AU1300388A - Device for nitrogen and hydrogen treatment with the aid of a catalyst - Google Patents

Device for nitrogen and hydrogen treatment with the aid of a catalyst

Info

Publication number
AU1300388A
AU1300388A AU13003/88A AU1300388A AU1300388A AU 1300388 A AU1300388 A AU 1300388A AU 13003/88 A AU13003/88 A AU 13003/88A AU 1300388 A AU1300388 A AU 1300388A AU 1300388 A AU1300388 A AU 1300388A
Authority
AU
Australia
Prior art keywords
heat exchanger
gas
catalyst bed
catalyst
aid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
AU13003/88A
Other versions
AU598111B2 (en
Inventor
Heinz Graeve
Hans-Joachim Herbort
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ThyssenKrupp Industrial Solutions AG
Original Assignee
Uhde GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Uhde GmbH filed Critical Uhde GmbH
Publication of AU1300388A publication Critical patent/AU1300388A/en
Application granted granted Critical
Publication of AU598111B2 publication Critical patent/AU598111B2/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/02—Preparation, purification or separation of ammonia
    • C01C1/04—Preparation of ammonia by synthesis in the gas phase
    • C01C1/0405—Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst
    • C01C1/0417—Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst characterised by the synthesis reactor, e.g. arrangement of catalyst beds and heat exchangers in the reactor
    • C01C1/0423—Cold wall reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/0005—Catalytic processes under superatmospheric pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0403—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal
    • B01J8/0407—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal through two or more cylindrical annular shaped beds
    • B01J8/0415—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal through two or more cylindrical annular shaped beds the beds being superimposed one above the other
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0496—Heating or cooling the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00194—Tubes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Fluid Mechanics (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Exhaust Gas Treatment By Means Of Catalyst (AREA)
  • Separation By Low-Temperature Treatments (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)
  • Electrical Discharge Machining, Electrochemical Machining, And Combined Machining (AREA)
  • Catalysts (AREA)

Abstract

The device having at least one heat exchanger (7) axially arranged concentrically in a pressure vessel (2) and a catalyst bed (5) surrounding the heat exchanger consists of an essentially centrally arranged feed bell (9) for feeding the gas to the tube bundle of the heat exchanger (7) and deflecting the gas leaving the heat exchanger tubes, so that it flows radially from the outside inwards through the first catalyst bed. In the interior of the first tube bundle heat exchanger (7), a concentric centrally located discharge tube (12) is provided for the gas which flows upwards, as viewed in the direction of gravity, around the heat exchanger tubes (7) and leaves the first catalyst bed (5), the central discharge tube (12) being provided with upper collection orifices (11) for this gas.
AU13003/88A 1987-03-26 1988-03-09 Device for nitrogen and hydrogen treatment with the aid of a catalyst Ceased AU598111B2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19873710004 DE3710004A1 (en) 1987-03-26 1987-03-26 DEVICE FOR THE CATALYTIC TREATMENT OF NITROGEN AND HYDROGEN
DE3710004 1987-03-26

Publications (2)

Publication Number Publication Date
AU1300388A true AU1300388A (en) 1988-09-29
AU598111B2 AU598111B2 (en) 1990-06-14

Family

ID=6324059

Family Applications (1)

Application Number Title Priority Date Filing Date
AU13003/88A Ceased AU598111B2 (en) 1987-03-26 1988-03-09 Device for nitrogen and hydrogen treatment with the aid of a catalyst

Country Status (12)

Country Link
EP (1) EP0285757B1 (en)
JP (1) JPH0672014B2 (en)
CN (1) CN1013574B (en)
AT (1) ATE67100T1 (en)
AU (1) AU598111B2 (en)
CA (1) CA1303824C (en)
DE (2) DE3710004A1 (en)
DK (1) DK166436B1 (en)
ES (1) ES2024559B3 (en)
FI (1) FI881443A (en)
NO (1) NO880787L (en)
ZA (1) ZA88986B (en)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0332757A3 (en) * 1987-12-24 1990-03-07 Ammonia Casale S.A. Converters for heterogeneous catalytic synthesis, particularly for ammonia and methanol, under pressure
CN1045100C (en) * 1996-12-26 1999-09-15 南京兴达石油化工科技工贸公司 Method for producing special kerosene type solvent naphtha
US6132687A (en) * 1998-05-21 2000-10-17 Kellogg Brown & Root, Inc. Horizontal ammonia converter adapted for high activity catalyst
EP2610001A1 (en) * 2011-12-27 2013-07-03 Ammonia Casale S.A. Adiabatic multi-bed catalytic converter with inter-bed cooling and a related process
CN105080434B (en) * 2014-04-18 2018-02-27 新特能源股份有限公司 A kind of catalytic reactor, system, the method for silicon tetrachloride catalytic hydrogenation
DE102016114710A1 (en) * 2016-08-09 2018-02-15 Thyssenkrupp Ag Plate heat exchanger, synthesizer and method of making a product
EP4025333A1 (en) 2019-09-03 2022-07-13 Haldor Topsøe A/S Reformer furnace with supported reformer tubes
CN115417428A (en) * 2022-06-29 2022-12-02 夏允涛 Ammonia converter

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3146778A (en) * 1962-04-26 1964-09-01 Henry A Krawiec Catheter supports
IT1041778B (en) * 1975-07-15 1980-01-10 Snam Progetti RADIAL FLOW REACTOR FOR AMMONIA SYNTHESIS WITH HIGH THERMAL LEVEL STEAM PRODUCTION
GB1574723A (en) * 1976-03-10 1980-09-10 Haldor Topsoe As Apparatus for the synthesis of ammonia
US4346060A (en) * 1978-07-17 1982-08-24 Pullman Incorporated Radial ammonia converters
US4341737A (en) * 1979-05-22 1982-07-27 The Lummus Company Apparatus for carrying out catalytic exothermic and endothermic high-pressure gas reactions
US4372920A (en) * 1979-07-13 1983-02-08 Ammonia Casale S.A. Axial-radial reactor for heterogeneous synthesis
IT1141102B (en) * 1980-11-28 1986-10-01 Ammonia Casale Sa AXIAL-RADIAL REACTOR FOR HETEROGENEOUS SYNTHESIS
DE3343114C2 (en) * 1983-11-29 1985-11-07 Uhde Gmbh, 4600 Dortmund Device for carrying out exothermic, catalytic gas reactions for ammonia or methanol synthesis
IN165082B (en) * 1985-05-15 1989-08-12 Ammonia Casale Sa
CH666198A5 (en) * 1985-09-13 1988-07-15 Ammonia Casale Sa REACTOR FOR CATALYTIC SYNTHESIS OF AMMONIA, METHANOL AND HIGHER ALCOHOLS.
DE3643856A1 (en) * 1986-12-22 1988-06-30 Uhde Gmbh DEVICE FOR REGULATING, IN PARTICULAR, AN AMMONIA CONVERTER

Also Published As

Publication number Publication date
DK74788A (en) 1988-09-27
FI881443A (en) 1988-09-27
DE3710004A1 (en) 1988-10-06
DE3864716D1 (en) 1991-10-17
CN1013574B (en) 1991-08-21
JPS63274612A (en) 1988-11-11
CN88101254A (en) 1988-10-19
ES2024559B3 (en) 1992-03-01
AU598111B2 (en) 1990-06-14
ZA88986B (en) 1988-08-11
CA1303824C (en) 1992-06-23
EP0285757A1 (en) 1988-10-12
NO880787L (en) 1988-09-27
EP0285757B1 (en) 1991-09-11
FI881443A0 (en) 1988-03-25
ATE67100T1 (en) 1991-09-15
DK166436B1 (en) 1993-05-24
JPH0672014B2 (en) 1994-09-14
DK74788D0 (en) 1988-02-12
NO880787D0 (en) 1988-02-23

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