ATE525127T1 - Verfahren zur veresterung mit einem wärmetauscher - Google Patents

Verfahren zur veresterung mit einem wärmetauscher

Info

Publication number
ATE525127T1
ATE525127T1 AT08858640T AT08858640T ATE525127T1 AT E525127 T1 ATE525127 T1 AT E525127T1 AT 08858640 T AT08858640 T AT 08858640T AT 08858640 T AT08858640 T AT 08858640T AT E525127 T1 ATE525127 T1 AT E525127T1
Authority
AT
Austria
Prior art keywords
esterification
heat exchanger
polyester production
producing
impurity concentration
Prior art date
Application number
AT08858640T
Other languages
English (en)
Inventor
Bruce Debruin
Richard Bonner
Original Assignee
Grupo Petrotemex Sa De Cv
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Grupo Petrotemex Sa De Cv filed Critical Grupo Petrotemex Sa De Cv
Application granted granted Critical
Publication of ATE525127T1 publication Critical patent/ATE525127T1/de

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • B01J19/2455Stationary reactors without moving elements inside provoking a loop type movement of the reactants
    • B01J19/2465Stationary reactors without moving elements inside provoking a loop type movement of the reactants externally, i.e. the mixture leaving the vessel and subsequently re-entering it
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78Preparation processes
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78Preparation processes
    • C08G63/785Preparation processes characterised by the apparatus used
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00092Tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094Jackets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00103Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18Details relating to the spatial orientation of the reactor
    • B01J2219/182Details relating to the spatial orientation of the reactor horizontal
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19Details relating to the geometry of the reactor
    • B01J2219/194Details relating to the geometry of the reactor round
    • B01J2219/1941Details relating to the geometry of the reactor round circular or disk-shaped
    • B01J2219/1943Details relating to the geometry of the reactor round circular or disk-shaped cylindrical

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
AT08858640T 2007-12-07 2008-11-21 Verfahren zur veresterung mit einem wärmetauscher ATE525127T1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US11/952,203 US7834109B2 (en) 2007-12-07 2007-12-07 System for producing low impurity polyester
PCT/US2008/013038 WO2009075722A1 (en) 2007-12-07 2008-11-21 Process for esterification comprising a heat exchanger

Publications (1)

Publication Number Publication Date
ATE525127T1 true ATE525127T1 (de) 2011-10-15

Family

ID=40409943

Family Applications (1)

Application Number Title Priority Date Filing Date
AT08858640T ATE525127T1 (de) 2007-12-07 2008-11-21 Verfahren zur veresterung mit einem wärmetauscher

Country Status (10)

Country Link
US (1) US7834109B2 (de)
EP (1) EP2222397B1 (de)
CN (1) CN101888899B (de)
AT (1) ATE525127T1 (de)
BR (1) BRPI0820364B1 (de)
CA (1) CA2706838C (de)
ES (1) ES2369122T3 (de)
MX (1) MX2010004590A (de)
PL (1) PL2222397T3 (de)
WO (1) WO2009075722A1 (de)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8431306B2 (en) 2010-03-09 2013-04-30 Xerox Corporation Polyester resin containing toner
WO2013003486A1 (en) * 2011-06-27 2013-01-03 Burton Rachel Reactor system
CN203030282U (zh) * 2013-01-28 2013-07-03 厦门巨晟机械工程有限公司 一种生产乙氧基化衍生物的装置

Family Cites Families (32)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1128657B (de) 1960-02-20 1962-04-26 Glanzstoff Ag Vorrichtung zur kontinuierlichen Polykondensation von Diolestern der Terephthalsaeure
GB1122538A (en) 1966-03-31 1968-08-07 Fischer Karl Process for the esterification of terephthalic acid with glycols
CH465875A (de) * 1966-09-16 1968-11-30 Inventa Ag Verfahren zur kontinuierlichen Herstellung von Polyestern
US3590072A (en) 1966-11-18 1971-06-29 Monsanto Co Method for direct esterification of terephthalic acid with ethylene glycol
GB1277376A (en) 1970-02-02 1972-06-14 Schwarza Chemiefaser A process and a device for the continuous esterification of di-carboxylic acids with alcohols
US3927982A (en) 1970-03-18 1975-12-23 Du Pont Recirculating apparatus for continuous esterification reactions
US3644096A (en) * 1970-03-30 1972-02-22 Eastman Kodak Co Apparatus for use in a continuous flow reaction for producing a monomer and/or a protopolymer
US4146729A (en) 1977-04-07 1979-03-27 E. I. Du Pont De Nemours And Company Process for preparing poly(ethylene terephthalate)
DE3235531A1 (de) 1982-09-25 1984-03-29 Chemische Werke Hüls AG, 4370 Marl Verfahren zur veresterung von essigsaeure mit alkoholen, die 4 und mehr c-atome enthalten, sowie mit glykolethern
US5324853A (en) 1993-01-19 1994-06-28 Exxon Chemical Patents Inc. Process for the production of plasticizer and polyolesters
US5811496A (en) 1995-12-21 1998-09-22 E.I. Du Pont De Nemours And Company Process for polymerization of polyester oligomers
TW541321B (en) 1996-09-04 2003-07-11 Hitachi Ltd Process and apparatus for continuous polycondensation
TW482790B (en) 1997-05-06 2002-04-11 Teijin Ltd Method for continuous production of polyester
WO2000048261A1 (fr) 1999-02-10 2000-08-17 Kabushiki Kaisha Toshiba Convertisseur de co et systeme de production pour pile a combustible
JP4109784B2 (ja) 1999-03-09 2008-07-02 株式会社日本触媒 蒸気分散装置を有する精製装置
DE19918728A1 (de) * 1999-04-24 2000-12-14 Bayer Ag Verfahren und Vorrichtung zum Eindampfen von Polymerlösungen thermoplastischer Polymere
BE1012945A6 (fr) * 1999-10-27 2001-06-05 Pantochim Sa Procede continu pour convertir un diester d'ether de polytetramethylene en ether glycol de polytetramethylene.
CN1322024C (zh) 2000-04-27 2007-06-20 帝人株式会社 聚酯的连续制造方法
CN1280331C (zh) * 2000-12-07 2006-10-18 伊斯曼化学公司 使用管式反应器的聚酯工艺
US6906164B2 (en) 2000-12-07 2005-06-14 Eastman Chemical Company Polyester process using a pipe reactor
DE10155419B4 (de) 2001-11-12 2005-06-16 Inventa-Fischer Gmbh & Co. Kg Verfahren zur kontinuierlichen Herstellung von hochmolekularem Polyester sowie Vorrichtung zur Durchführung des Verfahrens
US6649263B2 (en) 2001-11-16 2003-11-18 Honeywell International Inc. Polyester resin and industrial yarn process
DE10219671A1 (de) 2002-05-02 2003-11-20 Zimmer Ag Verfahren und Vorrichtung zur Herstellung von Polyestern, Copolyestern und Polycarbonaten
JP4262995B2 (ja) 2003-02-06 2009-05-13 帝人ファイバー株式会社 ポリエステル原料に適したテレフタル酸ケークの製造方法
US7074879B2 (en) 2003-06-06 2006-07-11 Eastman Chemical Company Polyester process using a pipe reactor
DE10336164B4 (de) 2003-08-07 2005-08-25 Zimmer Ag Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Polymeren durch Schmelzkondensation
DE102004034708B4 (de) 2004-07-17 2008-04-10 Lurgi Zimmer Gmbh Verfahren zur absatzweisen Herstellung von Polymeren durch Schmelzekondensation
WO2006083250A1 (en) 2005-02-03 2006-08-10 Stepan Company Continuous segmented plug flow reactor
CN1827581A (zh) * 2006-04-07 2006-09-06 华南理工大学 醋酸乙酯和醋酸丁酯的生产方法及其设备
US20080139780A1 (en) 2006-12-07 2008-06-12 Debruin Bruce Roger Polyester production system employing short residence time esterification
US7649109B2 (en) 2006-12-07 2010-01-19 Eastman Chemical Company Polyester production system employing recirculation of hot alcohol to esterification zone
US7943094B2 (en) 2006-12-07 2011-05-17 Grupo Petrotemex, S.A. De C.V. Polyester production system employing horizontally elongated esterification vessel

Also Published As

Publication number Publication date
BRPI0820364B1 (pt) 2019-03-26
CA2706838C (en) 2012-11-06
CN101888899A (zh) 2010-11-17
BRPI0820364A2 (pt) 2015-05-12
PL2222397T3 (pl) 2012-02-29
EP2222397B1 (de) 2011-09-21
EP2222397A1 (de) 2010-09-01
ES2369122T3 (es) 2011-11-25
CN101888899B (zh) 2013-06-19
MX2010004590A (es) 2010-05-13
WO2009075722A1 (en) 2009-06-18
US20090149626A1 (en) 2009-06-11
CA2706838A1 (en) 2009-06-18
US7834109B2 (en) 2010-11-16

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Legal Events

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