AU2001268529A1 - Method and apparatus for rapid fat content determination - Google Patents

Method and apparatus for rapid fat content determination

Info

Publication number
AU2001268529A1
AU2001268529A1 AU2001268529A AU6852901A AU2001268529A1 AU 2001268529 A1 AU2001268529 A1 AU 2001268529A1 AU 2001268529 A AU2001268529 A AU 2001268529A AU 6852901 A AU6852901 A AU 6852901A AU 2001268529 A1 AU2001268529 A1 AU 2001268529A1
Authority
AU
Australia
Prior art keywords
sample
sample pad
pad
wrapper
fats
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
AU2001268529A
Inventor
Michael J Collins
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
CEM Corp
Original Assignee
CEM Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by CEM Corp filed Critical CEM Corp
Publication of AU2001268529A1 publication Critical patent/AU2001268529A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N24/00Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects
    • G01N24/08Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects by using nuclear magnetic resonance
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/02Food
    • G01N33/04Dairy products
    • G01N33/06Determining fat content, e.g. by butyrometer
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N5/00Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid
    • G01N5/04Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid by removing a component, e.g. by evaporation, and weighing the remainder
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01RMEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00Arrangements or instruments for measuring magnetic variables
    • G01R33/20Arrangements or instruments for measuring magnetic variables involving magnetic resonance
    • G01R33/44Arrangements or instruments for measuring magnetic variables involving magnetic resonance using nuclear magnetic resonance [NMR]
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/44Sample treatment involving radiation, e.g. heat
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N24/00Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects
    • G01N24/08Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects by using nuclear magnetic resonance
    • G01N24/081Making measurements of geologic samples, e.g. measurements of moisture, pH, porosity, permeability, tortuosity or viscosity
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N24/00Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects
    • G01N24/08Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects by using nuclear magnetic resonance
    • G01N24/085Analysis of materials for the purpose of controlling industrial production systems
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00Chemistry: analytical and immunological testing
    • Y10T436/24Nuclear magnetic resonance, electron spin resonance or other spin effects or mass spectrometry
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00Chemistry: analytical and immunological testing
    • Y10T436/25Chemistry: analytical and immunological testing including sample preparation
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00Chemistry: analytical and immunological testing
    • Y10T436/25Chemistry: analytical and immunological testing including sample preparation
    • Y10T436/2525Stabilizing or preserving

Landscapes

  • Physics & Mathematics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • High Energy & Nuclear Physics (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Investigating Or Analysing Biological Materials (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)
  • Edible Oils And Fats (AREA)
  • Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Fats And Perfumes (AREA)

Abstract

Apparatus for determining the fat and oil content of a sample comprises a pliable, porous, hydrophilic and lipophillic sample pad (63), formed of glass fibres or quartz fibres and substantially transparent to microwave radiation. The sample is placed on the sample pad which in turn is placed on a wrapper (62) of sheet material that is non-porous to fats, oils and other liquids and is free of atoms that would interfere with or mask the NMR response in said analyser of the protons in fats and oils, said wrapper being large enough to wrap said sample pad with a sample thereon but small enough to fit within the sample field portion of an NMR analyser (36) when wrapped around the sample pad. The apparatus further includes a source (20) of microwave radiation for drying the sample, a cavity (24) in wave communication with said microwave source for receiving the sample and sample pad and a balance (28) with at least its pan inside cavity for weighing the sample and sample pad.
AU2001268529A 2000-06-23 2001-06-19 Method and apparatus for rapid fat content determination Abandoned AU2001268529A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US09/603,487 US6548303B2 (en) 2000-06-23 2000-06-23 Method and apparatus for rapid fat content determination
US09/603,487 2000-06-23
PCT/US2001/019461 WO2002001186A1 (en) 2000-06-23 2001-06-19 Method and apparatus for rapid fat content determination

Publications (1)

Publication Number Publication Date
AU2001268529A1 true AU2001268529A1 (en) 2002-01-08

Family

ID=24415647

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2001268529A Abandoned AU2001268529A1 (en) 2000-06-23 2001-06-19 Method and apparatus for rapid fat content determination

Country Status (8)

Country Link
US (5) US6548303B2 (en)
EP (2) EP1295104B1 (en)
JP (1) JP4837228B2 (en)
AT (1) ATE417259T1 (en)
AU (1) AU2001268529A1 (en)
CA (1) CA2413659C (en)
DE (1) DE60136929D1 (en)
WO (1) WO2002001186A1 (en)

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ATE237798T1 (en) * 2000-05-18 2003-05-15 Precisa Instr Ag AUTOMATIC SAMPLE PREPARATION
US7927212B2 (en) * 2001-08-03 2011-04-19 Igt Player tracking communication mechanisms in a gaming machine
US7771716B2 (en) * 2001-12-07 2010-08-10 Cytori Therapeutics, Inc. Methods of using regenerative cells in the treatment of musculoskeletal disorders
AU2002951784A0 (en) * 2002-09-26 2002-10-17 Callidan Instruments Pty Ltd Moisture analyser
US7439736B2 (en) * 2002-09-27 2008-10-21 The Trustees Of Dartmouth College Imaging by magnetic resonance adsorption, elastography and tomography
GB2400440B (en) * 2003-02-13 2006-01-04 Cohen Yosef A method for measuring the energy content of food and/or beverages using nuclear magnetic resonance and a weighing device
US7307248B2 (en) * 2003-12-09 2007-12-11 Cem Corporation Method and apparatus for microwave assisted high throughput high pressure chemical synthesis
US7494814B2 (en) * 2004-07-13 2009-02-24 Separation Technology, Inc. Apparatus and method for obtaining rapid creamatocrit and caloric content values of milk
DE102004050737B4 (en) * 2004-10-19 2012-01-05 Bruker Biospin Gmbh Device for determining the fat or oil content of a sample
JP2007326977A (en) * 2006-06-08 2007-12-20 Nippon Oil Corp A-type heavy oil
US7581876B2 (en) * 2006-07-15 2009-09-01 Cem Corporation Dual energy source loss-on-drying instrument
JP5294230B2 (en) * 2007-02-23 2013-09-18 独立行政法人産業技術総合研究所 Identification and quantification method of marbling and non-invasive measuring apparatus of marbling
US9921282B2 (en) 2012-04-10 2018-03-20 Cem Corporation Method for determining fat or moisture content
RU2506571C1 (en) * 2012-08-10 2014-02-10 Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Самарский государственный аэрокосмический университет имени академика С.П. Королева (национальный исследовательский университет)" (СГАУ) Method for measuring quality of oil products
RU2506572C1 (en) * 2012-08-16 2014-02-10 Федеральное бюджетное учреждение науки Государственный научный центр прикладной микробиологии и биотехнологии (ФБУН ГНЦ ПМБ) Method to determine content of solid fat according to data of nmr-relaxation, direct method
RU2506573C1 (en) * 2012-08-16 2014-02-10 Федеральное бюджетное учреждение науки Государственный научный центр прикладной микробиологии и биотехнологии (ФБУН ГНЦ ПМБ) Method to determine content of solid fat according to data of nmr-relaxation
CN103308543B (en) * 2013-06-05 2014-04-16 浙江大学 Quick measurement method for different forms of water in sludge
CN103728197A (en) * 2014-01-07 2014-04-16 江苏长乐纤维科技有限公司 Method for detecting moisture content and oil content of fibers
US9267877B2 (en) 2014-03-12 2016-02-23 Nxgen Partners Ip, Llc System and method for making concentration measurements within a sample material using orbital angular momentum
US9500586B2 (en) 2014-07-24 2016-11-22 Nxgen Partners Ip, Llc System and method using OAM spectroscopy leveraging fractional orbital angular momentum as signature to detect materials
US9575001B2 (en) * 2014-07-24 2017-02-21 Nxgen Partners Ip, Llc System and method for detection of materials using orbital angular momentum signatures
CN105758762A (en) * 2016-03-19 2016-07-13 江阴市纤维检验所 High-accuracy testing method of oil content of polyester staple fibers
CN110049699B (en) 2016-12-08 2021-05-07 皇家飞利浦有限公司 Food processing apparatus, control device and method of operation
CN111380745B (en) * 2018-12-29 2021-05-18 中国石油大学(北京) Device and method for measuring decomposition rate of combustible ice
WO2021037913A1 (en) 2019-08-27 2021-03-04 Nanonord A/S A method of and a system for determining fat concentration in a flowable sample by nuclear magnetic resonance
CN110470566A (en) * 2019-09-02 2019-11-19 山东省食品药品检验研究院 A kind of colla corii asini cake class product determination of fat method
CN110927004A (en) * 2019-11-21 2020-03-27 中国农业科学院北京畜牧兽医研究所 Fat analyzer

Family Cites Families (38)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FI51134C (en) 1970-01-28 1976-10-11 Valio Meijerien A method for analyzing a sample containing fat and water is the so-called NMR analyzer in the receiver.
US3971434A (en) 1973-12-03 1976-07-27 Shell Oil Company Apparatus and method for oil-in-wax determination
US3966973A (en) 1974-08-26 1976-06-29 The Pillsbury Company Process for determining and controlling the moisture of food products
US4554132A (en) * 1979-03-19 1985-11-19 Cem Corporation Analytical apparatus for determining volatiles, solids, and solvent extractables in a sample
FR2480086A1 (en) * 1980-04-11 1981-10-16 Tecnal Sa PROCESS AND PLANT FOR AUTOMATICALLY MEASURING AND ADJUSTING CONTINUOUSLY THE CONTENT OF WATER, FAT, NUTRIENT MILK MATTER (PROTEINS AND LACTOSE), SALT, BUTTER AND CHEESE CAIRES
US4753889A (en) * 1982-11-29 1988-06-28 Cem Corporation Analytical method for determining volatiles, solids and solvent extractables
US4681996A (en) * 1982-12-16 1987-07-21 Cem Corporation Analytical process in which materials to be analyzed are directly and indirectly heated and dried by microwave radiation
US4566312A (en) * 1984-05-02 1986-01-28 Cem Corporation Apparatus and process for automatically determining fat contents of foods
US4651285A (en) * 1984-05-02 1987-03-17 Cem Corporation Analytical apparatus and process
US4785245A (en) 1986-09-12 1988-11-15 Engineering Measurement Company Rapid pulse NMR cut meter
US4717986A (en) 1986-10-14 1988-01-05 Raymond L. Collins, Jr. Ignitor probe having replaceable tips
USH383H (en) * 1987-05-15 1987-12-01 The United States Of America As Represented By The United States Department Of Energy Laminated magnet field coil sheath
NZ228906A (en) * 1988-04-29 1990-12-21 Du Pont Multilayer laminated structure containing microwave receptor material for browning or crispening food cooked adjacent thereto
US5066843A (en) * 1989-01-18 1991-11-19 Cem Corporation Heat resistant and light weight container for materials to be ashed, and process for manufacture thereof
DE4024161A1 (en) 1989-08-11 1991-02-14 Siemens Ag PULSE SEQUENCE FOR QUICK DETERMINATION OF IMAGES OF FAT AND WATER DISTRIBUTION IN AN EXAMINATION OBJECT BY MEANS OF THE CORE MAGNETIC RESONANCE
US5209903A (en) 1989-09-06 1993-05-11 Toa Medical Electronics, Co., Ltd. Synthetic apparatus for inspection of blood
DE3937428A1 (en) 1989-11-10 1991-05-16 Philips Patentverwaltung Nuclear spin tomography method for generating separated fat and water images and arrangement for carrying out the method
US5328577A (en) * 1989-12-27 1994-07-12 Exxon Research & Engineering Co. Upgrading of low value hydrocarbons using a hydrogen donor and microwave radiation
GB9009476D0 (en) 1990-04-27 1990-06-20 Mansfield Peter Sample mount for nmr microscopy
PT97626A (en) * 1990-05-11 1992-03-31 Goodrich Co B F PROCESS FOR IMPROVING THE THERMAL STABILITY OF POLYVINYL HALOGENETH POLYMER
US5225781A (en) 1990-08-10 1993-07-06 General Electric Company Robust decomposition of NMR images by chemical species
US5144235A (en) 1990-08-10 1992-09-01 General Electric Company Method of decomposing nmr images by chemical species
AU644518B2 (en) 1991-04-29 1993-12-09 Labsphere, Inc. Integrating sphere for diffuse reflectance and transmittance measurements and the like
US5289124A (en) * 1991-09-20 1994-02-22 Exxon Research And Engineering Company Permeability determination from NMR relaxation measurements for fluids in porous media
DE4133643C1 (en) * 1991-10-11 1992-12-03 Bruker Analytische Messtechnik Gmbh, 7512 Rheinstetten, De
US5479009A (en) 1992-09-25 1995-12-26 Labsphere, Inc. Highly efficient collection optical systems for providing light detectors such as photodetectors and the like with hemispherical fields of view
DK119092D0 (en) * 1992-09-25 1992-09-25 Aarhus Oliefabrik As SURFACE TREATMENT AGENT
US5602477A (en) 1995-02-06 1997-02-11 The Regents Of The University Of California Nuclear magnetic resonance freezing sensor
US5909119A (en) 1995-08-18 1999-06-01 Toshiba America Mri, Inc. Method and apparatus for providing separate fat and water MRI images in a single acquisition scan
US5665312A (en) 1995-11-14 1997-09-09 Coulter International Corp. Blood analysis system having blood storage, transport and automatic slide-making capabilities
US5650332A (en) 1995-11-14 1997-07-22 Coulter International Corp. Method for the preparation of microscope slides
US6005389A (en) 1996-03-15 1999-12-21 Numar Corporation Pulse sequences and interpretation techniques for NMR measurements
US5770251A (en) 1997-08-20 1998-06-23 Lever Brothers Company, Division Of Conopco, Inc Process for accurately controlling moisture or solids levels of compositions with small amounts of or no surfactant
US6092924A (en) * 1998-02-10 2000-07-25 Denver Instrument Company Microwave moisture analyzer: apparatus and method
NO311111B1 (en) * 1998-04-03 2001-10-08 Geir H Soerland Method for determining the amount of fat and water in a biological sample
US6084226A (en) 1998-04-21 2000-07-04 Cem Corporation Use of continuously variable power in microwave assisted chemistry
US6227041B1 (en) * 1998-09-17 2001-05-08 Cem Corporation Method and apparatus for measuring volatile content
US6320170B1 (en) * 1999-09-17 2001-11-20 Cem Corporation Microwave volatiles analyzer with high efficiency cavity

Also Published As

Publication number Publication date
JP2004502165A (en) 2004-01-22
CA2413659C (en) 2007-08-14
ATE417259T1 (en) 2008-12-15
US20020164806A1 (en) 2002-11-07
EP2015052A1 (en) 2009-01-14
EP1295104B1 (en) 2008-12-10
CA2413659A1 (en) 2002-01-03
US6787362B2 (en) 2004-09-07
US6548303B2 (en) 2003-04-15
US20030124728A1 (en) 2003-07-03
US7125721B2 (en) 2006-10-24
JP4837228B2 (en) 2011-12-14
US20060263900A1 (en) 2006-11-23
EP1295104A1 (en) 2003-03-26
EP2015052B1 (en) 2016-11-23
US20020146833A1 (en) 2002-10-10
US8530239B2 (en) 2013-09-10
US6548304B2 (en) 2003-04-15
US20020119575A1 (en) 2002-08-29
DE60136929D1 (en) 2009-01-22
WO2002001186A1 (en) 2002-01-03

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