AR077798A1 - Metodo para la elaboracion de una composicion antitranspirante activa que tiene cromatograma sec que exhibe elevada intensidad de pico 4 sec - Google Patents
Metodo para la elaboracion de una composicion antitranspirante activa que tiene cromatograma sec que exhibe elevada intensidad de pico 4 secInfo
- Publication number
- AR077798A1 AR077798A1 ARP100102888A ARP100102888A AR077798A1 AR 077798 A1 AR077798 A1 AR 077798A1 AR P100102888 A ARP100102888 A AR P100102888A AR P100102888 A ARP100102888 A AR P100102888A AR 077798 A1 AR077798 A1 AR 077798A1
- Authority
- AR
- Argentina
- Prior art keywords
- sec
- aluminum
- salt solution
- preparation
- aluminum salt
- Prior art date
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q15/00—Anti-perspirants or body deodorants
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/48—Halides, with or without other cations besides aluminium
- C01F7/56—Chlorides
- C01F7/57—Basic aluminium chlorides, e.g. polyaluminium chlorides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/78—Compounds containing aluminium and two or more other elements, with the exception of oxygen and hydrogen
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G25/00—Compounds of zirconium
- C01G25/006—Compounds containing, besides zirconium, two or more other elements, with the exception of oxygen or hydrogen
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
- C01P2002/87—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by chromatography data, e.g. HPLC, gas chromatography
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Geology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Cosmetics (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
Un método para la elaboracion de las composiciones antitranspirantes activas que tienen un cromatograma SEC que exhibe una elevada intensidad de pico 4 SEC, las cuales se describen en la PCT/US2007/087145 (Publicada como WO2009/075678) y la PCT/US2008/086556 (Publicada como WO2009/076591). El método utiliza una combinacion de hidroxido de sodio con una fuente de iones calcio. Reivindicacion 1: Un método para la elaboracion de una composicion antitranspirante activa caracterizado porque comprende: i) el calentamiento de una solucion acuosa que contiene una sal de aluminio que tiene una relacion molar de aluminio a cloruro de aproximadamente 0,3:1 hasta aproximadamente 3:1, opcionalmente con un agente de regulacion, a una temperatura de aproximadamente 50sC hasta aproximadamente 100sC hasta refluir por un periodo de tiempo de aproximadamente 1 hora hasta aproximadamente 6 horas para obtener una solucion de sal de aluminio; ii) la adicion de una solucion acuosa de hidroxido de sodio para obtener una solucion de sal de aluminio que tiene una relacion molar OH:Al de aproximadamente 2:1 hasta aproximadamente 2,6:1 para obtener una solucion de sal de aluminio con pH ajustado que tiene un pH de aproximadamente 2 hasta aproximadamente 5; iii) la provision de un ion de calcio; y iv) opcionalmente la adicion de una solucion acuosa que contiene un compuesto de zirconio a la solucion de sal de aluminio con pH ajustado para obtener de esta manera una solucion de sal de aluminio-zirconio que tiene una relacion molar de aluminio a zirconio de aproximadamente 5:1 hasta aproximadamente 10:1. Reivindicacion 19: El método de acuerdo con la reivindicacion 11, caracterizado porque la composicion tiene un área de pico 4 SEC de 95 hasta 100%, ningun área de pico 3 SEC, y ningun área de pico 5 SEC de un área total de picos 1, 2, 3, 4, 5, y 6 en el cromatograma SEC.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PCT/US2009/052906 WO2011016807A1 (en) | 2009-08-06 | 2009-08-06 | Method of making an antiperspirant active composition having sec chromatogram exhibiting high sec peak 4 intensity |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AR077798A1 true AR077798A1 (es) | 2011-09-21 |
Family
ID=42101949
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ARP100102888A AR077798A1 (es) | 2009-08-06 | 2010-08-05 | Metodo para la elaboracion de una composicion antitranspirante activa que tiene cromatograma sec que exhibe elevada intensidad de pico 4 sec |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US8147810B2 (es) |
| EP (1) | EP2462061B1 (es) |
| AR (1) | AR077798A1 (es) |
| AU (1) | AU2009350958B2 (es) |
| BR (1) | BR112012002358B1 (es) |
| CA (1) | CA2769023C (es) |
| MX (1) | MX2012001239A (es) |
| RU (1) | RU2495657C1 (es) |
| WO (1) | WO2011016807A1 (es) |
| ZA (1) | ZA201200642B (es) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8961523B2 (en) * | 2007-07-13 | 2015-02-24 | K2M, Inc. | Rod reduction device and method of use |
| WO2013158077A1 (en) * | 2012-04-17 | 2013-10-24 | Colgate-Palmolive Company | Method of making an aluminum salt composition |
| WO2014143019A1 (en) | 2013-03-15 | 2014-09-18 | Colgate-Palmolive Company | Oral care compositions |
| MX2015016073A (es) | 2013-05-20 | 2016-03-21 | Unilever Nv | Metodo de fabricacion de sales antitranspirantes. |
| AU2014270473A1 (en) | 2013-05-20 | 2015-10-29 | Unilever Plc | Antiperspirant compositions |
| MX2017005488A (es) | 2014-10-27 | 2017-09-15 | Unilever Nv | Composiciones antitranspirantes anhidras. |
| MX364187B (es) | 2014-10-27 | 2019-04-16 | Unilever Nv | Composiciones antitranspirantes anhidras en aerosol. |
| US9867765B2 (en) | 2014-11-19 | 2018-01-16 | Conopco, Inc. | Antiperspirant compositions |
| EP3220878B1 (en) | 2014-11-19 | 2019-02-20 | Unilever PLC | Process of manufacture of an antiperspirant composition |
| US10682293B2 (en) | 2015-11-06 | 2020-06-16 | Conopco, Inc. | Aerosol antiperspirant product |
| ES2747499T3 (es) | 2015-11-06 | 2020-03-10 | Unilever Nv | Composiciones antitranspirantes |
Family Cites Families (40)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3979510A (en) * | 1973-11-23 | 1976-09-07 | Armour Pharmaceutical Company | Aluminum-zirconium anti-perspirant systems with complex aluminum buffers |
| US3991176A (en) * | 1973-11-23 | 1976-11-09 | Armour Pharmaceutical Company | Aluminum-zirconium anti-perspirant systems with hydroxy carboxylic compounds |
| US4900531A (en) * | 1982-06-22 | 1990-02-13 | Harry Levin | Converting a carbon preform object to a silicon carbide object |
| GB2144992A (en) | 1983-08-16 | 1985-03-20 | Gillette Co | Antiperspirants |
| US4871525A (en) | 1986-10-24 | 1989-10-03 | Westwood Chemical Corporation | Antiperspirant composition and method of preparation |
| US5358694A (en) | 1986-01-08 | 1994-10-25 | Westwood Chemical Corporation | Method for preparing basic aluminum halides and product produced therefrom |
| GB8619553D0 (en) | 1986-08-11 | 1986-09-24 | Unilever Plc | Antiperspirants |
| US5330751A (en) | 1988-04-14 | 1994-07-19 | The Gilette Company | Antiperspirant and method of making same |
| US5348720A (en) | 1988-08-17 | 1994-09-20 | The Mennen Company | Basic aluminum antiperspirant active material having enhanced activity, antiperspirant active composition containing such material, and methods for preparation of such material and composition |
| US5643558A (en) | 1994-11-02 | 1997-07-01 | The Gillette Company | Method of making polyhydric alcohol solutions of enhanced efficacy antiperspirant actives |
| US5725846A (en) | 1995-03-02 | 1998-03-10 | The Gillette Company | Clear antiperspirant stick containing dibenzylidene alditol and hydroxyalkyl cellulose |
| US6010688A (en) | 1997-06-25 | 2000-01-04 | The Gillette Company | Polyhydric alcohol stabilized antiperspirant salt solutions |
| US5997850C1 (en) | 1997-10-29 | 2001-11-27 | Colgate Palmolive Co | Antiperspirant actives and formulations made therefrom |
| US6042816A (en) * | 1998-08-19 | 2000-03-28 | The Gillette Company | Enhanced antiperspirant salts stabilized with calcium and concentrated aqueous solutions of such salts |
| US6136302A (en) | 1999-02-18 | 2000-10-24 | The Procter & Gamble Company | Process of making zirconium-aluminum antiperspirant active |
| US6149897A (en) | 1999-08-24 | 2000-11-21 | The Procter & Gamble Company | Process for making anhydrous compositions containing solubilized, enhanced antiperspirant active |
| US6375937B1 (en) | 2000-10-20 | 2002-04-23 | Colgate-Palmolive Company | Antiperspirant salts for enhanced cosmetic products |
| US6436381B1 (en) | 2000-10-25 | 2002-08-20 | The Gillette Company | Aluminum-zirconium antiperspirant salts with high peak 5 al content |
| GB0100549D0 (en) | 2001-01-09 | 2001-02-21 | Unilever Plc | Antiperspirant or deodorant compositions |
| US6342210B1 (en) | 2001-04-20 | 2002-01-29 | Colgate-Palmolive Company | Antiperspirant actives from a glass form and products made therewith |
| AU2003212794A1 (en) | 2002-01-10 | 2003-07-30 | Chemlmage Corporation | Method for detection of pathogenic microorganisms |
| US6726901B2 (en) | 2002-05-09 | 2004-04-27 | The Gillette Company | Stabilized antiperspirant compositions containing aluminum-zirconium salts with low M:Cl ratio |
| US6835373B2 (en) | 2002-07-12 | 2004-12-28 | The Procter & Gamble Company | Non-irritating antiperspirant compositions containing acidic antiperspirant active |
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| US6936242B2 (en) | 2002-11-15 | 2005-08-30 | The Gillette Company | Multi-portion antiperspirant composition |
| US20040198998A1 (en) | 2003-04-04 | 2004-10-07 | Marian Holerca | Glycine-free antiperspirant salts with betaine for enhanced cosmetic products |
| US7105691B2 (en) | 2003-06-26 | 2006-09-12 | Colgate-Palmolive Company | Aluminum / zirconium / glycine antiperspirant actives stabilized with Betaine |
| US6942850B2 (en) | 2003-08-15 | 2005-09-13 | The Gillette Company | Aqueous alcoholic antiperspirant composition containing calcium enhanced antiperspirant salt |
| US6902724B1 (en) | 2004-03-24 | 2005-06-07 | Reheis, Inc. | Enhanced efficacy basic aluminum halides, antiperspirant active compositions and methods for making |
| US7087220B2 (en) * | 2004-05-28 | 2006-08-08 | Reheis, Inc. | High pH antiperspirant compositions of enhanced efficacy |
| US8883129B2 (en) | 2005-01-13 | 2014-11-11 | The Procter & Gamble Company | Enhanced efficacy antiperspirant active |
| US7704531B2 (en) * | 2005-02-18 | 2010-04-27 | Colgate-Palmolive Company | Enhanced efficacy aluminum or aluminum-zirconium antiperspirant salt compositions containing calcium salt(s) and betaine |
| WO2006103092A1 (en) | 2005-03-31 | 2006-10-05 | Unilever Plc | Process of preparing aluminium species |
| US20060292098A1 (en) | 2005-05-19 | 2006-12-28 | Scavone Timothy A | Consumer noticeable improvement in wetness protection |
| US20070003499A1 (en) | 2005-06-30 | 2007-01-04 | The Gillette Company | Particulate enhanced efficacy antiperspirant salt with raised pH |
| US20070020211A1 (en) * | 2005-07-22 | 2007-01-25 | Reheis, Inc. | Betaine with Calcium and/or Strontium Antiperspirants |
| CL2006003116A1 (es) | 2005-11-16 | 2008-02-29 | Colgate Palmolive Co | Composicion antitranspirante que comprende al menos una sal elegida de aluminio, aluminio zirconio, una sal compleja de aluminio o una sal compleja de aluminio-zirconio, un hidroxiacido y un compuesto acido de amonio cuaternario; proceso para prepara |
| US8801909B2 (en) | 2006-01-06 | 2014-08-12 | Nextchem, Llc | Polymetal hydroxychloride processes and compositions: enhanced efficacy antiperspirant salt compositions |
| US20070196303A1 (en) | 2006-02-17 | 2007-08-23 | Reheis, Inc. | Stable buffered aluminum compositions having high hplc bands iii and iv containing calcium/strontium |
| US20100202993A1 (en) * | 2007-12-12 | 2010-08-12 | Long Pan | Antiperspirant Active Compositions Having SEC Chromatogram Exhibiting High SEC Peak 4 Intensity |
-
2009
- 2009-08-06 MX MX2012001239A patent/MX2012001239A/es active IP Right Grant
- 2009-08-06 AU AU2009350958A patent/AU2009350958B2/en not_active Ceased
- 2009-08-06 EP EP09791203.4A patent/EP2462061B1/en active Active
- 2009-08-06 CA CA2769023A patent/CA2769023C/en active Active
- 2009-08-06 RU RU2012108425/04A patent/RU2495657C1/ru active
- 2009-08-06 US US12/531,145 patent/US8147810B2/en not_active Expired - Fee Related
- 2009-08-06 BR BR112012002358-6A patent/BR112012002358B1/pt not_active IP Right Cessation
- 2009-08-06 WO PCT/US2009/052906 patent/WO2011016807A1/en active Application Filing
-
2010
- 2010-08-05 AR ARP100102888A patent/AR077798A1/es not_active Application Discontinuation
-
2012
- 2012-01-24 ZA ZA2012/00642A patent/ZA201200642B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CA2769023A1 (en) | 2011-02-10 |
| WO2011016807A1 (en) | 2011-02-10 |
| RU2012108425A (ru) | 2013-09-20 |
| EP2462061A1 (en) | 2012-06-13 |
| EP2462061B1 (en) | 2017-05-31 |
| BR112012002358A2 (pt) | 2020-08-18 |
| BR112012002358B1 (pt) | 2021-05-25 |
| AU2009350958A1 (en) | 2012-02-23 |
| MX2012001239A (es) | 2012-03-16 |
| US20110182841A1 (en) | 2011-07-28 |
| CA2769023C (en) | 2014-01-21 |
| RU2495657C1 (ru) | 2013-10-20 |
| US8147810B2 (en) | 2012-04-03 |
| AU2009350958B2 (en) | 2013-04-04 |
| ZA201200642B (en) | 2014-07-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FA | Abandonment or withdrawal |