AU2003267271B2 - Precipitation of solid particles from droplets formed using focused acoustic energy - Google Patents
Precipitation of solid particles from droplets formed using focused acoustic energy Download PDFInfo
- Publication number
- AU2003267271B2 AU2003267271B2 AU2003267271A AU2003267271A AU2003267271B2 AU 2003267271 B2 AU2003267271 B2 AU 2003267271B2 AU 2003267271 A AU2003267271 A AU 2003267271A AU 2003267271 A AU2003267271 A AU 2003267271A AU 2003267271 B2 AU2003267271 B2 AU 2003267271B2
- Authority
- AU
- Australia
- Prior art keywords
- compound
- interest
- solution
- reservoir
- droplet
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
- A61K9/16—Agglomerates; Granulates; Microbeadlets ; Microspheres; Pellets; Solid products obtained by spray drying, spray freeze drying, spray congealing,(multiple) emulsion solvent evaporation or extraction
- A61K9/1682—Processes
- A61K9/1688—Processes resulting in pure drug agglomerate optionally containing up to 5% of excipient
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/10—Dispersions; Emulsions
- A61K9/12—Aerosols; Foams
- A61K9/122—Foams; Dry foams
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/02—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/02—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops
- B01J2/04—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops in a gaseous medium
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Engineering & Computer Science (AREA)
- Veterinary Medicine (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Medicinal Preparation (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Glanulating (AREA)
- Special Spraying Apparatus (AREA)
- Medicines Containing Antibodies Or Antigens For Use As Internal Diagnostic Agents (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/244,128 US6869551B2 (en) | 2001-03-30 | 2002-09-13 | Precipitation of solid particles from droplets formed using focused acoustic energy |
| US10/244,128 | 2002-09-13 | ||
| PCT/US2003/029283 WO2004024343A1 (en) | 2002-09-13 | 2003-09-15 | Precipitation of solid particles from droplets formed using focused acoustic energy |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| AU2003267271A1 AU2003267271A1 (en) | 2004-04-30 |
| AU2003267271B2 true AU2003267271B2 (en) | 2009-03-12 |
Family
ID=31991830
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AU2003267271A Expired AU2003267271B2 (en) | 2002-09-13 | 2003-09-15 | Precipitation of solid particles from droplets formed using focused acoustic energy |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US6869551B2 (https=) |
| EP (1) | EP1551566B1 (https=) |
| JP (1) | JP5220263B2 (https=) |
| AU (1) | AU2003267271B2 (https=) |
| CA (1) | CA2498393C (https=) |
| WO (1) | WO2004024343A1 (https=) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2803538B1 (fr) * | 1999-12-15 | 2002-06-07 | Separex Sa | Procede et dispositif de captage de fines particules par percolation dans un lit de granules |
| US6713022B1 (en) | 2000-11-22 | 2004-03-30 | Xerox Corporation | Devices for biofluid drop ejection |
| US6740530B1 (en) | 2000-11-22 | 2004-05-25 | Xerox Corporation | Testing method and configurations for multi-ejector system |
| US6623700B1 (en) | 2000-11-22 | 2003-09-23 | Xerox Corporation | Level sense and control system for biofluid drop ejection devices |
| US6861034B1 (en) | 2000-11-22 | 2005-03-01 | Xerox Corporation | Priming mechanisms for drop ejection devices |
| US6893836B2 (en) * | 2000-11-29 | 2005-05-17 | Picoliter Inc. | Spatially directed ejection of cells from a carrier fluid |
| US7354141B2 (en) | 2001-12-04 | 2008-04-08 | Labcyte Inc. | Acoustic assessment of characteristics of a fluid relevant to acoustic ejection |
| US7070260B2 (en) * | 2003-01-09 | 2006-07-04 | Labcyte Inc. | Droplet dispensation from a reservoir with reduction in uncontrolled electrostatic charge |
| JP2007533647A (ja) * | 2003-10-24 | 2007-11-22 | アルザ・コーポレーシヨン | 脂質粒子の調製 |
| JP4786865B2 (ja) * | 2003-12-26 | 2011-10-05 | 関西ペイント株式会社 | 重合体膜および重合体膜の製造方法 |
| JP2005187769A (ja) * | 2003-12-26 | 2005-07-14 | Kansai Paint Co Ltd | 重合体 |
| US7975547B2 (en) * | 2004-11-23 | 2011-07-12 | Drexel University | Method and apparatus for interfacial sensing |
| US20060210443A1 (en) | 2005-03-14 | 2006-09-21 | Stearns Richard G | Avoidance of bouncing and splashing in droplet-based fluid transport |
| EP1925359A1 (en) | 2006-11-22 | 2008-05-28 | Covaris, Inc. | Methods and apparatus for treating samples with acoustic energy to form particles and particulates |
| US7753636B2 (en) * | 2008-03-25 | 2010-07-13 | Hennig Emmett D | Adjustable bale mover spikes |
| EP2200214A1 (en) | 2008-12-12 | 2010-06-23 | Alcatel, Lucent | Method for simultaneously transferring two data signals, optical access network, and central station |
| PT2732078T (pt) * | 2011-07-14 | 2017-06-26 | Covaris Inc | Sistemas e processos para preparar compostos nanocristalinos utilizando energia acústica focalizada |
| US9399019B2 (en) * | 2012-05-09 | 2016-07-26 | Evonik Corporation | Polymorph compositions, methods of making, and uses thereof |
| US9195156B2 (en) * | 2013-02-25 | 2015-11-24 | Ricoh Company, Ltd. | Particulate material production method, and particulate material production apparatus |
| CN114302911A (zh) * | 2019-08-29 | 2022-04-08 | 陶氏环球技术有限责任公司 | 制备聚烯烃固体和碳固体的均匀混合物的方法 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4308547A (en) * | 1978-04-13 | 1981-12-29 | Recognition Equipment Incorporated | Liquid drop emitter |
| US5041849A (en) * | 1989-12-26 | 1991-08-20 | Xerox Corporation | Multi-discrete-phase Fresnel acoustic lenses and their application to acoustic ink printing |
| US5874029A (en) * | 1996-10-09 | 1999-02-23 | The University Of Kansas | Methods for particle micronization and nanonization by recrystallization from organic solutions sprayed into a compressed antisolvent |
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| CH588887A5 (https=) | 1974-07-19 | 1977-06-15 | Battelle Memorial Institute | |
| US3986669A (en) | 1976-03-23 | 1976-10-19 | Martner John G | Ultrasonic tubular emulsifier and atomizer apparatus and method |
| US4697195A (en) | 1985-09-16 | 1987-09-29 | Xerox Corporation | Nozzleless liquid droplet ejectors |
| US4719476A (en) | 1986-04-17 | 1988-01-12 | Xerox Corporation | Spatially addressing capillary wave droplet ejectors and the like |
| US4801411A (en) | 1986-06-05 | 1989-01-31 | Southwest Research Institute | Method and apparatus for producing monosize ceramic particles |
| US4751534A (en) | 1986-12-19 | 1988-06-14 | Xerox Corporation | Planarized printheads for acoustic printing |
| US4751530A (en) | 1986-12-19 | 1988-06-14 | Xerox Corporation | Acoustic lens arrays for ink printing |
| US4751529A (en) | 1986-12-19 | 1988-06-14 | Xerox Corporation | Microlenses for acoustic printing |
| US4797693A (en) | 1987-06-02 | 1989-01-10 | Xerox Corporation | Polychromatic acoustic ink printing |
| US4801953A (en) | 1987-06-02 | 1989-01-31 | Xerox Corporation | Perforated ink transports for acoustic ink printing |
| US4764329A (en) * | 1987-06-12 | 1988-08-16 | The United States Of American As Represented By The Secretary Of The Army | Producing explosive material in granular form |
| US4812856A (en) | 1987-10-30 | 1989-03-14 | Microfab Technologies, Inc. | Method and apparatus for dispensing a fluid with dispersed particles therein |
| GB8822228D0 (en) | 1988-09-21 | 1988-10-26 | Southern E M | Support-bound oligonucleotides |
| US5122818A (en) | 1988-12-21 | 1992-06-16 | Xerox Corporation | Acoustic ink printers having reduced focusing sensitivity |
| US5744101A (en) | 1989-06-07 | 1998-04-28 | Affymax Technologies N.V. | Photolabile nucleoside protecting groups |
| US4959674A (en) | 1989-10-03 | 1990-09-25 | Xerox Corporation | Acoustic ink printhead having reflection coating for improved ink drop ejection control |
| US5087931A (en) | 1990-05-15 | 1992-02-11 | Xerox Corporation | Pressure-equalized ink transport system for acoustic ink printers |
| US5231426A (en) | 1990-12-26 | 1993-07-27 | Xerox Corporation | Nozzleless droplet projection system |
| US5229793A (en) | 1990-12-26 | 1993-07-20 | Xerox Corporation | Liquid surface control with an applied pressure signal in acoustic ink printing |
| US5229016A (en) | 1991-08-08 | 1993-07-20 | Microfab Technologies, Inc. | Method and apparatus for dispensing spherical-shaped quantities of liquid solder |
| US6063910A (en) | 1991-11-14 | 2000-05-16 | The Trustees Of Princeton University | Preparation of protein microparticles by supercritical fluid precipitation |
| US5392064A (en) | 1991-12-19 | 1995-02-21 | Xerox Corporation | Liquid level control structure |
| US5339101A (en) | 1991-12-30 | 1994-08-16 | Xerox Corporation | Acoustic ink printhead |
| JP3259305B2 (ja) * | 1992-02-04 | 2002-02-25 | 日揮株式会社 | 均一な液滴を形成する方法 |
| US5629724A (en) | 1992-05-29 | 1997-05-13 | Xerox Corporation | Stabilization of the free surface of a liquid |
| GB9226474D0 (en) * | 1992-12-18 | 1993-02-10 | Ici Plc | Production of particulate materials |
| US5216451A (en) | 1992-12-27 | 1993-06-01 | Xerox Corporation | Surface ripple wave diffusion in apertured free ink surface level controllers for acoustic ink printers |
| US5377902A (en) | 1994-01-14 | 1995-01-03 | Microfab Technologies, Inc. | Method of making solder interconnection arrays |
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| US6015880A (en) | 1994-03-16 | 2000-01-18 | California Institute Of Technology | Method and substrate for performing multiple sequential reactions on a matrix |
| US5669971A (en) | 1994-04-06 | 1997-09-23 | Specialty Coating Systems, Inc. | Selective coating apparatus |
| DE69523815T2 (de) | 1994-05-18 | 2002-04-18 | Xerox Corp., Rochester | Akustischbeschichtung von Materialschichten |
| US5643353A (en) | 1994-05-31 | 1997-07-01 | Microfab Technologies, Inc. | Controlling depoling and aging of piezoelectric transducers |
| US5807522A (en) | 1994-06-17 | 1998-09-15 | The Board Of Trustees Of The Leland Stanford Junior University | Methods for fabricating microarrays of biological samples |
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| US5520715A (en) | 1994-07-11 | 1996-05-28 | The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration | Directional electrostatic accretion process employing acoustic droplet formation |
| US5608433A (en) | 1994-08-25 | 1997-03-04 | Xerox Corporation | Fluid application device and method of operation |
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| US5631678A (en) | 1994-12-05 | 1997-05-20 | Xerox Corporation | Acoustic printheads with optical alignment |
| JPH08254446A (ja) | 1995-03-16 | 1996-10-01 | Fujitsu Ltd | 超音波印字方法,超音波印字装置及び音響レンズの成形方法 |
| IN1996KO01040A (https=) * | 1995-06-07 | 2005-03-04 | Clarence S Freeman | |
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| US6010316A (en) | 1996-01-16 | 2000-01-04 | The Board Of Trustees Of The Leland Stanford Junior University | Acoustic micropump |
| EP0885038B1 (en) * | 1996-03-01 | 2011-06-15 | The University Of Kansas | Methods and apparatus for particle precipitation and coating using near-critical and supercritical antisolvents |
| US5808636A (en) | 1996-09-13 | 1998-09-15 | Xerox Corporation | Reduction of droplet misdirectionality in acoustic ink printing |
| US6028189A (en) | 1997-03-20 | 2000-02-22 | University Of Washington | Solvent for oligonucleotide synthesis and methods of use |
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| DE19752585B4 (de) | 1997-11-27 | 2007-06-28 | Inotech Ag | Vorrichtung und Verfahren zum Verkapseln von mikrobiellen, pflanzlichen und tierischen Zellen bzw. von biologischen und chemischen Substanzen |
| CA2345299A1 (en) | 1998-08-26 | 2000-03-09 | Superior Micropowders, Llc | Aerosol method and apparatus for making particulate products |
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| DK1173265T3 (da) | 1999-01-29 | 2006-04-10 | Bristol Myers Squibb Co | Apparat og fremgangsmåde til krystallisation med ultralydstråler |
| JP4271294B2 (ja) * | 1999-04-28 | 2009-06-03 | 旭化成ケミカルズ株式会社 | 均一粒子径を有する粒子の製造方法 |
| GB9927011D0 (en) * | 1999-11-16 | 2000-01-12 | Advanced Phytonics Ltd | Method for the production of particles |
| US6620351B2 (en) | 2000-05-24 | 2003-09-16 | Auburn University | Method of forming nanoparticles and microparticles of controllable size using supercritical fluids with enhanced mass transfer |
| GB0016002D0 (en) | 2000-06-29 | 2000-08-23 | Glaxo Group Ltd | Novel process for preparing crystalline particles |
| US6666541B2 (en) | 2000-09-25 | 2003-12-23 | Picoliter Inc. | Acoustic ejection of fluids from a plurality of reservoirs |
| AU2001293086B2 (en) * | 2000-09-25 | 2006-04-13 | Picoliter Inc. | Focused acoustic energy method and device for generating droplets of immiscible fluids |
| US20020037359A1 (en) | 2000-09-25 | 2002-03-28 | Mutz Mitchell W. | Focused acoustic energy in the preparation of peptide arrays |
| WO2002024324A2 (en) * | 2000-09-25 | 2002-03-28 | Picoliter Inc. | Focused acoustic energy in the preparation and screening of combinatorial libraries |
| US20020064809A1 (en) * | 2000-11-29 | 2002-05-30 | Mutz Mitchell W. | Focused acoustic ejection cell sorting system and method |
| US8122880B2 (en) | 2000-12-18 | 2012-02-28 | Palo Alto Research Center Incorporated | Inhaler that uses focused acoustic waves to deliver a pharmaceutical product |
| US7121275B2 (en) | 2000-12-18 | 2006-10-17 | Xerox Corporation | Method of using focused acoustic waves to deliver a pharmaceutical product |
| US6622720B2 (en) | 2000-12-18 | 2003-09-23 | Xerox Corporation | Using capillary wave driven droplets to deliver a pharmaceutical product |
| US6596206B2 (en) * | 2001-03-30 | 2003-07-22 | Picoliter Inc. | Generation of pharmaceutical agent particles using focused acoustic energy |
-
2002
- 2002-09-13 US US10/244,128 patent/US6869551B2/en not_active Expired - Lifetime
-
2003
- 2003-09-15 CA CA2498393A patent/CA2498393C/en not_active Expired - Lifetime
- 2003-09-15 AU AU2003267271A patent/AU2003267271B2/en not_active Expired
- 2003-09-15 EP EP03749743.5A patent/EP1551566B1/en not_active Expired - Lifetime
- 2003-09-15 WO PCT/US2003/029283 patent/WO2004024343A1/en not_active Ceased
- 2003-09-15 JP JP2004536598A patent/JP5220263B2/ja not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4308547A (en) * | 1978-04-13 | 1981-12-29 | Recognition Equipment Incorporated | Liquid drop emitter |
| US5041849A (en) * | 1989-12-26 | 1991-08-20 | Xerox Corporation | Multi-discrete-phase Fresnel acoustic lenses and their application to acoustic ink printing |
| US5874029A (en) * | 1996-10-09 | 1999-02-23 | The University Of Kansas | Methods for particle micronization and nanonization by recrystallization from organic solutions sprayed into a compressed antisolvent |
Also Published As
| Publication number | Publication date |
|---|---|
| JP2005538835A (ja) | 2005-12-22 |
| EP1551566A1 (en) | 2005-07-13 |
| US20030012892A1 (en) | 2003-01-16 |
| CA2498393A1 (en) | 2004-03-25 |
| WO2004024343A1 (en) | 2004-03-25 |
| EP1551566B1 (en) | 2020-07-01 |
| US6869551B2 (en) | 2005-03-22 |
| CA2498393C (en) | 2011-04-12 |
| JP5220263B2 (ja) | 2013-06-26 |
| EP1551566A4 (en) | 2011-11-09 |
| AU2003267271A1 (en) | 2004-04-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FGA | Letters patent sealed or granted (standard patent) | ||
| MK14 | Patent ceased section 143(a) (annual fees not paid) or expired |