AT51608B - Method of fixing the anthraquinone dyes described in Patent Specification No. 47522. - Google Patents

Method of fixing the anthraquinone dyes described in Patent Specification No. 47522.

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Publication number
AT51608B
AT51608B AT51608DA AT51608B AT 51608 B AT51608 B AT 51608B AT 51608D A AT51608D A AT 51608DA AT 51608 B AT51608 B AT 51608B
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AT
Austria
Prior art keywords
sep
yellow
fixing
patent specification
dyes described
Prior art date
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German (de)
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Hoechst Ag
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Publication date
Application filed by Hoechst Ag filed Critical Hoechst Ag
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Publication of AT51608B publication Critical patent/AT51608B/en

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Description

  

   <Desc/Clms Page number 1> 
 
 EMI1.1 
 
 EMI1.2 
 

 <Desc/Clms Page number 2> 

 
 EMI2.1 
   ss. AnthrMhinonylharnatoffclorid und Anilin erhalten wird, wird mit 50 Teilen Wasser und 2 Teilen Natronlauge von 40  B@ angerührt, mit 1¸ Teilen Hydrosulfit konzentriert Pulver   versetzt und auf 80 bis 50  erwärmt, bis Lösung eingetreten ist. Diese Stammküpe wird in die   500   Teile Wasser und 10 Teile   Glaubersalz enthaltende Farbekupe   gegeben und darin Baumwolle   VJ.   Stunde lang kalt unter der Flotte   ausgefärbt,   abgequetscht und an der Luft oxydiert. Man erhält dabei   (ei gelbe klare Färbungen. Wolle   wird in ähnlicher Weise behandelt, die Färbungen   sind kräftiger   und sehr schön klar.

   In derselben Weise werden die Produkte aus ss-Anthrachinonylharnstoffchlorid + p-Toluidin, ss-Naphtylamin usw. gefärbt. 



    Beispiel III (Druckverfahren):   
 EMI2.2 
   410 et   Wasser im Wasserbade auf   500 erwärmt, bis Reduktion   eingetreten ist, dann mit
400 g Britishgum 2 : 1 und
50 g Hydrosulfit NF konz. 1 : 1 verrührt. 



  Drucken, trocknen, 10 Minuten bei. 1000 unter Ausschluss von Luft dämpfen, waschen und bei 60  seifen. 



     H e i   s piel IV (Druckverfahren) : 
 EMI2.3 
 
50 9 Hydrosulfit konz. Pulver,
410 cm3 Wasser im Wasserbade auf   500 erwärmt,   bis Reduktion eingetreten ist, dann mit
400 9   Britisbgum     2 : 1   und
50 Hydrosulfit NF konz. 1 : 1 verrührt. 



  Drucken, trocknen, 10 Minuten bei 1000 unter Ausschluss von Luft dämpfen, waschen und 
 EMI2.4 
 
 EMI2.5 
 
<tb> 
<tb> Farbstoff <SEP> Fä@bt <SEP> Wolle
<tb> aut <SEP> Baumwolle
<tb> ss <SEP> ss-Dianthrachinonylharnstoff <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> gelb <SEP> gelb
<tb> ss-&alpha;-Dianthrachinonylharnstoff <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> grüngelb <SEP> bräu@lichgelb
<tb> ss-ss-Dianthrachinonyl-1.4-Anthrachinonylend@harnstoff <SEP> (aus <SEP> 2 <SEP> Molekülen
<tb> ss-Anthrachinonylharustoffchlorid <SEP> + <SEP> 1 <SEP> :

   <SEP> 4-Diaminoanthrachinon) <SEP> . <SEP> . <SEP> . <SEP> . <SEP> rotbraun <SEP> braun
<tb> ss-ss-Dianthrachinonyl-1.5-Anthrachinonylendiharnstoff <SEP> (aus <SEP> 2 <SEP> Mulekuleu
<tb> ss-Anthrachinonylharnstoffchlorid <SEP> + <SEP> 1.5-Diaminoanthrach@non) <SEP> . <SEP> . <SEP> . <SEP> . <SEP> gelbbraun <SEP> braun
<tb> ss-ss-Diantbrachinonyl-1.8-Anthrachiuouylendiharnstoft <SEP> (aus <SEP> 2 <SEP> Molekülen
<tb> ss-Antrachino@ylharnstoffchlorid <SEP> + <SEP> 1.8-Diaminoanthrachinon@ <SEP> . <SEP> . <SEP> . <SEP> gelbbraun <SEP> braun
<tb> Phenyl-ss-Authrachiuonylharustoff <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> reingelb <SEP> reingelb
<tb> p-Tolyl-ss-Authrachinonylharnstoft <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> .

   <SEP> hellgelb <SEP> hellgelb
<tb> @-Naphtyl-ss-Anthrachinonylharnstoff <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> goldgelb <SEP> gelb
<tb> @
<tb> 




   <Desc / Clms Page number 1>
 
 EMI1.1
 
 EMI1.2
 

 <Desc / Clms Page number 2>

 
 EMI2.1
   ss. AnthrMhinonylharnatoffclorid and aniline is obtained, is mixed with 50 parts of water and 2 parts of sodium hydroxide solution of 40 B @, mixed with 1¸ parts of hydrosulfite concentrated powder and heated to 80 to 50 until solution has occurred. This stock vat is placed in the color cup containing 500 parts of water and 10 parts of Glauber's salt and cotton VJ. Dyed cold under the liquor for hours, squeezed off and oxidized in the air. This gives (egg yellow, clear dyeings. Wool is treated in a similar way, the dyeings are stronger and very clear.

   In the same way, the products of ß-anthraquinonylurea chloride + p-toluidine, ß-naphthylamine, etc. are colored.



    Example III (printing process):
 EMI2.2
   410 et water in a water bath heated to 500 until reduction has occurred, then with
400 g Britishgum 2: 1 and
50 g hydrosulfite NF conc. Stirred 1: 1.



  Print, dry, 10 minutes at. Steam 1000 in the absence of air, wash and soap at 60.



     H i s pel IV (printing process):
 EMI2.3
 
50 9 hydrosulfite conc. Powder,
410 cm3 of water in the water bath heated to 500 until reduction has occurred, then with
400 9 Britisbgum 2: 1 and
50 hydrosulfite NF conc. Stirred 1: 1.



  Print, dry, steam 10 minutes at 1000 in the absence of air, wash and
 EMI2.4
 
 EMI2.5
 
<tb>
<tb> dye <SEP> dyes <SEP> wool
<tb> aut <SEP> cotton
<tb> ss <SEP> ss-Dianthraquinonylurea <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP> yellow <SEP> yellow
<tb> ss-α-dianthraquinonylurea <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP> green yellow <SEP> brown @ light yellow
<tb> ss-ss-Dianthraquinonyl-1.4-Anthrachinonylend@urea <SEP> (from <SEP> 2 <SEP> molecules
<tb> ss-anthraquinonyl urea chloride <SEP> + <SEP> 1 <SEP>:

   <SEP> 4-diaminoanthraquinone) <SEP>. <SEP>. <SEP>. <SEP>. <SEP> red-brown <SEP> brown
<tb> ss-ss-dianthraquinonyl-1.5-anthraquinonylenediurea <SEP> (from <SEP> 2 <SEP> Mulekuleu
<tb> ss-anthraquinonylurea chloride <SEP> + <SEP> 1.5-Diaminoanthrach@non) <SEP>. <SEP>. <SEP>. <SEP>. <SEP> yellow-brown <SEP> brown
<tb> ss-ss-Diantbrachinonyl-1.8-Anthrachiuouylendiharnstoft <SEP> (from <SEP> 2 <SEP> molecules
<tb> ss-Antrachino @ ylurea chloride <SEP> + <SEP> 1.8-diaminoanthraquinone @ <SEP>. <SEP>. <SEP>. <SEP> yellow-brown <SEP> brown
<tb> Phenyl-ss-Authrachiuonylharustoff <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP> pure yellow <SEP> pure yellow
<tb> p-Tolyl-ss-Authraquinonyl urine <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>.

   <SEP> light yellow <SEP> light yellow
<tb> @ -naphthyl-ss-anthraquinonylurea <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP> golden yellow <SEP> yellow
<tb> @
<tb>

Claims (1)

EMI2.6 chinonfarbstoffe, dadurch gekennzeichnet, dass man diese Farbstoffe durch Behandlung mit alkalischen Reduktionsmitteln in Lösung bringt und die Faser aus diesen Küpen färbt, oder dass man die Faser mit Druckpasten bedruckt, die den Farbstoff oder seine Leuko- EMI2.7 EMI2.6 quinone dyes, characterized in that these dyes are brought into solution by treatment with alkaline reducing agents and the fibers are dyed from these vats, or that the fibers are printed with printing pastes which contain the dye or its leuco EMI2.7
AT51608D 1909-02-01 1909-12-18 Method of fixing the anthraquinone dyes described in Patent Specification No. 47522. AT51608B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE51608X 1909-02-01

Publications (1)

Publication Number Publication Date
AT51608B true AT51608B (en) 1912-01-10

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AT51608D AT51608B (en) 1909-02-01 1909-12-18 Method of fixing the anthraquinone dyes described in Patent Specification No. 47522.

Country Status (1)

Country Link
AT (1) AT51608B (en)

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