ZA872255B - Process for purifying and recovering catalyst solution contaminated during the carbonylation of methyl acetate and/or dimethylether - Google Patents

Process for purifying and recovering catalyst solution contaminated during the carbonylation of methyl acetate and/or dimethylether

Info

Publication number
ZA872255B
ZA872255B ZA872255A ZA872255A ZA872255B ZA 872255 B ZA872255 B ZA 872255B ZA 872255 A ZA872255 A ZA 872255A ZA 872255 A ZA872255 A ZA 872255A ZA 872255 B ZA872255 B ZA 872255B
Authority
ZA
South Africa
Prior art keywords
catalyst solution
ether phase
dialkylether
alkanol
dimethylether
Prior art date
Application number
ZA872255A
Other languages
English (en)
Inventor
Heinz Erpenbach
Erpenbach Heinz
Klaus Gehrmann
Gehrmann Klaus
Winfried Lork
Lork Winfried
Peter Prinz
Prinz Peter
Original Assignee
Hoechst Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst Ag filed Critical Hoechst Ag
Publication of ZA872255B publication Critical patent/ZA872255B/xx

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0234—Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds
    • B01J31/0255—Phosphorus containing compounds
    • B01J31/0267—Phosphines or phosphonium compounds, i.e. phosphorus bonded to at least one carbon atom, including e.g. sp2-hybridised phosphorus compounds such as phosphabenzene, the other atoms bonded to phosphorus being either carbon or hydrogen
    • B01J31/0268—Phosphonium compounds, i.e. phosphine with an additional hydrogen or carbon atom bonded to phosphorous so as to result in a formal positive charge on phosphorous
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0234—Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds
    • B01J31/0235—Nitrogen containing compounds
    • B01J31/0239—Quaternary ammonium compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/20—Carbonyls
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/40—Regeneration or reactivation
    • B01J31/4015—Regeneration or reactivation of catalysts containing metals
    • B01J31/4023—Regeneration or reactivation of catalysts containing metals containing iron group metals, noble metals or copper
    • B01J31/4038—Regeneration or reactivation of catalysts containing metals containing iron group metals, noble metals or copper containing noble metals
    • B01J31/4046—Regeneration or reactivation of catalysts containing metals containing iron group metals, noble metals or copper containing noble metals containing rhodium
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/54—Preparation of carboxylic acid anhydrides
    • C07C51/573—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
    • B01J2231/30—Addition reactions at carbon centres, i.e. to either C-C or C-X multiple bonds
    • B01J2231/34—Other additions, e.g. Monsanto-type carbonylations, addition to 1,2-C=X or 1,2-C-X triplebonds, additions to 1,4-C=C-C=X or 1,4-C=-C-X triple bonds with X, e.g. O, S, NH/N
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B01J2531/82—Metals of the platinum group
    • B01J2531/822—Rhodium
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
ZA872255A 1986-03-29 1987-03-27 Process for purifying and recovering catalyst solution contaminated during the carbonylation of methyl acetate and/or dimethylether ZA872255B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19863610603 DE3610603A1 (de) 1986-03-29 1986-03-29 Verfahren zur reinigung und rueckgewinnung der bei der carbonylierung von methylacetat und/oder dimethylether anfallenden verunreinigten katalysatorloesung

Publications (1)

Publication Number Publication Date
ZA872255B true ZA872255B (en) 1987-11-25

Family

ID=6297504

Family Applications (1)

Application Number Title Priority Date Filing Date
ZA872255A ZA872255B (en) 1986-03-29 1987-03-27 Process for purifying and recovering catalyst solution contaminated during the carbonylation of methyl acetate and/or dimethylether

Country Status (10)

Country Link
US (1) US4746640A (es)
EP (1) EP0240703B1 (es)
JP (1) JPS62237949A (es)
AT (1) ATE41884T1 (es)
AU (1) AU581166B2 (es)
BR (1) BR8701411A (es)
CA (1) CA1280400C (es)
DE (2) DE3610603A1 (es)
MX (1) MX169423B (es)
ZA (1) ZA872255B (es)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4952542A (en) * 1987-06-19 1990-08-28 Union Carbide Chemicals And Plastics Company Inc. Process for the production of alkylene carbonate and recovery of catalyst
DE3902515A1 (de) * 1989-01-28 1990-08-02 Hoechst Ag Verfahren zur reinigung und rueckgewinnung der bei der carbonylierung von methanol und/oder methylacetat und/oder dimethylether anfallenden verunreinigten katalysatorloesung
DE3903909A1 (de) * 1989-02-10 1990-08-16 Hoechst Ag Verfahren zur entfernung metallischer korrosionsprodukte aus einer bei der carbonylierung von methanol und/oder methylacetat und/oder dimethylether anfallenden, verunreinigten katalysatorloesung
DE3909445A1 (de) * 1989-03-22 1990-09-27 Hoechst Ag Verfahren zur reinigung und rueckgewinnung der bei der carbonylierung von methanol und/oder methylacetat und/oder dimethylether anfallenden verunreinigten katalysatorloesung
DE4210027A1 (de) * 1992-03-27 1993-09-30 Hoechst Ag Verfahren zur Rückgewinnung von Rhodium aus Rückständen von Carbonylierungsreaktionen
GB9218346D0 (en) * 1992-08-28 1992-10-14 Bp Chem Int Ltd Process
US5510524A (en) * 1995-02-21 1996-04-23 Bp Chemicals Limited Process for the production of a carboxylic acid
US5915062A (en) * 1997-07-01 1999-06-22 Lucent Technologies Inc. Low loss optical fiber reel
EP1575705A2 (en) * 2002-12-23 2005-09-21 Eastman Chemical Company Process for the recovery of phosphorus and iodine containing catalyst components

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0234656B2 (es) * 1980-11-24 1990-08-06 Eastman Kodak Co
US4364907A (en) * 1981-06-18 1982-12-21 Eastman Kodak Company Process for recovery of rhodium values
DE3134350A1 (de) * 1981-08-31 1983-03-17 Hoechst Ag, 6000 Frankfurt Verfahren zur reinigung und rueckgewinnung der bei der carbonylierung von methylacetat und/oder dimethylether anfallenden, verunreinigten katalysatorloesung
DE3134347A1 (de) * 1981-08-31 1983-03-10 Hoechst Ag, 6000 Frankfurt Verfahren zur reinigung und rueckgewinnung der bei der carbonylierung von methylacetat und/oder dimethylether anfallenden, verunreinigten katalysatorloesung
DE3320630A1 (de) * 1983-06-08 1985-02-21 Hoechst Ag, 6230 Frankfurt Verfahren zur rueckgewinnung von edelmetallen der gruppe viii des periodensystems der elemente aus der bei der carbonylierung von methylacetat und/oder dimethylether anfallenden verunreinigten katalysatorloesung
DE3515396A1 (de) * 1985-04-29 1986-10-30 Hoechst Ag, 6230 Frankfurt Verfahren zur reinigung und rueckgewinnung der bei der carbonylierung von methylacetat und/oder dimethylether anfallenden verunreinigten katalysatorloesung
US4659682A (en) * 1985-07-08 1987-04-21 The Halcon Sd Group, Inc. Recovery of noble metal values from carbonylation residues
US4650649A (en) * 1986-01-21 1987-03-17 Eastman Kodak Company Catalyst recovery process

Also Published As

Publication number Publication date
MX169423B (es) 1993-07-05
EP0240703B1 (de) 1989-04-05
ATE41884T1 (de) 1989-04-15
CA1280400C (en) 1991-02-19
DE3610603A1 (de) 1987-10-01
JPS62237949A (ja) 1987-10-17
DE3760086D1 (en) 1989-05-11
JPH0512983B2 (es) 1993-02-19
EP0240703A2 (de) 1987-10-14
EP0240703A3 (en) 1987-12-16
AU581166B2 (en) 1989-02-09
US4746640A (en) 1988-05-24
AU7073987A (en) 1987-10-01
BR8701411A (pt) 1987-12-29

Similar Documents

Publication Publication Date Title
AU576150B2 (en) Process for purifying and recovering contaminated catalyst solution obtained in the carbonylation of methyl acetate and/or dimethylether
DE3267795D1 (en) Process for the purification and recovery of the impure catalyst solution obtained in the carbonylation of methyl acetate and/or dimethyl ether
AU581166B2 (en) Process for purifying and recovering catalyst solution contaminated during the carbonylation of methyl acetate and/or dimethylether
DE3267794D1 (en) Process for the purification and recovery of the impure catalyst solution obtained in the carbonylation of methyl acetate and/or dimethyl ether
DE3270403D1 (en) Process for the purification and recovery of the impure catalyst solution obtained in the carbonylation of methyl acetate and/or dimethyl ether
CA2012567C (en) Process for purifying and recovering the contaminated catalyst solution arising in the carbonylation of methanol and/or methyl acetate and/or dimethyl ether
ATE70739T1 (de) Verfahren zur reinigung und rueckgewinnung der bei der carbonylierung von methanol und/oder methylacetat und/oder dimethylether anfallenden verunreinigten katalysatorloesung.
JP3085467B2 (ja) アセトン除去方法
ZA90965B (en) Process for removing metallic corrosion products from a contaminated catalyst solution
ATE67477T1 (de) Extraktionsverfahren zur abtrennung einer carbonsaeure aus wasserhaltiger loesung solcher saeure.