ZA901345B - Process and apparatus for air fractionation by rectification - Google Patents

Process and apparatus for air fractionation by rectification

Info

Publication number
ZA901345B
ZA901345B ZA901345A ZA901345A ZA901345B ZA 901345 B ZA901345 B ZA 901345B ZA 901345 A ZA901345 A ZA 901345A ZA 901345 A ZA901345 A ZA 901345A ZA 901345 B ZA901345 B ZA 901345B
Authority
ZA
South Africa
Prior art keywords
rectification
air fractionation
fractionation
air
Prior art date
Application number
ZA901345A
Other languages
English (en)
Inventor
Dietrich Rottmann
Rottmann Dietrich
Original Assignee
Linde Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE19893905521 external-priority patent/DE3905521A1/de
Application filed by Linde Ag filed Critical Linde Ag
Publication of ZA901345B publication Critical patent/ZA901345B/xx

Links

Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04642Recovering noble gases from air
    • F25J3/04648Recovering noble gases from air argon
    • F25J3/04654Producing crude argon in a crude argon column
    • F25J3/04666Producing crude argon in a crude argon column as a parallel working rectification column of the low pressure column in a dual pressure main column system
    • F25J3/04672Producing crude argon in a crude argon column as a parallel working rectification column of the low pressure column in a dual pressure main column system having a top condenser
    • F25J3/04678Producing crude argon in a crude argon column as a parallel working rectification column of the low pressure column in a dual pressure main column system having a top condenser cooled by oxygen enriched liquid from high pressure column bottoms
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04151Purification and (pre-)cooling of the feed air; recuperative heat-exchange with product streams
    • F25J3/04187Cooling of the purified feed air by recuperative heat-exchange; Heat-exchange with product streams
    • F25J3/0423Subcooling of liquid process streams
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04284Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams
    • F25J3/04327Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams of argon or argon enriched stream
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04406Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system
    • F25J3/04412Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system in a classical double column flowsheet, i.e. with thermal coupling by a main reboiler-condenser in the bottom of low pressure respectively top of high pressure column
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04642Recovering noble gases from air
    • F25J3/04648Recovering noble gases from air argon
    • F25J3/04654Producing crude argon in a crude argon column
    • F25J3/04709Producing crude argon in a crude argon column as an auxiliary column system in at least a dual pressure main column system
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00Processes or apparatus using separation by rectification
    • F25J2200/20Processes or apparatus using separation by rectification in an elevated pressure multiple column system wherein the lowest pressure column is at a pressure well above the minimum pressure needed to overcome pressure drop to reject the products to atmosphere
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2230/00Processes or apparatus involving steps for increasing the pressure of gaseous process streams
    • F25J2230/52Processes or apparatus involving steps for increasing the pressure of gaseous process streams the fluid being oxygen enriched compared to air, e.g. "crude oxygen"
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2235/00Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams
    • F25J2235/58Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams the fluid being argon or crude argon
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2245/00Processes or apparatus involving steps for recycling of process streams
    • F25J2245/02Recycle of a stream in general, e.g. a by-pass stream
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S62/00Refrigeration
    • Y10S62/923Inert gas
    • Y10S62/924Argon

Landscapes

  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Separation By Low-Temperature Treatments (AREA)
ZA901345A 1989-02-23 1990-02-22 Process and apparatus for air fractionation by rectification ZA901345B (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19893905521 DE3905521A1 (de) 1989-02-23 1989-02-23 Verfahren und vorrichtung zur luftzerlegung durch rektifikation
US07/483,142 US5034043A (en) 1989-02-23 1990-02-22 Air separation with argon recovery

Publications (1)

Publication Number Publication Date
ZA901345B true ZA901345B (en) 1992-06-24

Family

ID=47087703

Family Applications (1)

Application Number Title Priority Date Filing Date
ZA901345A ZA901345B (en) 1989-02-23 1990-02-22 Process and apparatus for air fractionation by rectification

Country Status (6)

Country Link
US (1) US5034043A (fr)
EP (1) EP0384213B1 (fr)
JP (1) JPH02247485A (fr)
CN (1) CN1025067C (fr)
DE (1) DE59000514D1 (fr)
ZA (1) ZA901345B (fr)

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5129932A (en) * 1990-06-12 1992-07-14 Air Products And Chemicals, Inc. Cryogenic process for the separation of air to produce moderate pressure nitrogen
US5161380A (en) * 1991-08-12 1992-11-10 Union Carbide Industrial Gases Technology Corporation Cryogenic rectification system for enhanced argon production
DE4126945A1 (de) * 1991-08-14 1993-02-18 Linde Ag Verfahren zur luftzerlegung durch rektifikation
US5235816A (en) * 1991-10-10 1993-08-17 Praxair Technology, Inc. Cryogenic rectification system for producing high purity oxygen
US5207066A (en) * 1991-10-22 1993-05-04 Bova Vitaly I Method of air separation
US5255522A (en) * 1992-02-13 1993-10-26 Air Products And Chemicals, Inc. Vaporization of liquid oxygen for increased argon recovery
US5245831A (en) * 1992-02-13 1993-09-21 Air Products And Chemicals, Inc. Single heat pump cycle for increased argon recovery
US5228296A (en) * 1992-02-27 1993-07-20 Praxair Technology, Inc. Cryogenic rectification system with argon heat pump
ES2085116T3 (es) * 1992-07-20 1996-05-16 Air Prod & Chem Licuador a presion elevada.
US5275003A (en) * 1992-07-20 1994-01-04 Air Products And Chemicals, Inc. Hybrid air and nitrogen recycle liquefier
US5305611A (en) * 1992-10-23 1994-04-26 Praxair Technology, Inc. Cryogenic rectification system with thermally integrated argon column
US5311744A (en) * 1992-12-16 1994-05-17 The Boc Group, Inc. Cryogenic air separation process and apparatus
FR2699992B1 (fr) * 1992-12-30 1995-02-10 Air Liquide Procédé et installation de production d'oxygène gazeux sous pression.
US6082136A (en) * 1993-11-12 2000-07-04 Daido Hoxan Inc. Oxygen gas manufacturing equipment
US5469710A (en) * 1994-10-26 1995-11-28 Praxair Technology, Inc. Cryogenic rectification system with enhanced argon recovery
AU743283B2 (en) * 1998-04-21 2002-01-24 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Method and installation for air distillation with production of argon
FR2787562B1 (fr) * 1998-12-22 2001-02-09 Air Liquide Procede et installation de distillation d'air avec production d'argon
FR2777641B1 (fr) * 1998-04-21 2000-05-19 Air Liquide Procede et installation de distillation d'air avec production d'argon
US6318120B1 (en) * 2000-08-11 2001-11-20 L'air Liquide Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Cryogenic distillation system for air separation
EP1300640A1 (fr) * 2001-10-04 2003-04-09 Linde Aktiengesellschaft Procédé et dispositif de production d'azote ultra-pur par séparation cryogénique d'air
US7549301B2 (en) 2006-06-09 2009-06-23 Praxair Technology, Inc. Air separation method
CN100445671C (zh) * 2007-02-12 2008-12-24 庞启东 利用尾气余热的氨水吸收式制冷装置
US8448463B2 (en) * 2009-03-26 2013-05-28 Praxair Technology, Inc. Cryogenic rectification method
FR2953915B1 (fr) * 2009-12-11 2011-12-02 Air Liquide Procede et appareil de separation d'air par distillation cryogenique
CN104406364B (zh) * 2014-11-06 2016-10-05 杭州杭氧股份有限公司 一种双塔耦合的氩气回收纯化设备及氩气回收纯化方法

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3127260A (en) * 1964-03-31 Separation of air into nitrogen
US3079759A (en) * 1961-03-22 1963-03-05 Air Prod & Chem Separation of gaseous mixtures
FR2041701B1 (fr) * 1969-05-05 1974-02-01 Air Liquide
DE1922956B1 (de) * 1969-05-06 1970-11-26 Hoechst Ag Verfahren zur Erzeugung von argonfreiem Sauerstoff durch Rektifikation von Luft
IT1034545B (it) * 1975-03-26 1979-10-10 Siad Processo ed impianto per l otte nimento dell argon a partire da un processo di frazionamento dell aria
DE3436897A1 (de) * 1984-10-08 1986-04-10 Linde Ag, 6200 Wiesbaden Verfahren und vorrichtung zum betreiben einer luftzerlegungsanlage
US4756731A (en) * 1986-02-20 1988-07-12 Erickson Donald C Oxygen and argon by back-pressured distillation
EP0269342B1 (fr) * 1986-11-24 1991-06-12 The BOC Group plc Séparation de l'air
US4842625A (en) * 1988-04-29 1989-06-27 Air Products And Chemicals, Inc. Control method to maximize argon recovery from cryogenic air separation units

Also Published As

Publication number Publication date
EP0384213B1 (fr) 1992-12-02
EP0384213A3 (en) 1990-10-24
JPH02247485A (ja) 1990-10-03
CN1045172A (zh) 1990-09-05
DE59000514D1 (de) 1993-01-14
CN1025067C (zh) 1994-06-15
US5034043A (en) 1991-07-23
EP0384213A2 (fr) 1990-08-29

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