AR124802A1 - Método para producir borohidruro de sodio - Google Patents
Método para producir borohidruro de sodioInfo
- Publication number
- AR124802A1 AR124802A1 ARP220100219A ARP220100219A AR124802A1 AR 124802 A1 AR124802 A1 AR 124802A1 AR P220100219 A ARP220100219 A AR P220100219A AR P220100219 A ARP220100219 A AR P220100219A AR 124802 A1 AR124802 A1 AR 124802A1
- Authority
- AR
- Argentina
- Prior art keywords
- hermetically sealed
- sealed container
- formula
- expressed
- raw material
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title 1
- 229910000033 sodium borohydride Inorganic materials 0.000 title 1
- 239000012279 sodium borohydride Substances 0.000 title 1
- 239000002994 raw material Substances 0.000 abstract 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 abstract 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 abstract 1
- 229910052782 aluminium Inorganic materials 0.000 abstract 1
- 229910021538 borax Inorganic materials 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 235000010339 sodium tetraborate Nutrition 0.000 abstract 1
- 238000003756 stirring Methods 0.000 abstract 1
- BSVBQGMMJUBVOD-UHFFFAOYSA-N trisodium borate Chemical compound [Na+].[Na+].[Na+].[O-]B([O-])[O-] BSVBQGMMJUBVOD-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B6/00—Hydrides of metals including fully or partially hydrided metals, alloys or intermetallic compounds ; Compounds containing at least one metal-hydrogen bond, e.g. (GeH3)2S, SiH GeH; Monoborane or diborane; Addition complexes thereof
- C01B6/06—Hydrides of aluminium, gallium, indium, thallium, germanium, tin, lead, arsenic, antimony, bismuth or polonium; Monoborane; Diborane; Addition complexes thereof
- C01B6/10—Monoborane; Diborane; Addition complexes thereof
- C01B6/13—Addition complexes of monoborane or diborane, e.g. with phosphine, arsine or hydrazine
- C01B6/15—Metal borohydrides; Addition complexes thereof
- C01B6/19—Preparation from other compounds of boron
- C01B6/21—Preparation of borohydrides of alkali metals, alkaline earth metals, magnesium or beryllium; Addition complexes thereof, e.g. LiBH4.2N2H4, NaB2H7
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/03—Particle morphology depicted by an image obtained by SEM
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Abstract
Método que comprende mezclar y hacer reaccionar al mismo tiempo borato de sodio, aluminio en polvo y un fluoruro en polvo en un recipiente sellado herméticamente relleno con hidrógeno gaseoso a una temperatura de 560ºC o menos, se agita usando un agitador presente en el recipiente sellado herméticamente, y la relación de alturas de agitación (X) expresada por la siguiente fórmula (1) es del 75% o más, donde la fórmula está expresada por un espacio mínimo (a) entre el agitador y la parte más baja del recipiente sellado herméticamente en dirección del gradiente gravitatorio, y una altura de materia prima cargada (b) cuando se carga una materia prima en dicho recipiente sellado herméticamente: X = [(b - a)/b] × 100 fórmula (1).
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2021017828 | 2021-02-05 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AR124802A1 true AR124802A1 (es) | 2023-05-03 |
Family
ID=82741308
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ARP220100219A AR124802A1 (es) | 2021-02-05 | 2022-02-03 | Método para producir borohidruro de sodio |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US20230373785A1 (es) |
| EP (1) | EP4289783A1 (es) |
| JP (1) | JPWO2022168684A1 (es) |
| CN (1) | CN116806207A (es) |
| AR (1) | AR124802A1 (es) |
| TW (1) | TWI801121B (es) |
| WO (1) | WO2022168684A1 (es) |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2809666B2 (ja) | 1989-02-17 | 1998-10-15 | 三井化学株式会社 | ナトリウムボロハイドライドの製造法 |
| US20070128509A1 (en) * | 2005-12-05 | 2007-06-07 | Zongxuan Hong | Producing sodium borohydride with high energy efficiency and recycles of by-product materials |
| JP4965589B2 (ja) * | 2008-02-26 | 2012-07-04 | ローム アンド ハース カンパニー | 水素化ホウ素化合物の製造方法 |
| CN101519188A (zh) * | 2008-02-27 | 2009-09-02 | 中国科学院金属研究所 | 一种用化学机械力学法制备硼氢化钠的方法 |
| CN102300804B (zh) * | 2009-01-27 | 2015-04-29 | H2燃料系统有限公司 | 用于制氢的方法、装置和燃料 |
| WO2015190004A1 (ja) * | 2014-06-11 | 2015-12-17 | 吉崎 敦浩 | 水素化ホウ素ナトリウムの製造方法 |
| JP6977968B2 (ja) | 2018-04-24 | 2021-12-08 | 日本軽金属株式会社 | 水素化ホウ素ナトリウムの製造方法 |
| TWI768420B (zh) * | 2019-08-06 | 2022-06-21 | 日商日本輕金屬股份有限公司 | 硼氫化鈉的製造方法 |
-
2022
- 2022-01-25 JP JP2022579472A patent/JPWO2022168684A1/ja active Pending
- 2022-01-25 CN CN202280013123.1A patent/CN116806207A/zh active Pending
- 2022-01-25 WO PCT/JP2022/002731 patent/WO2022168684A1/ja active Application Filing
- 2022-01-25 EP EP22749558.7A patent/EP4289783A1/en active Pending
- 2022-01-28 TW TW111104095A patent/TWI801121B/zh active
- 2022-02-03 AR ARP220100219A patent/AR124802A1/es unknown
-
2023
- 2023-08-01 US US18/228,784 patent/US20230373785A1/en active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| TWI801121B (zh) | 2023-05-01 |
| US20230373785A1 (en) | 2023-11-23 |
| TW202241804A (zh) | 2022-11-01 |
| EP4289783A1 (en) | 2023-12-13 |
| CN116806207A (zh) | 2023-09-26 |
| JPWO2022168684A1 (es) | 2022-08-11 |
| WO2022168684A1 (ja) | 2022-08-11 |
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