AU2001219191A1 - Sol-gel method of preparing powder for use in forming glass - Google Patents

Sol-gel method of preparing powder for use in forming glass

Info

Publication number
AU2001219191A1
AU2001219191A1 AU2001219191A AU1919101A AU2001219191A1 AU 2001219191 A1 AU2001219191 A1 AU 2001219191A1 AU 2001219191 A AU2001219191 A AU 2001219191A AU 1919101 A AU1919101 A AU 1919101A AU 2001219191 A1 AU2001219191 A1 AU 2001219191A1
Authority
AU
Australia
Prior art keywords
sol
gel method
forming glass
preparing powder
preparing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
AU2001219191A
Inventor
Lauren K. Cornelius
Adam J. Ellison
Ljerka Ukrainczyk
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Corning Inc
Original Assignee
Corning Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Corning Inc filed Critical Corning Inc
Publication of AU2001219191A1 publication Critical patent/AU2001219191A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01—Manufacture of glass fibres or filaments
    • C03B37/012—Manufacture of preforms for drawing fibres or filaments
    • C03B37/014—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD]
    • C03B37/016—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD] by a liquid phase reaction process, e.g. through a gel phase
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B19/00—Other methods of shaping glass
    • C03B19/10—Forming beads
    • C03B19/1005—Forming solid beads
    • C03B19/106—Forming solid beads by chemical vapour deposition; by liquid phase reaction
    • C03B19/1065—Forming solid beads by chemical vapour deposition; by liquid phase reaction by liquid phase reactions, e.g. by means of a gel phase
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B19/00—Other methods of shaping glass
    • C03B19/12—Other methods of shaping glass by liquid-phase reaction processes
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01—Manufacture of glass fibres or filaments
    • C03B37/012—Manufacture of preforms for drawing fibres or filaments
    • C03B37/0128—Manufacture of preforms for drawing fibres or filaments starting from pulverulent glass
    • C03B37/01291—Manufacture of preforms for drawing fibres or filaments starting from pulverulent glass by progressive melting, e.g. melting glass powder during delivery to and adhering the so-formed melt to a target or preform, e.g. the Plasma Oxidation Deposition [POD] process
    • C03B37/01297—Manufacture of preforms for drawing fibres or filaments starting from pulverulent glass by progressive melting, e.g. melting glass powder during delivery to and adhering the so-formed melt to a target or preform, e.g. the Plasma Oxidation Deposition [POD] process by melting glass powder in a mould
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01—Manufacture of glass fibres or filaments
    • C03B37/012—Manufacture of preforms for drawing fibres or filaments
    • C03B37/014—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD]
    • C03B37/018—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD] by glass deposition on a glass substrate, e.g. by inside-, modified-, plasma-, or plasma modified- chemical vapour deposition [ICVD, MCVD, PCVD, PMCVD], i.e. by thin layer coating on the inside or outside of a glass tube or on a glass rod
    • C03B37/01807—Reactant delivery systems, e.g. reactant deposition burners
    • C03B37/01838—Reactant delivery systems, e.g. reactant deposition burners for delivering and depositing additional reactants as liquids or solutions, e.g. for solution doping of the deposited glass
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
    • C03C1/006—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels to produce glass through wet route
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
    • C03C1/02—Pretreated ingredients
    • C03C1/026—Pelletisation or prereacting of powdered raw materials
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C3/00—Glass compositions
    • C03C3/04—Glass compositions containing silica
    • C03C3/06—Glass compositions containing silica with more than 90% silica by weight, e.g. quartz
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2201/00—Type of glass produced
    • C03B2201/06—Doped silica-based glasses
    • C03B2201/07—Impurity concentration specified
    • C03B2201/075—Hydroxyl ion (OH)
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2201/00—Type of glass produced
    • C03B2201/06—Doped silica-based glasses
    • C03B2201/08—Doped silica-based glasses doped with boron or fluorine or other refractive index decreasing dopant
    • C03B2201/12—Doped silica-based glasses doped with boron or fluorine or other refractive index decreasing dopant doped with fluorine
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2201/00—Type of glass produced
    • C03B2201/06—Doped silica-based glasses
    • C03B2201/30—Doped silica-based glasses doped with metals, e.g. Ga, Sn, Sb, Pb or Bi
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2201/00—Type of glass produced
    • C03B2201/06—Doped silica-based glasses
    • C03B2201/30—Doped silica-based glasses doped with metals, e.g. Ga, Sn, Sb, Pb or Bi
    • C03B2201/34—Doped silica-based glasses doped with metals, e.g. Ga, Sn, Sb, Pb or Bi doped with rare earth metals, i.e. with Sc, Y or lanthanides, e.g. for laser-amplifiers
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2201/00—Type of glass produced
    • C03B2201/06—Doped silica-based glasses
    • C03B2201/30—Doped silica-based glasses doped with metals, e.g. Ga, Sn, Sb, Pb or Bi
    • C03B2201/34—Doped silica-based glasses doped with metals, e.g. Ga, Sn, Sb, Pb or Bi doped with rare earth metals, i.e. with Sc, Y or lanthanides, e.g. for laser-amplifiers
    • C03B2201/36—Doped silica-based glasses doped with metals, e.g. Ga, Sn, Sb, Pb or Bi doped with rare earth metals, i.e. with Sc, Y or lanthanides, e.g. for laser-amplifiers doped with rare earth metals and aluminium, e.g. Er-Al co-doped
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2201/00—Glass compositions
    • C03C2201/06—Doped silica-based glasses
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2201/00—Glass compositions
    • C03C2201/06—Doped silica-based glasses
    • C03C2201/08—Doped silica-based glasses containing boron or halide
    • C03C2201/12—Doped silica-based glasses containing boron or halide containing fluorine
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2201/00—Glass compositions
    • C03C2201/06—Doped silica-based glasses
    • C03C2201/30—Doped silica-based glasses containing metals
    • C03C2201/34—Doped silica-based glasses containing metals containing rare earth metals
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2201/00—Glass compositions
    • C03C2201/06—Doped silica-based glasses
    • C03C2201/30—Doped silica-based glasses containing metals
    • C03C2201/34—Doped silica-based glasses containing metals containing rare earth metals
    • C03C2201/3476—Erbium
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2203/00—Production processes
    • C03C2203/20—Wet processes, e.g. sol-gel process
    • C03C2203/26—Wet processes, e.g. sol-gel process using alkoxides
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S65/00—Glass manufacturing
    • Y10S65/901—Liquid phase reaction process

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Glass Compositions (AREA)
  • Glass Melting And Manufacturing (AREA)
  • Silicon Compounds (AREA)
AU2001219191A 2000-01-20 2000-11-16 Sol-gel method of preparing powder for use in forming glass Abandoned AU2001219191A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US09488300 2000-01-20
US09/488,300 US6360564B1 (en) 2000-01-20 2000-01-20 Sol-gel method of preparing powder for use in forming glass
PCT/US2000/031362 WO2001053223A1 (en) 2000-01-20 2000-11-16 Sol-gel method of preparing powder for use in forming glass

Publications (1)

Publication Number Publication Date
AU2001219191A1 true AU2001219191A1 (en) 2001-07-31

Family

ID=23939167

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2001219191A Abandoned AU2001219191A1 (en) 2000-01-20 2000-11-16 Sol-gel method of preparing powder for use in forming glass

Country Status (7)

Country Link
US (1) US6360564B1 (en)
EP (1) EP1254078A4 (en)
JP (1) JP2003520180A (en)
CN (1) CN1423623A (en)
AU (1) AU2001219191A1 (en)
CA (1) CA2396955A1 (en)
WO (1) WO2001053223A1 (en)

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US7003981B2 (en) * 2001-10-02 2006-02-28 University Of Southhampton Low phonon energy gain medium and related active devices
EP1441991B1 (en) * 2001-10-18 2006-02-08 Council of Scientific and Industrial Research A process of making rare earth doped optical fibre
CA2386380A1 (en) * 2002-05-27 2003-11-27 Mohammed Saad Heavy metal oxide thin film, active and passive planar waveguides and optical devices
CN100532433C (en) * 2003-03-14 2009-08-26 中央硝子株式会社 Organic-inorganic hybrid vitreous material and method for producing same
WO2004081086A1 (en) * 2003-03-14 2004-09-23 Central Glass Company, Limited Organic-inorganic hybrid vitreous material and method for producing same
US7802450B2 (en) * 2003-03-14 2010-09-28 Central Glass Company, Limited Organic-inorganic hybrid glassy materials and their production processes
ITNO20030005A1 (en) * 2003-03-21 2004-09-22 Novara Technology Srl HIGH HOMOGENEITY SiO2 GLASSES.
US20060179879A1 (en) * 2004-12-29 2006-08-17 Ellison Adam J G Adjusting expansivity in doped silica glasses
US8197782B2 (en) 2010-02-08 2012-06-12 Momentive Performance Materials Method for making high purity metal oxide particles and materials made thereof
US9249028B2 (en) 2010-02-08 2016-02-02 Momentive Performance Materials Inc. Method for making high purity metal oxide particles and materials made thereof
WO2012096279A1 (en) * 2011-01-13 2012-07-19 オリンパスメディカルシステムズ株式会社 Glass material and method for producing glass material
CN102351414B (en) * 2011-07-05 2015-07-15 华南师范大学 Method for preparing rare earth doped microstructure optical fiber
DE102014113854A1 (en) * 2014-09-24 2016-03-24 Ev Group E. Thallner Gmbh Method for producing a glass optical element
US10427970B1 (en) * 2016-10-03 2019-10-01 Owens-Brockway Glass Container Inc. Glass coatings and methods to deposit same

Family Cites Families (23)

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US4465656A (en) 1981-08-19 1984-08-14 Hughes Aircraft Company Process for preparation of water-free oxide material
US4462974A (en) 1981-08-19 1984-07-31 Hughes Aircraft Company Process for preparation of water-free oxide material
US4605428A (en) 1984-08-03 1986-08-12 At&T Bell Laboratories Sintered high-silica glass and articles comprising same
JPS6191024A (en) 1984-10-05 1986-05-09 Seiko Epson Corp Production of cylindrical silica glass
JPH066493B2 (en) * 1985-03-06 1994-01-26 住友電気工業株式会社 Method for producing low OH glass
US4810415A (en) 1985-09-24 1989-03-07 Dresser Industries, Inc. Process for manufacturing ultra pure silica and resulting encapsulated products
US4759879A (en) * 1986-01-28 1988-07-26 The United States Of America As Represented By The United States Department Of Energy Glass former composition and method for immobilizing nuclear waste using the same
US4961767A (en) * 1987-05-20 1990-10-09 Corning Incorporated Method for producing ultra-high purity, optical quality, glass articles
US4786618A (en) 1987-05-29 1988-11-22 Corning Glass Works Sol-gel method for making ultra-low expansion glass
JPH0624993B2 (en) * 1987-12-28 1994-04-06 信越石英株式会社 Quartz glass manufacturing method
JPH02172830A (en) 1988-12-26 1990-07-04 Hoya Corp Production of glass
US5071674A (en) 1989-11-30 1991-12-10 The University Of Florida Method for producing large silica sol-gels doped with inorganic and organic compounds
EP0443781A1 (en) 1990-02-23 1991-08-28 AT&T Corp. Method for doping optical fibers
EP0474158B1 (en) 1990-09-07 1995-04-19 Mitsubishi Chemical Corporation Silica glass powder and a method for its production and a silica glass body product made thereof
AU649845B2 (en) 1991-06-24 1994-06-02 Sumitomo Electric Industries, Ltd. Method for producing glass preform for optical fiber
DE4129409A1 (en) * 1991-09-04 1993-03-11 Inst Neue Mat Gemein Gmbh Prodn. of photochromic glass for optical lens, sensor and recording medium - by hydrolysis and condensation, reacting obtd. sol with silver salt soln., condensing sol to gel, drying and comminuting to fine powder, etc.
FR2689879B1 (en) 1992-04-08 1994-10-07 France Telecom Process for the synthesis of fluoride glass by sol-gel and optical fiber carried out in the fluoride glass obtained according to this process.
FR2693451B1 (en) * 1992-07-07 1994-08-19 Alcatel Nv Method of manufacturing a silica powder and application of such a powder to the production of a preform for optical fiber.
JPH06183769A (en) * 1992-12-18 1994-07-05 Showa Electric Wire & Cable Co Ltd Production of functional optical fiber rod
US6131409A (en) * 1995-05-26 2000-10-17 Mitsubishi Chemical Corporation Process for producing a high purity synthetic quartz
DE19533851A1 (en) * 1995-09-13 1997-03-20 Hoechst Ag Organofunctionalized aerogels
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KR100229884B1 (en) 1997-03-10 1999-11-15 윤종용 Method for making silica glass

Also Published As

Publication number Publication date
EP1254078A1 (en) 2002-11-06
JP2003520180A (en) 2003-07-02
WO2001053223A1 (en) 2001-07-26
CN1423623A (en) 2003-06-11
EP1254078A4 (en) 2006-08-02
US6360564B1 (en) 2002-03-26
CA2396955A1 (en) 2001-07-26

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