ATE20242T1 - PROCESS FOR THE PREPARATION OF STORAGE-STABLE AQUEOUS SOLUTIONS OF MELAMINE-FORMALDEHYDE RESINS. - Google Patents
PROCESS FOR THE PREPARATION OF STORAGE-STABLE AQUEOUS SOLUTIONS OF MELAMINE-FORMALDEHYDE RESINS.Info
- Publication number
- ATE20242T1 ATE20242T1 AT81109882T AT81109882T ATE20242T1 AT E20242 T1 ATE20242 T1 AT E20242T1 AT 81109882 T AT81109882 T AT 81109882T AT 81109882 T AT81109882 T AT 81109882T AT E20242 T1 ATE20242 T1 AT E20242T1
- Authority
- AT
- Austria
- Prior art keywords
- melamine
- aqueous solutions
- formaldehyde resins
- preparation
- storage
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G12/00—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
- C08G12/02—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes
- C08G12/26—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with heterocyclic compounds
- C08G12/30—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with heterocyclic compounds with substituted triazines
- C08G12/32—Melamines
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G12/00—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
- C08G12/02—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes
- C08G12/26—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with heterocyclic compounds
- C08G12/34—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with heterocyclic compounds and acyclic or carbocyclic compounds
- C08G12/36—Ureas; Thioureas
- C08G12/38—Ureas; Thioureas and melamines
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Phenolic Resins Or Amino Resins (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
An improved process for substantially increasing the shelf-life of aqueous solutions of melamine-formaldehyde resins wherein the molar ratio of melamine to formaldehyde is from 1:1.7 to 1:3.5 by the addition of a stabilizing amount of urea after condensation, which process includes the steps of adjusting pH of the resin solution before and after the dissolution of the urea within certain narrow but easily controllable pH ranges. The properties of the resin solution can be further improved and the stabilizing effect of the addition of urea increased by adding a monohydric C1-C4 alkanol during condensation of the resin.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19803048448 DE3048448A1 (en) | 1980-12-22 | 1980-12-22 | METHOD FOR THE PRODUCTION OF STORAGE-STABLE AQUEOUS SOLUTIONS OF MELAMINE FORMALDEHYDE RESIN |
EP81109882A EP0054755B1 (en) | 1980-12-22 | 1981-11-25 | Method of preparing storage-stable aqueous melamine resin solutions |
Publications (1)
Publication Number | Publication Date |
---|---|
ATE20242T1 true ATE20242T1 (en) | 1986-06-15 |
Family
ID=6119928
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AT81109882T ATE20242T1 (en) | 1980-12-22 | 1981-11-25 | PROCESS FOR THE PREPARATION OF STORAGE-STABLE AQUEOUS SOLUTIONS OF MELAMINE-FORMALDEHYDE RESINS. |
Country Status (8)
Country | Link |
---|---|
US (1) | US4454277A (en) |
EP (1) | EP0054755B1 (en) |
AT (1) | ATE20242T1 (en) |
CA (1) | CA1191979A (en) |
DE (2) | DE3048448A1 (en) |
ES (1) | ES8300820A1 (en) |
YU (1) | YU41802B (en) |
ZA (1) | ZA818442B (en) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4605478A (en) * | 1984-07-03 | 1986-08-12 | Ppg Industries, Inc. | Cationic electrodepositable compositions containing formaldehyde scavenger |
US4560717A (en) * | 1984-07-03 | 1985-12-24 | Ppg Industries, Inc. | Cationic electrodepositable compositions containing formaldehyde scavenger |
US4806579A (en) * | 1986-01-30 | 1989-02-21 | The British Petroleum Co. P.L.C. | Polymer composites |
DE3929052A1 (en) * | 1989-09-01 | 1991-03-07 | Basf Ag | METHOD FOR PRODUCING SPHERICAL, HARD MONO- OR OLIGODISPERSE PARTICLES MELAMINE RESIN |
CN110894272B (en) * | 2019-11-04 | 2022-09-13 | 圣象实业(江苏)有限公司 | Synthesis process of melamine resin for long-storage-period impregnation |
CN112341968A (en) * | 2020-11-20 | 2021-02-09 | 江苏健坤木业有限公司 | Adhesive for routing plate and preparation method thereof |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA526114A (en) * | 1956-06-12 | D. Pollard John | Stabilized high solids melamine formaldehyde resin solutions and process for preparing the same | |
GB691053A (en) * | 1949-01-25 | 1953-05-06 | American Cyanamid Co | Improvements in or relating to the stabilization against rapid gelation of acidic, aqueous, colloidal solutions of partially polymerized unalkylated and alkylated melamine-formaldehyde condensation products |
US2640041A (en) * | 1950-03-09 | 1953-05-26 | Du Pont | Process for preparation of melamine-formaldehyde reaction products |
US2697086A (en) * | 1952-03-18 | 1954-12-14 | American Cyanamid Co | Modified melamine-formaldehyde resin and process of preparing the same |
CH342753A (en) * | 1955-09-07 | 1959-11-30 | Ciba Geigy | Process for the preparation of a stable solution of a curable condensation product from melamine, thiourea and formaldehyde |
CH362228A (en) * | 1957-11-01 | 1962-05-31 | Sueddeutsche Kalkstickstoff | Process for the production of melamine-formaldehyde resins |
GB936620A (en) * | 1959-05-19 | 1963-09-11 | Montedison Spa | Process for the production of a stable solution of melamine formaldehyde condensation products |
DE1570240C3 (en) * | 1965-02-17 | 1982-05-27 | Basf Ag, 6700 Ludwigshafen | Process for the production of impregnating resins |
DE2455420A1 (en) * | 1974-11-22 | 1976-05-26 | Lentia Gmbh | Formaldehyde-urea-melamine condensates - by initially condensing formaldehyde and urea, adding melamine, and condensing under alkaline conditions |
-
1980
- 1980-12-22 DE DE19803048448 patent/DE3048448A1/en not_active Withdrawn
-
1981
- 1981-11-25 EP EP81109882A patent/EP0054755B1/en not_active Expired
- 1981-11-25 DE DE8181109882T patent/DE3174782D1/en not_active Expired
- 1981-11-25 AT AT81109882T patent/ATE20242T1/en active
- 1981-12-04 ZA ZA818442A patent/ZA818442B/en unknown
- 1981-12-15 CA CA000392285A patent/CA1191979A/en not_active Expired
- 1981-12-21 YU YU3033/81A patent/YU41802B/en unknown
- 1981-12-21 ES ES508193A patent/ES8300820A1/en not_active Expired
-
1982
- 1982-04-05 US US06/365,126 patent/US4454277A/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
US4454277A (en) | 1984-06-12 |
EP0054755B1 (en) | 1986-06-04 |
ES508193A0 (en) | 1982-11-01 |
ZA818442B (en) | 1982-10-27 |
DE3174782D1 (en) | 1986-07-10 |
YU41802B (en) | 1987-12-31 |
EP0054755A1 (en) | 1982-06-30 |
DE3048448A1 (en) | 1982-07-22 |
YU303381A (en) | 1983-09-30 |
ES8300820A1 (en) | 1982-11-01 |
CA1191979A (en) | 1985-08-13 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
RVE | Rejection due to an opposition filed with the epo |