ATE40094T1 - PROCESS FOR THE PRODUCTION OF SILICA COLLOIDS AND SPHERICAL SILICA. - Google Patents
PROCESS FOR THE PRODUCTION OF SILICA COLLOIDS AND SPHERICAL SILICA.Info
- Publication number
- ATE40094T1 ATE40094T1 AT85401378T AT85401378T ATE40094T1 AT E40094 T1 ATE40094 T1 AT E40094T1 AT 85401378 T AT85401378 T AT 85401378T AT 85401378 T AT85401378 T AT 85401378T AT E40094 T1 ATE40094 T1 AT E40094T1
- Authority
- AT
- Austria
- Prior art keywords
- silica
- production
- colloids
- alkali metal
- solution
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
- C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
- C01B33/193—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates of aqueous solutions of silicates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
- C01B33/141—Preparation of hydrosols or aqueous dispersions
- C01B33/142—Preparation of hydrosols or aqueous dispersions by acidic treatment of silicates
- C01B33/143—Preparation of hydrosols or aqueous dispersions by acidic treatment of silicates of aqueous solutions of silicates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/30—Particle morphology extending in three dimensions
- C01P2004/32—Spheres
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
Abstract
1. A process for producing silica colloid by the reaction of a solution of an alkali metal silicate with an acidifying agent by forming a bottoms material containing an aqueous substance by the simultaneous addition of an acidifying agent and the solution of alkali metal silicate characterised by effecting said addition of the reactants at constant volume and continously drawing off the reaction medium and while maintaining a concentration of silica in the reaction medium such as to avoid the agglomeration of colloidal particles.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR8411003A FR2567504B1 (en) | 1984-07-11 | 1984-07-11 | SILICA COLLOIDS AND SPHERICAL SILICES AND METHODS FOR OBTAINING SAME |
EP85401378A EP0170578B1 (en) | 1984-07-11 | 1985-07-08 | Processes for the preparation of silica colloids and spherical silicas |
Publications (1)
Publication Number | Publication Date |
---|---|
ATE40094T1 true ATE40094T1 (en) | 1989-02-15 |
Family
ID=9306011
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AT85401378T ATE40094T1 (en) | 1984-07-11 | 1985-07-08 | PROCESS FOR THE PRODUCTION OF SILICA COLLOIDS AND SPHERICAL SILICA. |
Country Status (8)
Country | Link |
---|---|
US (1) | US5066420A (en) |
EP (1) | EP0170578B1 (en) |
JP (1) | JPS6140812A (en) |
KR (1) | KR910003970B1 (en) |
AT (1) | ATE40094T1 (en) |
CA (1) | CA1309839C (en) |
DE (1) | DE3567622D1 (en) |
FR (1) | FR2567504B1 (en) |
Families Citing this family (29)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5236623A (en) * | 1984-07-11 | 1993-08-17 | Rhone-Poulenc Chimie | Process for the production of a silica colloid |
SE500387C2 (en) * | 1989-11-09 | 1994-06-13 | Eka Nobel Ab | Silica sols, process for making silica sols and using the soles in paper making |
US5409687A (en) * | 1990-02-22 | 1995-04-25 | Vereinigte Aluminum-Werke Aktiengesellschaft | Gallosilicate catalysts and method of making same |
US5980836A (en) * | 1992-05-26 | 1999-11-09 | E. I. Du Pont De Nemours And Company | Apparatus for preparing low-concentration polyaluminosilicate microgels |
US5503820A (en) * | 1992-05-26 | 1996-04-02 | E. I. Du Pont De Nemours And Company | Method for preparing low-concentration polysilicate microgels |
US5648055A (en) * | 1992-05-26 | 1997-07-15 | E. I. Du Pont De Nemours And Company | Method for preparing low-concentration polyaluminosilicate microgels |
US5279807A (en) * | 1992-05-26 | 1994-01-18 | E. I. Du Pont De Nemours And Company | Method for preparing low-concentration polysilicate microgels |
DE4218306C2 (en) * | 1992-06-03 | 1995-06-22 | Bayer Ag | Process for the continuous production of large particulate silica sols |
US5652192A (en) * | 1992-07-10 | 1997-07-29 | Battelle Memorial Institute | Catalyst material and method of making |
SE501214C2 (en) * | 1992-08-31 | 1994-12-12 | Eka Nobel Ab | Silica sol and process for making paper using the sun |
EP0643015B1 (en) * | 1993-08-07 | 1996-09-18 | Degussa Aktiengesellschaft | Process for the preparation of precipitated silica |
US6001322A (en) * | 1993-09-29 | 1999-12-14 | Rhone-Poulenc Chimie | Precipitated silicas |
US6977065B1 (en) * | 1993-10-07 | 2005-12-20 | Degussa Ag | Precipitated silicas |
JP2908253B2 (en) * | 1994-09-26 | 1999-06-21 | 日本化学工業株式会社 | Hydrated silica and its production method |
US5571494A (en) * | 1995-01-20 | 1996-11-05 | J. M. Huber Corporation | Temperature-activated polysilicic acids |
KR100573343B1 (en) * | 1997-06-13 | 2006-04-24 | 이 아이 듀폰 디 네모아 앤드 캄파니 | Improved Method for Preparing Low-Concentration Polyaluminosilicate Microgels |
US6060523A (en) * | 1998-07-20 | 2000-05-09 | E. I. Du Pont De Nemours And Company | Continuous process for preparing microgels |
JP3785322B2 (en) * | 1999-05-04 | 2006-06-14 | アクゾ ノーベル エヌ.ブイ. | Silica-based sol |
US7169261B2 (en) | 1999-05-04 | 2007-01-30 | Akzo Nobel N.V. | Silica-based sols |
US6274112B1 (en) | 1999-12-08 | 2001-08-14 | E. I. Du Pont De Nemours And Company | Continuous production of silica-based microgels |
FR2818630B1 (en) * | 2000-12-26 | 2003-10-03 | Rhodia Chimie Sa | PROCESS FOR THE PREPARATION OF SILICA SOILS |
US6857824B2 (en) * | 2001-10-18 | 2005-02-22 | Akzo Nobel N.V. | Sealing composition and its use |
FR2833937B1 (en) * | 2001-12-26 | 2004-11-12 | Rhodia Chimie Sa | SILICA WITH LOW WATER RESUME |
JP4846193B2 (en) * | 2002-07-10 | 2011-12-28 | 株式会社トクヤマ | Easily dispersible precipitated silica cake and method for producing the same |
WO2004007366A1 (en) * | 2002-07-10 | 2004-01-22 | Tokuyama Corporation | Cake of easily dispersible precipitated silica and process for producing the same |
US6972307B2 (en) * | 2003-07-29 | 2005-12-06 | The Goodyear Tire & Rubber Company | Rubber composition containing nanoscaled zinc oxide particles |
US8829064B2 (en) * | 2005-12-29 | 2014-09-09 | Polyone Corporation | Diffused light transmitter |
US8609068B2 (en) * | 2010-02-24 | 2013-12-17 | J.M. Huber Corporation | Continuous silica production process and silica product prepared from same |
US9028605B2 (en) | 2011-02-25 | 2015-05-12 | J.M. Huber Corporation | Coating compositions comprising spheroid silica or silicate |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2466842A (en) * | 1945-11-15 | 1949-04-12 | Davison Chemical Corp | Method for making silica hydrosol |
US2577485A (en) * | 1950-09-08 | 1951-12-04 | Du Pont | Process of making stable silica sols and resulting composition |
GB710015A (en) * | 1950-12-02 | 1954-06-02 | Degussa | An improved process for the production of finely divided silica |
US2731326A (en) * | 1951-08-31 | 1956-01-17 | Du Pont | Process of preparing dense amorphous silica aggregates and product |
CH341802A (en) * | 1955-02-03 | 1959-10-31 | Basf Ag | Process for the continuous production of silicic acid-containing hydrogels |
US2956957A (en) * | 1956-04-02 | 1960-10-18 | Grace W R & Co | Method for producing clear, homogeneous silica hydrosols |
GB1044019A (en) * | 1963-10-17 | 1966-09-28 | Permutit Co Ltd | Improvements relating to the production of silica sol |
DE1299617B (en) * | 1965-01-13 | 1969-07-24 | Degussa | Process for the manufacture of finely divided precipitated silica |
US3337299A (en) * | 1965-05-24 | 1967-08-22 | Jr Oliver W Burke | Silica pigments and process for producing same |
US4356107A (en) * | 1979-11-26 | 1982-10-26 | Nalco Chemical Company | Process for preparing silica sols |
JPS60191016A (en) * | 1984-03-12 | 1985-09-28 | Nippon Chem Ind Co Ltd:The | High-purity silica and its manufacture |
-
1984
- 1984-07-11 FR FR8411003A patent/FR2567504B1/en not_active Expired
-
1985
- 1985-07-08 DE DE8585401378T patent/DE3567622D1/en not_active Expired
- 1985-07-08 EP EP85401378A patent/EP0170578B1/en not_active Expired
- 1985-07-08 AT AT85401378T patent/ATE40094T1/en not_active IP Right Cessation
- 1985-07-09 CA CA000486500A patent/CA1309839C/en not_active Expired - Fee Related
- 1985-07-10 JP JP15214985A patent/JPS6140812A/en active Granted
- 1985-07-11 KR KR1019850004951A patent/KR910003970B1/en not_active IP Right Cessation
-
1987
- 1987-08-05 US US07/082,988 patent/US5066420A/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
KR860001007A (en) | 1986-02-22 |
FR2567504B1 (en) | 1989-12-29 |
FR2567504A1 (en) | 1986-01-17 |
EP0170578B1 (en) | 1989-01-18 |
US5066420A (en) | 1991-11-19 |
JPS6140812A (en) | 1986-02-27 |
DE3567622D1 (en) | 1989-02-23 |
EP0170578A1 (en) | 1986-02-05 |
KR910003970B1 (en) | 1991-06-17 |
CA1309839C (en) | 1992-11-10 |
JPH0335245B2 (en) | 1991-05-27 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
UEP | Publication of translation of european patent specification | ||
REN | Ceased due to non-payment of the annual fee |