing this family (35)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8241543B2 (en) | 2003-08-07 | 2012-08-14 | The Procter & Gamble Company | Method and apparatus for making an apertured web |
US20050215146A1 (en) * | 2004-03-24 | 2005-09-29 | Kimberly-Clark Worldwide, Inc. | Wiping products containing deliquescent materials |
SE529130C2 (sv) * | 2004-05-26 | 2007-05-08 | Metso Paper Karlstad Ab | Pappersmaskin för framställning av mjukpapper, metod för framställning av mjukpapper samt mjukpapper |
US7854822B2 (en) * | 2004-12-02 | 2010-12-21 | Rayonier Trs Holdings Inc. | Plasticizing formulation for fluff pulp and plasticized fluff pulp products made therefrom |
US20070048357A1 (en) * | 2005-08-31 | 2007-03-01 | Kimberly-Clark Worldwide, Inc. | Fibrous wiping products |
US7622022B2 (en) | 2006-06-01 | 2009-11-24 | Benny J Skaggs | Surface treatment of substrate or paper/paperboard products using optical brightening agent |
SE530020C2 (sv) * | 2006-06-15 | 2008-02-12 | Holmen Ab | Förfarande för stabilisering av vitheten hos i ytbehandlingslim/smet för papper ingående fluroescerande vitmedel (FWA) och hos av detta/dessa formade ytbehandlingsskikt |
US20080008865A1 (en) * | 2006-06-23 | 2008-01-10 | Georgia-Pacific Consumer Products Lp | Antimicrobial hand towel for touchless automatic dispensers |
US7585392B2 (en) * | 2006-10-10 | 2009-09-08 | Georgia-Pacific Consumer Products Lp | Method of producing absorbent sheet with increased wet/dry CD tensile ratio |
US7704601B2 (en) | 2008-02-29 | 2010-04-27 | The Procter & Gamble Company | Fibrous structures |
US7687140B2 (en) | 2008-02-29 | 2010-03-30 | The Procter & Gamble Company | Fibrous structures |
US7811665B2 (en) | 2008-02-29 | 2010-10-12 | The Procter & Gamble Compmany | Embossed fibrous structures |
US8025966B2 (en) * | 2008-02-29 | 2011-09-27 | The Procter & Gamble Company | Fibrous structures |
US7960020B2 (en) * | 2008-02-29 | 2011-06-14 | The Procter & Gamble Company | Embossed fibrous structures |
WO2010033536A2 (en) | 2008-09-16 | 2010-03-25 | Dixie Consumer Products Llc | Food wrap basesheet with regenerated cellulose microfiber |
FR2940330B1 (fr) * | 2008-12-18 | 2017-06-23 | Georgia-Pacific France | Feuille de papier delitable dans l'eau, mandrin pour rouleau de papier constitue d'une telle feuille |
FR2940331B1 (fr) | 2008-12-18 | 2010-12-17 | Georgia Pacific France | Procede de fabrication d'une feuille de papier delitable, utilisation de la feuille pour la fabrication d'un mandrin formant support de rouleau, feuille de papier delitable et mandrin constitue d'au moins une desdites feuilles |
FR2948696A1 (fr) | 2009-08-03 | 2011-02-04 | Georgia Pacific France | Procede de fabrication d'une feuille de papier delitable, feuille de papier delitable, mandrin constitue d'au moins une desdites feuilles |
US8334050B2 (en) | 2010-02-04 | 2012-12-18 | The Procter & Gamble Company | Fibrous structures |
US8383235B2 (en) | 2010-02-04 | 2013-02-26 | The Procter & Gamble Company | Fibrous structures |
US8334049B2 (en) | 2010-02-04 | 2012-12-18 | The Procter & Gamble Company | Fibrous structures |
US8449976B2 (en) | 2010-02-04 | 2013-05-28 | The Procter & Gamble Company | Fibrous structures |
CN103038402B (zh) | 2010-05-11 | 2015-07-15 | Fp创新研究中心 | 纤维素纳米纤丝及其制造方法 |
US9752281B2 (en) | 2010-10-27 | 2017-09-05 | The Procter & Gamble Company | Fibrous structures and methods for making same |
US20120107511A1 (en) | 2010-11-01 | 2012-05-03 | Georgia-Pacific Consumer Products Lp | Method Of Applying Fugitive Hydrophobic Treatment To Tissue Product |
US9365980B2 (en) | 2010-11-05 | 2016-06-14 | International Paper Company | Packaging material having moisture barrier and methods for preparing same |
US9358576B2 (en) | 2010-11-05 | 2016-06-07 | International Paper Company | Packaging material having moisture barrier and methods for preparing same |
AU2012208922B2 (en) | 2011-01-21 | 2016-10-13 | Fpinnovations | High aspect ratio cellulose nanofilaments and method for their production |
US8657596B2 (en) | 2011-04-26 | 2014-02-25 | The Procter & Gamble Company | Method and apparatus for deforming a web |
US9925731B2 (en) | 2011-04-26 | 2018-03-27 | The Procter & Gamble Company | Corrugated and apertured web |
US9242406B2 (en) | 2011-04-26 | 2016-01-26 | The Procter & Gamble Company | Apparatus and process for aperturing and stretching a web |
US20130189457A1 (en) | 2012-01-23 | 2013-07-25 | International Paper Company | SEPARATED TREATMENT OF PAPER SUBSTRATE WITH MULTIVALENT METAL SALTS AND OBAs |
CN105155341B (zh) * | 2015-10-05 | 2017-03-29 | 福建农林大学 | 一种高强度高柔软性高抗菌性生活用纸及其制备方法 |
US11000428B2 (en) | 2016-03-11 | 2021-05-11 | The Procter & Gamble Company | Three-dimensional substrate comprising a tissue layer |
JP2021532945A (ja) | 2018-08-22 | 2021-12-02 | ザ プロクター アンド ギャンブル カンパニーThe Procter & Gamble Company | 使い捨て吸収性物品 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4529480A (en) * | 1983-08-23 | 1985-07-16 | The Procter & Gamble Company | Tissue paper |
US6162329A (en) * | 1997-10-01 | 2000-12-19 | The Procter & Gamble Company | Soft tissue paper having a softening composition containing an electrolyte deposited thereon |
WO2001038638A1 (en) * | 1999-11-23 | 2001-05-31 | Kimberly-Clark Worldwide, Inc. | Sanitary tissue products with improved flushability |
Family Cites Families (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4528239A (en) * | 1983-08-23 | 1985-07-09 | The Procter & Gamble Company | Deflection member |
US4514345A (en) * | 1983-08-23 | 1985-04-30 | The Procter & Gamble Company | Method of making a foraminous member |
US5217576A (en) * | 1991-11-01 | 1993-06-08 | Dean Van Phan | Soft absorbent tissue paper with high temporary wet strength |
JP2996319B2 (ja) | 1991-12-03 | 1999-12-27 | 河野製紙株式会社 | 高水分含有性を有するティッシュペーパー |
CZ50695A3 (en) * | 1992-08-26 | 1995-09-13 | Procter & Gamble | Cellulose fibrous structure and a band for producing thereof |
CA2098326A1 (en) | 1993-03-24 | 1994-09-25 | Steven A. Engel | Method for making smooth uncreped throughdried sheets |
US5449551A (en) * | 1993-06-03 | 1995-09-12 | Kawano Paper Co., Ltd. | Highly water absorbent fibrous web and a process for producing the same |
JP3860615B2 (ja) | 1994-01-27 | 2006-12-20 | 大王製紙株式会社 | 柔軟性を有する繊維ウェブおよびその製造方法 |
CA2142805C (en) | 1994-04-12 | 1999-06-01 | Greg Arthur Wendt | Method of making soft tissue products |
DE69512572T2 (de) | 1994-06-21 | 2000-05-25 | Kimberly Clark Co | Glycerin und quaternäre Ammonium-Verbindungen enthaltendes Tissuepapier |
US6059928A (en) * | 1995-09-18 | 2000-05-09 | Fort James Corporation | Prewettable high softness paper product having temporary wet strength |
JP3454997B2 (ja) | 1995-12-06 | 2003-10-06 | 河野製紙株式会社 | 保湿性を有する水解紙及びその製造方法 |
US5785813A (en) * | 1997-02-24 | 1998-07-28 | Kimberly-Clark Worldwide Inc. | Method of treating a papermaking furnish for making soft tissue |
DE19711452A1 (de) | 1997-03-19 | 1998-09-24 | Sca Hygiene Paper Gmbh | Feuchtigkeitsregulatoren enthaltende Zusammensetzung für Tissueprodukte, Verfahren zur Herstellung dieser Produkte, Verwendung der Zusammensetzung für die Behandlung von Tissueprodukten sowie Tissueprodukte in Form von wetlaid einschließlich TAD oder Airlaid (non-woven) auf Basis überwiegend Cellulosefasern enthaltender flächiger Trägermaterialien |
JP3865506B2 (ja) * | 1997-09-08 | 2007-01-10 | ユニ・チャーム株式会社 | 繊維長が違う繊維を含有する水解性の繊維シート |
US6468392B2 (en) * | 1997-09-26 | 2002-10-22 | Fort James Corporation | Soft chemi-mechanically embossed absorbent paper product and method of making same |
JP3297035B2 (ja) | 2000-03-17 | 2002-07-02 | 大王製紙株式会社 | 柔軟性を有する繊維ウェブおよびその製造方法 |
EP1176254A1 (en) * | 2000-07-24 | 2002-01-30 | The Dow Chemical Company | Use of dispersions of crosslinked cationic starch in papermaking |
US7311853B2 (en) * | 2002-09-20 | 2007-12-25 | The Procter & Gamble Company | Paper softening compositions containing quaternary ammonium compound and high levels of free amine and soft tissue paper products comprising said compositions |
-
2002
- 2002-11-22 US US10/302,228 patent/US6818101B2/en not_active Expired - Lifetime
-
2003
- 2003-11-20 BR BR0316513-2A patent/BR0316513A/pt not_active IP Right Cessation
- 2003-11-20 CN CNB2003801037075A patent/CN100402749C/zh not_active Expired - Fee Related
- 2003-11-20 CN CN200380103705.6A patent/CN100582367C/zh not_active Expired - Fee Related
- 2003-11-20 AU AU2003295736A patent/AU2003295736B2/en not_active Ceased
- 2003-11-20 JP JP2004555530A patent/JP2006506556A/ja active Pending
- 2003-11-20 CA CA002506939A patent/CA2506939C/en not_active Expired - Fee Related
- 2003-11-20 EP EP03786939A patent/EP1563142A2/en not_active Withdrawn
- 2003-11-20 MX MXPA05004551A patent/MXPA05004551A/es active IP Right Grant
- 2003-11-20 WO PCT/US2003/037217 patent/WO2004048694A2/en active Application Filing
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4529480A (en) * | 1983-08-23 | 1985-07-16 | The Procter & Gamble Company | Tissue paper |
US6162329A (en) * | 1997-10-01 | 2000-12-19 | The Procter & Gamble Company | Soft tissue paper having a softening composition containing an electrolyte deposited thereon |
WO2001038638A1 (en) * | 1999-11-23 | 2001-05-31 | Kimberly-Clark Worldwide, Inc. | Sanitary tissue products with improved flushability |
Also Published As
Publication number | Publication date |
---|---|
WO2004048694A3 (en) | 2004-07-15 |
CA2506939C (en) | 2008-11-18 |
EP1563142A2 (en) | 2005-08-17 |
CN1714201A (zh) | 2005-12-28 |
WO2004048694A2 (en) | 2004-06-10 |
CN100582367C (zh) | 2010-01-20 |
JP2006506556A (ja) | 2006-02-23 |
MXPA05004551A (es) | 2005-07-26 |
BR0316513A (pt) | 2005-10-04 |
US20040099387A1 (en) | 2004-05-27 |
AU2003295736A1 (en) | 2004-06-18 |
US6818101B2 (en) | 2004-11-16 |
CN1714203A (zh) | 2005-12-28 |
CA2506939A1 (en) | 2004-06-10 |
CN100402749C (zh) | 2008-07-16 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FGA | Letters patent sealed or granted (standard patent) | ||
MK14 | Patent ceased section 143(a) (annual fees not paid) or expired |