AT311967B - Process for the preparation of a new pyridoxine derivative - Google Patents
Process for the preparation of a new pyridoxine derivativeInfo
- Publication number
- AT311967B AT311967B AT103272A AT103272A AT311967B AT 311967 B AT311967 B AT 311967B AT 103272 A AT103272 A AT 103272A AT 103272 A AT103272 A AT 103272A AT 311967 B AT311967 B AT 311967B
- Authority
- AT
- Austria
- Prior art keywords
- preparation
- new
- pyridoxine derivative
- derivative
- pyridoxine
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/62—Oxygen or sulfur atoms
- C07D213/63—One oxygen atom
- C07D213/65—One oxygen atom attached in position 3 or 5
- C07D213/66—One oxygen atom attached in position 3 or 5 having in position 3 an oxygen atom and in each of the positions 4 and 5 a carbon atom bound to an oxygen, sulphur, or nitrogen atom, e.g. pyridoxal
- C07D213/67—2-Methyl-3-hydroxy-4,5-bis(hydroxy-methyl)pyridine, i.e. pyridoxine
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pyridine Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Description
<Desc/Clms Page number 1>
Die Patentschrift Nr. 300810 betrifft ein Verfahren zur Herstellung neuer Pyridoxinderivate der Formel
EMI1.1
in der X ein Wasserstoffatom, ein Alkali- oder Erdalkalimetall oder eine organische Base ist.
Nach dem Verfahren des Stammpatentes erfolgt die Herstellung von Verbindungen der vorstehend angegebenen Formel (Pyridoxin-a-ketoglutarat) in der Weise, dass man Lösungen von vorzugsweise äquimolekularen Mengen von Pyridoxin und cx-Ketoglutarsäure bzw. deren Derivate in einem organischen oder anorganischen Lösungsmittel mischt und das Verfahrensprodukt in bekannter Weise fällt und aus dem Lösungsmittelgemisch aufnimmt. Nach dem Verfahren des Stammpatentes ist ferner vorgesehen, dass man die Lösungen unmittelbar vor dem Mischen herstellt und als Lösungsmittel Äthanol verwendet.
Vorliegende Erfindung betrifft in Weiterbildung der Erfindung des Stammpatentes ein Verfahren zur Herstellung einer Verbindung der Formel
EMI1.2
EMI1.3
<Desc / Clms Page number 1>
Patent specification No. 300810 relates to a process for the preparation of new pyridoxine derivatives of the formula
EMI1.1
in which X is a hydrogen atom, an alkali or alkaline earth metal or an organic base.
According to the method of the parent patent, compounds of the formula given above (pyridoxine-a-ketoglutarate) are prepared in such a way that solutions of preferably equimolecular amounts of pyridoxine and cx-ketoglutaric acid or their derivatives are mixed in an organic or inorganic solvent and the process product falls in a known manner and takes up from the solvent mixture. According to the method of the parent patent, it is also provided that the solutions are prepared immediately before mixing and that ethanol is used as the solvent.
In a further development of the invention of the parent patent, the present invention relates to a method for producing a compound of the formula
EMI1.2
EMI1.3
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AT103272A AT311967B (en) | 1972-02-09 | 1972-02-09 | Process for the preparation of a new pyridoxine derivative |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AT300810D | |||
AT103272A AT311967B (en) | 1972-02-09 | 1972-02-09 | Process for the preparation of a new pyridoxine derivative |
Publications (1)
Publication Number | Publication Date |
---|---|
AT311967B true AT311967B (en) | 1973-12-10 |
Family
ID=25594657
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AT103272A AT311967B (en) | 1972-02-09 | 1972-02-09 | Process for the preparation of a new pyridoxine derivative |
Country Status (1)
Country | Link |
---|---|
AT (1) | AT311967B (en) |
-
1972
- 1972-02-09 AT AT103272A patent/AT311967B/en not_active IP Right Cessation
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
ELJ | Ceased due to non-payment of the annual fee |