WO2023125568A1 - Aerosol producing product, preparation method therefor, and aerosol producing system - Google Patents

Aerosol producing product, preparation method therefor, and aerosol producing system Download PDF

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Publication number
WO2023125568A1
WO2023125568A1 PCT/CN2022/142490 CN2022142490W WO2023125568A1 WO 2023125568 A1 WO2023125568 A1 WO 2023125568A1 CN 2022142490 W CN2022142490 W CN 2022142490W WO 2023125568 A1 WO2023125568 A1 WO 2023125568A1
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WO
WIPO (PCT)
Prior art keywords
aerosol
forming substrate
absorbing material
infrared absorbing
generating
Prior art date
Application number
PCT/CN2022/142490
Other languages
French (fr)
Chinese (zh)
Inventor
柳胜耀
徐中立
李永海
Original Assignee
深圳市合元科技有限公司
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by 深圳市合元科技有限公司 filed Critical 深圳市合元科技有限公司
Priority to KR1020247025271A priority Critical patent/KR20240118907A/en
Publication of WO2023125568A1 publication Critical patent/WO2023125568A1/en

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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/40Constructional details, e.g. connection of cartridges and battery parts
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/20Devices using solid inhalable precursors
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/40Constructional details, e.g. connection of cartridges and battery parts
    • A24F40/46Shape or structure of electric heating means
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/50Control or monitoring
    • A24F40/51Arrangement of sensors
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/50Control or monitoring
    • A24F40/53Monitoring, e.g. fault detection
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/50Control or monitoring
    • A24F40/57Temperature control
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/70Manufacture

Definitions

  • the embodiments of the present application relate to the technical field of products, in particular to an aerosol generating product, a preparation method thereof, and an aerosol generating system.
  • Smoking articles eg, cigarettes, cigars, etc.
  • Burn tobacco during use to produce tobacco smoke.
  • Attempts have been made to replace these tobacco-burning smoking products by making products that release compounds without burning them.
  • a heating device which releases the compound by heating rather than burning the smokeable material in the article.
  • the smokeable material may be tobacco or other non-tobacco products, which may or may not contain nicotine.
  • the embodiments of the present application provide an aerosol generating product, a preparation method thereof, and an aerosol generating system.
  • the term 'aerosol-forming substrate' is used to describe a substrate which, when heated, releases volatile compounds which form an aerosol.
  • the aerosol generated by the aerosol-forming substrate of the aerosol-generating articles described herein may or may not be visible, and may include vapors (e.g., fine particles of substances that are in a gaseous state, that are Usually liquid or solid) and liquid droplets of gases and condensed vapors.
  • the terms 'upstream' and 'downstream' are used to describe the relative position of an element, or part of an element, of an aerosol-generating article with respect to the direction in which a user draws on the aerosol-generating article during its use.
  • the term 'mass fraction' refers to the percentage by mass of a substance in the total mass of a mixture.
  • Total Particulate Matter means total particulate matter.
  • Aerosol-generating articles comprise two ends: a proximal end and a distal end, through which aerosol exits the aerosol-generating article and is delivered to a user.
  • the user may draw on the proximal end to inhale the aerosol generated by the aerosol-generating article.
  • the proximal end may also be referred to as the downstream end, and is downstream of the distal end.
  • the distal end may also be referred to as the upstream end, and is upstream of the proximal end.
  • the term 'cooling element' is used to describe an element having a relatively large surface area and low resistance to draw.
  • an aerosol formed from volatile compounds released from the aerosol-forming substrate passes through and is cooled by the cooling element before being inhaled by a user.
  • the cooling element has a low-draw-resistance.
  • the aerosol-generating article is a smoking article that generates an aerosol that is inhalable directly into the lungs of the user through the mouth of the user. More preferably, the smoking article produces a nicotine-containing aerosol which is inhalable directly into the lungs of the user through the mouth of the user.
  • the aerosol-forming substrate is arranged at the upstream end of the aerosol-generating article.
  • an aerosol-generating article for use with an aerosol-generating device, comprising an outer wrapper, and an aerosol-forming substrate and infrared absorbing material confined within said outer wrapper;
  • the aerosol-forming substrate is configured to generate an aerosol for inhalation when heated
  • the infrared absorbing material is configured to absorb infrared light for radiative heating of the aerosol-forming substrate
  • the wavelength range of the absorption peak of the infrared absorbing material at least partially coincides with the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate.
  • the wavelength range of the absorption peak of the infrared absorbing material is within the wavelength range of the absorption peak of moisture in the aerosol-forming substrate; or,
  • the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate is within the wavelength range of the absorption peak of the infrared absorbing material;
  • the wavelength range of the absorption peak of the infrared absorbing material partially coincides with the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate; or,
  • the wavelength range of the absorption peak of the infrared absorbing material is exactly the same as the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate.
  • the infrared absorbing material is in at least one of the following shapes: powder, granule, pellet, chip, strand, ribbon or sheet.
  • said infrared absorbing material is disposed between said aerosol-forming substrate and said outer wrap; alternatively, said infrared absorbing material is disposed within said aerosol-forming substrate.
  • the infrared absorbing material is disposed in the aerosol-forming substrate, including the case where the infrared-absorbing material is mixed with the aerosol-forming substrate.
  • the infrared absorbing material is bonded to a part of the aerosol-forming substrate; wherein, this part of the aerosol-forming substrate is disposed close to the downstream end of the aerosol-forming substrate.
  • the infrared absorbing material is combined on part of the aerosol forming substrate, including that the infrared absorbing material is arranged between a part of the aerosol forming substrate and the outer wrapper, and the infrared absorbing material is arranged on a part of the aerosol forming substrate.
  • the aerosol-forming matrix and the like are examples of the infrared absorbing material.
  • part of the aerosol-forming substrate is disposed close to the downstream end of the aerosol-forming substrate, including the case where part of the aerosol-forming substrate forms the downstream end of the aerosol-forming substrate.
  • the infrared absorbing material includes at least one of metals, inorganic non-metals, organics, and superabsorbing materials.
  • the mass fraction of the infrared absorbing material is between 2% and 30%; preferably, between 2% and 25%. ; More preferably, between 2% and 20%; More preferably, between 2% and 15%; More preferably, between 5% and 15%.
  • suction nozzle confined within said outer wrapper, said suction nozzle being arranged downstream of said aerosol-forming substrate.
  • cooling element confined within said outer wrapper, said cooling element being disposed between said aerosol-forming substrate and said mouthpiece.
  • the suction nozzle, the cooling element, and the aerosol-forming substrate may be bounded by different outer wrappers.
  • one outer wrapper confines the aerosol-forming substrate and another outer wrapper confines the mouthpiece and cooling element, the two outer wrappers may be of the same or different materials.
  • An embodiment of the present application also provides an aerosol-generating article, including an outer wrapper, and an aerosol-forming substrate and an infrared-absorbing material confined within the outer wrapper;
  • the aerosol-forming substrate is configured to generate an aerosol for inhalation when heated
  • the infrared absorbing material is configured to absorb infrared light for radiative heating of the aerosol-forming substrate
  • the wavelength range of the absorption peak of the infrared absorbing material is between 3 ⁇ m and 5 ⁇ m.
  • An embodiment of the present application also proposes a method for preparing an aerosol-generating product, the method comprising:
  • the aerosol-generating product After mixing the aerosol-forming substrate and the infrared-absorbing material, the aerosol-generating product is prepared by conventional product technology.
  • mixing includes the pulverized mixing of the aerosol-forming matrix and the infrared absorbing material, for example: (powder, granule, pellet, fragment) aerosol-forming matrix and (powder, Mixture of infrared absorbing materials in the form of granules, pellets, and fragments; also includes the mixture of the aerosol-forming substrate and the layered form of the infrared absorbing materials, for example: (wire strip, strip or sheet) gas The mist forms a laminate of the substrate and the infrared absorbing material (in the form of threads, strips or sheets).
  • Yet another embodiment of the present application also proposes an aerosol generating system, including an aerosol generating device and the aforementioned aerosol generating product, the aerosol generating device is configured to radiate infrared rays to heat the aerosol generating product to generate aerosol.
  • the infrared rays used to radiate and heat the aerosol-forming substrate are absorbed by the infrared absorbing material.
  • the temperature of the aerosol is reduced, especially the first puff.
  • the rate of change of the TPM value has been increased, thereby improving the user's smoking experience; at the same time, after the temperature of the infrared absorbing material rises, it can be heated together and atomized to form a matrix, which improves to a certain extent Product heating efficiency.
  • Figure 1 is a schematic diagram of an aerosol-generating product provided by an embodiment of the present application.
  • Fig. 2 is a schematic diagram of the test results of the aerosol temperature of a conventional aerosol-generating product
  • Fig. 3 is a schematic diagram of the test results of the aerosol temperature of the aerosol-generating product prepared in one embodiment
  • Fig. 4 is a schematic diagram of the test results of the aerosol temperature of the aerosol-generating product prepared in another embodiment
  • Fig. 5 is a schematic diagram of an aerosol generating system proposed in an embodiment of the present application.
  • the present application proposes an aerosol-generating article for use with an aerosol-generating device, the aerosol-generating article comprising an aerosol-forming substrate which, when heated by a heating element inside the aerosol-generating device, serves to generate Inhalable mist.
  • the overall appearance of the aerosol-generating product has a vertically elongated cylindrical structure.
  • the aerosol-generating article comprises three elements arranged in a coaxial arrangement:
  • the aerosol-generating article has an opposite proximal end 41 and a distal end 42.
  • the user inserts the proximal end 41 into the mouth for suction, and the distal end 42 is arranged between the aerosol-generating article and the distal end 42.
  • the proximal end 41 is at the opposite end.
  • air passes from the distal end 42 through the aerosol-generating article to the proximal end 41 .
  • the distal end 42 of the aerosol-generating article may also be described as the upstream end of the aerosol-generating article, and the proximal end 41 of the aerosol-generating article may also be described as the downstream end of the aerosol-generating article.
  • the elements of the aerosol-generating article disposed between the proximal end 41 and the distal end 42 may be described as upstream of the proximal end 41 , or alternatively downstream of the distal end 42 .
  • the appearance of the aerosol-generating article can mimic that of a conventional smokeable cigarette.
  • the aerosol-generating article may have an outer diameter of between approximately 5 mm and 12 mm, such as between approximately 6 mm and 8 mm.
  • the overall length of the aerosol-generating article is preferably at least about 35 millimeters. More preferably, the aerosol-generating article has an overall length of at least about 40 millimeters. Even more preferably, the aerosol-generating article has an overall length of at least about 45 millimeters. Additionally or alternatively, the overall length of the aerosol-generating article is preferably less than about 80 millimeters. More preferably, the overall length of the aerosol-generating article is less than about 75 millimeters. Even more preferably, the total length of the aerosol-generating article is less than about 70 millimeters.
  • the aerosol-generating article has an overall length of from about 35 mm to about 80 mm, more preferably from about 40 mm to about 75 mm, even more preferably from about 45 mm to about 70 mm.
  • the aerosol-forming substrate 10 is disposed at the distal end 42 of the aerosol-generating article.
  • the aerosol-forming substrate 10 may comprise nicotine.
  • the nicotine-containing aerosol-forming substrate 10 may comprise a nicotine salt substrate.
  • the aerosol-forming substrate 10 may comprise a plant-based material.
  • the aerosol-forming substrate 10 preferably comprises a tobacco-containing material.
  • the aerosol-forming substrate 10 may comprise a homogenized tobacco material, which may be formed by agglomerating particulate tobacco. Alternatively or additionally, the aerosol-forming substrate 10 may comprise a tobacco-free material.
  • the aerosol-forming substrate 10 may comprise a homogenized plant-based material.
  • the aerosol-forming substrate 10 may comprise, for example, one or more of the following forms: powder, granules, pellets, chips, strands, strips or sheets.
  • the aerosol-forming substrate 10 may comprise one or more of the following materials: tobacco leaf, tobacco vein segments, reconstituted tobacco, homogenized tobacco, extruded tobacco, tobacco pulp, cast leaf tobacco, and expanded tobacco.
  • the aerosol-forming substrate 10 may comprise at least one aerosol-forming agent.
  • Aerosol-forming agent is used to describe any suitable known compound or mixture of compounds which, in use, promotes the formation of Thermal degradation at temperature.
  • Suitable aerosol formers are known in the art and include, but are not limited to: polyols such as propylene glycol, triethylene glycol, 1,3-butanediol, and glycerin; esters of polyols such as glycerol mono, di- or triacetate; and aliphatic esters of mono-, di-, or polycarboxylic acids, such as dimethyl dodecanedioate and dimethyl tetradecenoate.
  • the aerosol-forming substrate may comprise any suitable amount of an aerosol-forming agent.
  • the amount of aerosol-forming agent may be equal to or greater than 5% by dry weight of the aerosol-forming substrate, and preferably greater than 30% by weight by dry weight.
  • the aerosol former may comprise less than about 95% by dry weight.
  • the aerosol former is present in an amount up to about 55%.
  • the aerosol-forming substrate 10 may also contain tobacco or tobacco-free volatile flavoring compounds that are released upon heating of the aerosol-forming substrate 10 .
  • the aerosol-forming substrate 10 may also comprise one or more capsules comprising, for example, additional tobacco volatile flavoring compounds or non-tobacco volatile flavoring compounds, and such capsules are formed on the aerosol-forming substrate 10. May melt during heating.
  • the aerosol-forming substrate 10 may be provided on or embedded in a thermally stable carrier.
  • thermally stable carrier means a material that does not substantially degrade at temperatures to which aerosol-forming substrate 10 is typically heated (eg, from about 150°C to about 300°C).
  • the carrier may take the form of powder, granules, pellets, chips, strands, ribbons or sheets.
  • the aerosol-forming substrate 10 may be deposited on the surface of the carrier in the form of, for example, a sheet, foam, glue or paste.
  • the aerosol-forming substrate 10 may be deposited over the entire surface of the carrier, or alternatively, may be deposited in a pattern so as to provide non-uniform flavor delivery during use.
  • the cooling element 20 is arranged immediately downstream of the aerosol-forming substrate 10 and adjoins the aerosol-forming substrate 10 .
  • the volatile substances released pass along the cooling element 20 toward the proximal end 41 of the aerosol-generating article, and the volatile substances can cool down in the cooling element 20 to form Inhaled mist.
  • the cooling element 20 comprises a cavity extending along the length of the cooling element 20 . Through the above axially extending cavity, the air flow through the cooling element 20 is in the longitudinal direction without considerable radial deviation.
  • the cooling element 20 can cool the temperature of the aerosol stream drawn through the cooling element 20 by means of heat transfer. Components of the aerosol will interact with the space within the cooling element 20 and lose thermal energy.
  • the temperature of the aerosol stream may decrease by more than 10 degrees Celsius as it is drawn through the cooling element 20 . In some embodiments, the temperature of the aerosol stream may decrease by more than 25 degrees Celsius or by more than 30 degrees Celsius as it is drawn through the cooling element 20 .
  • the suction nozzle 30 is arranged immediately downstream of the cooling element 20 and adjoins the cooling element 20 .
  • the mouthpiece 30 may be a conventional cellulose acetate or polypropylene tow filter.
  • the three components described above are aligned and tightly wrapped within the outer wrapper 40 .
  • the outer wrapper 40 may be conventional cigarette paper.
  • the aerosol-generating article shown in Figure 1 is designed to be engaged with an aerosol-generating device comprising a heating element for inhalation by a user.
  • the heating element of the aerosol-generating device heats the aerosol-forming substrate 10 of the aerosol-generating article to a temperature sufficient to generate an aerosol that is drawn downstream through the aerosol-generating article and inhaled by the user. .
  • An embodiment of the present application also proposes an infrared absorbing material configured to absorb infrared rays that radiate to heat the aerosol-forming substrate 10 .
  • the absorption peak of the infrared absorbing material is correlated with the absorption peak of the moisture in the aerosol-forming substrate.
  • the infrared absorbing material absorbs the infrared rays that radiate and heat the aerosol to form the substrate 10, so that the evaporated and atomized water is reduced in a certain proportion, and the water vapor with high heat content is avoided to cause the smoker to have a burning sensation when inhaling, especially It is to reduce the temperature of the first puff of aerosol, which improves the user's inhalation experience; at the same time, after the temperature of the infrared absorbing material rises, it can be heated together and atomized to form the matrix 10, which improves the quality of the product to a certain extent. Heating efficiency.
  • the wavelength range of the absorption peak of the infrared absorbing material at least partially coincides with the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate 10 .
  • the wavelength range of the absorption peak of the infrared absorbing material is within the wavelength range of the absorption peak of the moisture in the aerosol forming substrate 10; or, the wavelength range of the absorption peak of the moisture in the aerosol forming substrate 10 is within the wavelength range of the absorption peak of the infrared absorbing material.
  • the wavelength range of the absorption peak of the infrared absorbing material partially overlaps with the wavelength range of the absorption peak of the moisture in the aerosol forming substrate 10; or, the wavelength range of the absorption peak of the infrared absorbing material is in the aerosol formation
  • the wavelength ranges of the absorption peaks of water in the matrix 10 are exactly the same.
  • the wavelength range of the absorption peak of the infrared absorbing material is between 3 ⁇ m ⁇ 5 ⁇ m.
  • the infrared absorbing material is in at least one of the following forms: powder, granules, pellets, chips, strands, ribbons, or sheets.
  • the infrared absorbing material can be arranged between the aerosol-forming substrate 10 and the outer wrapping member 40, for example, a sheet-shaped infrared-absorbing material is sandwiched between the aerosol-forming substrate 10 and the outer wrapping member 40; Within the aerosol-forming substrate 10 .
  • the numeral 11 in the figure represents the granular aerosol forming matrix
  • the numeral 12 represents the moisture in the granular aerosol forming matrix
  • the numeral 13 represents the granular aerosol Infrared absorbing material; granular infrared absorbing material mixed with a granular aerosol-forming substrate and its moisture.
  • the granular infrared-absorbing material and water absorb infrared rays of 3 ⁇ m to 5 ⁇ m together; in this way, the evaporated and atomized water is reduced in a certain proportion, avoiding the water vapor with high heat and causing the smoker to lose weight during the pumping process. Burning sensation when inhaled, especially lowering the temperature of the first puff of aerosol. At the same time, the temperature of the granular infrared absorbing material rises after absorbing radiant heat, heating and atomizing the adjacent granular aerosol forming substrate, which improves the heating efficiency of the product to a certain extent.
  • the infrared absorbing material includes at least one of metals, inorganic non-metals, organics, and superabsorbing materials.
  • metals include but not limited to copper and nickel; inorganic non-metals include but not limited to silicon carbide and graphene; organic substances include but not limited to sucrose and fibers; 5 ⁇ m infrared.
  • the mass fraction of the infrared absorbing material is between 2% and 30%; preferably, between 2% and 25%; more preferably, between Between 2% and 20%; more preferably, between 2% and 15%; more preferably, between 5% and 15%.
  • the above outer wrapper 40 is preferably made of infrared-transmitting material.
  • it is prepared by using inorganic fiber materials, specifically including one or more of hydroxyapatite fibers, silicon carbide fibers, and barium titanate fibers.
  • the above hydroxyapatite fiber, silicon carbide fiber, and barium titanate fiber are materials with excellent infrared permeability, so that when the aerosol-generating product can be heated by infrared radiation, the outer wrapper 40 generally does not absorb infrared rays , thereby effectively promoting the heating efficiency of the inner aerosol-forming substrate 10 .
  • the prepared aerosol-generating products are illustrated through specific examples below and description of the test results.
  • a plant-based material for preparing an aerosol-forming substrate eg, tobacco material.
  • Silicon carbide material can be used, wherein the mass fraction of silicon carbide material is 10%, and the particle size is 24 mesh.
  • Graphene material can also be used, wherein the mass fraction of graphene material is 10%.
  • the steps S11 and S12 can be performed in any order.
  • It can be prepared by adopting a granular product technology to obtain a granular aerosol-generating product.
  • It can also be prepared by conventional reconstituted tobacco leaf product technology (such as papermaking method, dry method, thick pulp method, rolling method, etc.) to obtain reconstituted tobacco leaf-type aerosol products.
  • conventional reconstituted tobacco leaf product technology such as papermaking method, dry method, thick pulp method, rolling method, etc.
  • the above-mentioned product technology can refer to the existing technology, for example: “Dong Gaofeng, Tian Yongfeng, Shang Shanzhai, etc. Research progress in the production process of reconstituted tobacco leaves for heat-not-burn (HnB) cigarettes [J]. Chinese Journal of Tobacco, 2020, 26(1)", the details will not be repeated here.
  • the aerosol-generating products prepared in the above examples were tested for the aerosol temperature and the rate of change of the TPM value, and the contents of the tests were compared with conventional heat-not-burn products.
  • Test purpose to test the aerosol temperature of the product when inhaled
  • Test environment ambient temperature: 25°C, relative humidity: 65RH%.
  • Test instrument K-type thermocouple is used for temperature sensor; temperature recorder: GRAPHTEC GL240; smoking machine: self-owned equipment is used.
  • Test working conditions smoke machine working condition setting: suction volume 55ml/3s, suction interval: 27s; gas mist temperature collection point setting: K-type thermocouple is arranged at the center of the end face of the product suction nozzle; data recording frequency: 10Hz, that is, record data once every 100ms.
  • the tested product includes the aerosol generating product prepared in Example 1 and Example 2 and a conventional heat-not-burn product; each test uses the same aerosol generating device. device to ensure that the heating conditions of the products are the same; multiple products of the same type can be tested to ensure the test results;
  • the tested product is a conventional heat-not-burn product, and its test results can be referred to as shown in Figure 2;
  • the tested product uses silicon carbide material as the infrared absorbing material, wherein the mass fraction of silicon carbide material is 10%, and the particle size is 24 mesh; the granular aerosol generating product prepared by adopting the granular product process, the test results can refer to Shown in accompanying drawing 3;
  • the tested product uses graphene material as the infrared absorbing material, and the mass fraction of graphene material is 10%; the reconstituted tobacco leaf-type aerosol product is prepared by the conventional reconstituted tobacco leaf-type product process, and the test results can refer to the accompanying drawings 4.
  • the abscissa in Fig. 2-Fig. 4 represents the time of collection, and the ordinate represents the corresponding temperature, and it can be seen from the test results in Fig. 2-Fig. 4 that in the conventional heat-not-burn products shown in Fig. 2 , the temperature of the first inhaled aerosol is about 55°C, compared with conventional heat-not-burn products, the aerosol generating product shown in Figure 3, the temperature of the first inhaled aerosol is about 50°C, Decrease by about 5°C; for the aerosol-generating product shown in Figure 4, the temperature of the first inhaled aerosol is about 51°C, which is about 4°C lower. Hence, the problem of burning sensation when users take the first puff is reduced.
  • Test purpose To test the change rate of TPM value of aerosol product product 1 and aerosol-generating product 2 relative to conventional heat-not-burn products.
  • aerosol product product 1 uses silicon carbide material as the infrared absorbing material, wherein the mass fraction of silicon carbide material is 10%, and the particle size is 24 meshes; a granular aerosol generating product prepared by adopting a granular product process; aerosol Product 2 is a reconstituted tobacco leaf-type aerosol product that uses graphene material as an infrared absorbing material, and the mass fraction of graphene material is 10%; it is prepared by a conventional reconstituted tobacco leaf-type product process.
  • the change rate of the TPM value of the aerosol-generating article 2 is about 6.9%.
  • the present application also proposes an aerosol generating system comprising the above aerosol generating product and a heating device, and the structure in one embodiment is shown in FIG. 5 ;
  • the heating device 200 includes a heating element 210;
  • the heating element 210 is in the shape of a tube, at least a part of which is configured to receive the chamber of the aerosol generating product 100, and the heating element 210 radiates infrared rays to the aerosol generating product 100 to further heat the aerosol generating product 100. heating.
  • the heating element 210 radiates infrared rays to the aerosol generating product 100 to further heat the aerosol generating product 100. heating.
  • the aerosol-generating article 100 reference may be made to the aforementioned content, and details are not repeated here.
  • the infrared absorbing material in the gas mist generating product 100 absorbs the infrared rays of radiation heating the gas mist forming substrate, so that the evaporated and atomized water is reduced in a certain proportion, avoiding high heat content
  • the water vapor in the smoke makes it easy for the smoker to have a burning sensation when smoking, especially reducing the temperature of the first puff of the mist, which improves the user's suction experience; at the same time, after the temperature of the infrared absorbing material rises, it can Heating together and atomizing the aerosol to form a matrix improves the heating efficiency of the product to a certain extent.

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Abstract

Provided in the present application are an aerosol producing product, a preparation method therefor and an aerosol producing system. The aerosol producing product comprises an external wrapper, and an aerosol forming substrate and an infrared absorption material which are limited in the external wrapper. The infrared absorption material is configured to absorb infrared rays used for radiation heating of the aerosol forming substrate; and the wavelength range of the absorption peak of the infrared absorption material at least partially coincides with the wavelength range of the absorption peak of moisture in the aerosol forming substrate. When the aerosol producing product is heated, the infrared absorption material absorbs the infrared rays used for radiation heating of the aerosol forming substrate. Compared with a conventional heat-not-burn product, the aerosol producing product has lowered aerosol temperature, especially lowered aerosol temperature of first vaping, and has an increased change rate of the TPM value, thus improving the vaping experience of a user. Meanwhile, after the temperature of the infrared absorption material rises, the infrared absorption material can also heat and atomize the aerosol forming substrate, thus improving the heating efficiency of the product to a certain extent.

Description

气雾产生制品及其制备方法、气雾产生系统Aerosol generating product and its preparation method, aerosol generating system
相关申请的交叉参考Cross References to Related Applications
本申请要求于2021年12月28日提交中国专利局,申请号为202111621279.1,名称为“气雾产生制品及其制备方法、气雾产生系统”的中国专利申请的优先权,其全部内容通过引用结合在本申请中。This application claims the priority of the Chinese patent application filed on December 28, 2021 with the application number 202111621279.1 entitled "Aerosol-generating articles and their preparation method, and aerosol-generating system" filed with the China Patent Office, the entire contents of which are incorporated by reference incorporated in this application.
技术领域technical field
本申请实施例涉及制品技术领域,尤其涉及一种气雾产生制品及其制备方法、气雾产生系统。The embodiments of the present application relate to the technical field of products, in particular to an aerosol generating product, a preparation method thereof, and an aerosol generating system.
背景技术Background technique
烟制品(例如,香烟、雪茄等)在使用过程中燃烧烟草以产生烟草烟雾。人们试图通过制造在不燃烧的情况下释放化合物的产品来替代这些燃烧烟草的烟制品。Smoking articles (eg, cigarettes, cigars, etc.) burn tobacco during use to produce tobacco smoke. Attempts have been made to replace these tobacco-burning smoking products by making products that release compounds without burning them.
此类产品的示例为加热装置,其通过加热而不是燃烧制品中的可抽吸材料来释放化合物。例如,该可抽吸材料可为烟草或其它非烟草产品,这些非烟草产品可包含或可不包含尼古丁。作为另一示例,存在有通过红外辐射方式对制品进行加热使其释放化合物生成气溶胶的加热装置。An example of such a product is a heating device, which releases the compound by heating rather than burning the smokeable material in the article. For example, the smokeable material may be tobacco or other non-tobacco products, which may or may not contain nicotine. As another example, there are heating devices that heat an article by means of infrared radiation to release a compound to form an aerosol.
由于红外线具有较强的穿透性,可以穿透制品的外围进入内部,使得制品内外的受热较为均匀。不利的是,这种受热均匀会使得制品中的大部分水分均受热蒸发,而含有较高热量的水蒸气使得抽吸者在抽吸时很容易产生灼痛感,尤其是在抽吸第一口时感觉更为明显。Due to the strong penetrability of infrared rays, it can penetrate the periphery of the product and enter the interior, so that the heating inside and outside of the product is relatively uniform. The disadvantage is that this kind of uniform heating will cause most of the water in the product to be heated and evaporate, and the water vapor with higher heat will make the smoker easily feel burning pain when smoking, especially at the first puff. feel more pronounced.
申请内容application content
为了解决现有制品在被红外辐射加热时易使得抽吸者在抽吸时产生灼痛感的问题,本申请实施例提供一种气雾产生制品及其制备方法、气雾产生系统。In order to solve the problem that existing products tend to cause burning pain to smokers when they are heated by infrared radiation, the embodiments of the present application provide an aerosol generating product, a preparation method thereof, and an aerosol generating system.
如这里使用的那样,术语‘气雾形成基体’用来描述能够在加热时释放易挥发化合物的基体,这些易挥发化合物可形成气雾。由这里描述的,气雾产生制品的气雾形成基体产生的气雾可以是可见的或不可见的,并且可以包括蒸气(例如,物质的细颗粒,这些颗粒处于气态下,这些 颗粒在室温下通常是液体或固体)以及气体和冷凝蒸气的液滴。As used herein, the term 'aerosol-forming substrate' is used to describe a substrate which, when heated, releases volatile compounds which form an aerosol. The aerosol generated by the aerosol-forming substrate of the aerosol-generating articles described herein may or may not be visible, and may include vapors (e.g., fine particles of substances that are in a gaseous state, that are Usually liquid or solid) and liquid droplets of gases and condensed vapors.
如这里使用的那样,术语‘上游’和‘下游’用来关于用户对气雾产生制品在其使用期间进行抽吸的方向,描述气雾产生制品的元件、或元件的部分的相对位置。As used herein, the terms 'upstream' and 'downstream' are used to describe the relative position of an element, or part of an element, of an aerosol-generating article with respect to the direction in which a user draws on the aerosol-generating article during its use.
如这里使用的那样,术语‘质量分数’指混合物中某种物质质量占总质量的百分比。As used herein, the term 'mass fraction' refers to the percentage by mass of a substance in the total mass of a mixture.
如这里使用的那样,术语‘TPM(Total Particulate Matter)’表示总粒相物。As used herein, the term 'TPM (Total Particulate Matter)' means total particulate matter.
气雾产生制品包括两个端部:近端和远端,穿过该近端,气雾离开气雾产生制品并且被输送到用户。在使用中,用户可以对近端抽吸,以便吸入由气雾产生制品产生的气雾。在使用中,近端也可以称作下游端,并且在远端的下游。远侧端部也可以称作上游端,并且在近端的上游。Aerosol-generating articles comprise two ends: a proximal end and a distal end, through which aerosol exits the aerosol-generating article and is delivered to a user. In use, the user may draw on the proximal end to inhale the aerosol generated by the aerosol-generating article. In use, the proximal end may also be referred to as the downstream end, and is downstream of the distal end. The distal end may also be referred to as the upstream end, and is upstream of the proximal end.
如这里使用的那样,术语‘冷却元件’用来描述具有相对大的表面面积和低抽吸阻力的元件。在使用中,由从气雾形成基体释放的易挥发化合物形成的气雾在由用户吸入之前经过冷却元件,并且由冷却元件冷却。与高抽吸阻力过滤吸嘴和其它嘴口相反,冷却元件具有低抽吸阻力。As used herein, the term 'cooling element' is used to describe an element having a relatively large surface area and low resistance to draw. In use, an aerosol formed from volatile compounds released from the aerosol-forming substrate passes through and is cooled by the cooling element before being inhaled by a user. In contrast to high-draw-resistance filter nozzles and other mouthpieces, the cooling element has a low-draw-resistance.
优选地,气雾产生制品是发烟制品,该发烟制品产生通过用户的嘴直接可吸入到用户的肺中的气雾。更优选地,该发烟制品产生通过用户的嘴直接可吸入到用户的肺中的含尼古丁的气雾。Preferably, the aerosol-generating article is a smoking article that generates an aerosol that is inhalable directly into the lungs of the user through the mouth of the user. More preferably, the smoking article produces a nicotine-containing aerosol which is inhalable directly into the lungs of the user through the mouth of the user.
在优选实施例中,气雾形成基体布置在气雾产生制品的上游端部处。In a preferred embodiment, the aerosol-forming substrate is arranged at the upstream end of the aerosol-generating article.
在一个实施例中,与气雾产生装置一起使用的气雾产生制品,包括外部包裹件,以及被限制于所述外部包裹件内的气雾形成基体和红外吸收材料;In one embodiment, an aerosol-generating article for use with an aerosol-generating device, comprising an outer wrapper, and an aerosol-forming substrate and infrared absorbing material confined within said outer wrapper;
所述气雾形成基体被配置为被加热时产生供吸食的气雾;the aerosol-forming substrate is configured to generate an aerosol for inhalation when heated;
所述红外吸收材料被配置为吸收用于辐射加热所述气雾形成基体的红外线;the infrared absorbing material is configured to absorb infrared light for radiative heating of the aerosol-forming substrate;
其中,所述红外吸收材料的吸收峰的波长范围与所述气雾形成基体中水分的吸收峰的波长范围至少部分重合。Wherein, the wavelength range of the absorption peak of the infrared absorbing material at least partially coincides with the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate.
在优选实施例中,所述红外吸收材料的吸收峰的波长范围在所述气雾形成基体中水分的吸收峰的波长范围之内;或者,In a preferred embodiment, the wavelength range of the absorption peak of the infrared absorbing material is within the wavelength range of the absorption peak of moisture in the aerosol-forming substrate; or,
所述气雾形成基体中水分的吸收峰的波长范围在所述红外吸收材料的吸收峰的波长范围之内;或者,the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate is within the wavelength range of the absorption peak of the infrared absorbing material; or,
所述红外吸收材料的吸收峰的波长范围与所述气雾形成基体中水分的吸收峰的波长范围部分重合;或者,The wavelength range of the absorption peak of the infrared absorbing material partially coincides with the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate; or,
所述红外吸收材料的吸收峰的波长范围与所述气雾形成基体中水 分的吸收峰的波长范围完全一样。The wavelength range of the absorption peak of the infrared absorbing material is exactly the same as the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate.
在优选实施例中,所述红外吸收材料是至少一种以下形状:粉末状、颗粒状、丸粒状、碎片状、丝条状、条带状或片状。In a preferred embodiment, the infrared absorbing material is in at least one of the following shapes: powder, granule, pellet, chip, strand, ribbon or sheet.
在优选实施例中,所述红外吸收材料设置在所述气雾形成基体与所述外部包裹件之间;或者,所述红外吸收材料设置在所述气雾形成基体内。In a preferred embodiment, said infrared absorbing material is disposed between said aerosol-forming substrate and said outer wrap; alternatively, said infrared absorbing material is disposed within said aerosol-forming substrate.
其中,所述红外吸收材料设置在所述气雾形成基体内,包括所述红外吸收材料与所述气雾形成基体混合的情形。Wherein, the infrared absorbing material is disposed in the aerosol-forming substrate, including the case where the infrared-absorbing material is mixed with the aerosol-forming substrate.
在优选实施例中,所述红外吸收材料结合在部分所述气雾形成基体上;其中,该部分所述气雾形成基体靠近所述气雾形成基体的下游端设置。In a preferred embodiment, the infrared absorbing material is bonded to a part of the aerosol-forming substrate; wherein, this part of the aerosol-forming substrate is disposed close to the downstream end of the aerosol-forming substrate.
其中,所述红外吸收材料结合在部分所述气雾形成基体上,包括所述红外吸收材料设置在部分所述气雾形成基体与所述外部包裹件之间、所述红外吸收材料设置在部分所述气雾形成基体内等情形。Wherein, the infrared absorbing material is combined on part of the aerosol forming substrate, including that the infrared absorbing material is arranged between a part of the aerosol forming substrate and the outer wrapper, and the infrared absorbing material is arranged on a part of the aerosol forming substrate. The aerosol-forming matrix and the like.
其中,部分所述气雾形成基体靠近所述气雾形成基体的下游端设置,包括部分所述气雾形成基体形成所述气雾形成基体的下游端的情形。Wherein, part of the aerosol-forming substrate is disposed close to the downstream end of the aerosol-forming substrate, including the case where part of the aerosol-forming substrate forms the downstream end of the aerosol-forming substrate.
在优选实施例中,所述红外吸收材料包括金属、无机非金属、有机物、超吸收材料中的至少一种。In a preferred embodiment, the infrared absorbing material includes at least one of metals, inorganic non-metals, organics, and superabsorbing materials.
在优选实施例中,以所述气雾形成基体和所述红外吸收材料的总质量计,所述红外吸收材料的质量分数介于2%~30%;优选的,介于2%~25%;进一步优选的,介于2%~20%;进一步优选的,介于2%~15%;进一步优选的,介于5%~15%。In a preferred embodiment, based on the total mass of the aerosol-forming substrate and the infrared absorbing material, the mass fraction of the infrared absorbing material is between 2% and 30%; preferably, between 2% and 25%. ; More preferably, between 2% and 20%; More preferably, between 2% and 15%; More preferably, between 5% and 15%.
在优选实施例中,还包括被限制于所述外部包裹件内的吸嘴,所述吸嘴布置在所述气雾形成基体的下游。In a preferred embodiment, further comprising a suction nozzle confined within said outer wrapper, said suction nozzle being arranged downstream of said aerosol-forming substrate.
在优选实施例中,还包括被限制于所述外部包裹件内的冷却元件,所述冷却元件布置在所述气雾形成基体与所述吸嘴之间。In a preferred embodiment, further comprising a cooling element confined within said outer wrapper, said cooling element being disposed between said aerosol-forming substrate and said mouthpiece.
需要说明的是,在其它示例中,所述吸嘴、所述冷却元件以及所述气雾形成基体可以通过不同的外部包裹件限制。例如,一外部包裹件限制所述气雾形成基体,另一外部包裹件限制所述吸嘴和所述冷却元件,两个外部包裹件可以采用相同或者不同材料制成。It should be noted that, in other examples, the suction nozzle, the cooling element, and the aerosol-forming substrate may be bounded by different outer wrappers. For example, one outer wrapper confines the aerosol-forming substrate and another outer wrapper confines the mouthpiece and cooling element, the two outer wrappers may be of the same or different materials.
本申请一个实施例还提出一种气雾产生制品,包括外部包裹件,以及被限制于所述外部包裹件内的气雾形成基体和红外吸收材料;An embodiment of the present application also provides an aerosol-generating article, including an outer wrapper, and an aerosol-forming substrate and an infrared-absorbing material confined within the outer wrapper;
所述气雾形成基体被配置为被加热时产生供吸食的气雾;the aerosol-forming substrate is configured to generate an aerosol for inhalation when heated;
所述红外吸收材料被配置为吸收用于辐射加热所述气雾形成基体的红外线;the infrared absorbing material is configured to absorb infrared light for radiative heating of the aerosol-forming substrate;
其中,所述红外吸收材料的吸收峰的波长范围介于3μm~5μm。Wherein, the wavelength range of the absorption peak of the infrared absorbing material is between 3 μm and 5 μm.
本申请一个实施例还提出一种气雾产生制品的制备方法,所述方法包括:An embodiment of the present application also proposes a method for preparing an aerosol-generating product, the method comprising:
制备气雾形成基体;preparing an aerosol-forming substrate;
制备红外吸收材料;Preparation of infrared absorbing materials;
将所述气雾形成基体与所述红外吸收材料混合后,采用常规制品工艺进行制备,以得到所述气雾产生制品。After mixing the aerosol-forming substrate and the infrared-absorbing material, the aerosol-generating product is prepared by conventional product technology.
需要说明的是,‘混合’包括所述气雾形成基体与所述红外吸收材料粉碎后的混合,例如:(粉末状、颗粒状、丸粒状、碎片状)气雾形成基体与(粉末状、颗粒状、丸粒状、碎片状)红外吸收材料的混合;还包括所述气雾形成基体与所述红外吸收材料的层叠方式的混合,例如:(丝条状、条带状或片状)气雾形成基体与(丝条状、条带状或片状)红外吸收材料的层叠。It should be noted that "mixing" includes the pulverized mixing of the aerosol-forming matrix and the infrared absorbing material, for example: (powder, granule, pellet, fragment) aerosol-forming matrix and (powder, Mixture of infrared absorbing materials in the form of granules, pellets, and fragments; also includes the mixture of the aerosol-forming substrate and the layered form of the infrared absorbing materials, for example: (wire strip, strip or sheet) gas The mist forms a laminate of the substrate and the infrared absorbing material (in the form of threads, strips or sheets).
本申请又一个实施例还提出一种气雾产生系统,包括气雾产生装置、前述的气雾产生制品,所述气雾产生装置被配置为辐射红外线加热所述气雾产生制品以产生供吸食的气雾。Yet another embodiment of the present application also proposes an aerosol generating system, including an aerosol generating device and the aforementioned aerosol generating product, the aerosol generating device is configured to radiate infrared rays to heat the aerosol generating product to generate aerosol.
以上气雾产生制品进行加热时,通过红外吸收材料吸收用于辐射加热气雾形成基体的红外线,相对常规的加热不燃烧制品,气雾的温度有所降低,尤其是降低了第一口抽吸的气雾温度,另外TPM值变化率有所提升,从而提升了用户的抽吸体验;同时,红外吸收材料的温度升高后,可一起加热并雾化气雾形成基体,一定程度上提升了制品的加热效率。When the above aerosol-generating products are heated, the infrared rays used to radiate and heat the aerosol-forming substrate are absorbed by the infrared absorbing material. Compared with conventional heat-not-burn products, the temperature of the aerosol is reduced, especially the first puff. In addition, the rate of change of the TPM value has been increased, thereby improving the user's smoking experience; at the same time, after the temperature of the infrared absorbing material rises, it can be heated together and atomized to form a matrix, which improves to a certain extent Product heating efficiency.
附图说明Description of drawings
一个或多个实施例通过与之对应的附图中的图片进行示例性说明,这些示例性说明并不构成对实施例的限定,附图中具有相同参考数字标号的元件表示为类似的元件,除非有特别申明,附图中的图不构成比例限制。One or more embodiments are exemplified by the pictures in the corresponding drawings, and these exemplifications do not constitute a limitation to the embodiments. Elements with the same reference numerals in the drawings represent similar elements. Unless otherwise stated, the drawings in the drawings are not limited to scale.
图1是本申请实施例提供的气雾产生制品的示意图;Figure 1 is a schematic diagram of an aerosol-generating product provided by an embodiment of the present application;
图2是常规的气雾产生制品的气雾温度测试结果示意图;Fig. 2 is a schematic diagram of the test results of the aerosol temperature of a conventional aerosol-generating product;
图3是一个实施例制备的气雾产生制品的气雾温度测试结果示意图;Fig. 3 is a schematic diagram of the test results of the aerosol temperature of the aerosol-generating product prepared in one embodiment;
图4是另一个实施例制备的气雾产生制品的气雾温度测试结果示意图;Fig. 4 is a schematic diagram of the test results of the aerosol temperature of the aerosol-generating product prepared in another embodiment;
图5是本申请实施例提出的气雾生成系统的示意图。Fig. 5 is a schematic diagram of an aerosol generating system proposed in an embodiment of the present application.
具体实施方式Detailed ways
为了便于理解本申请,下面结合附图和具体实施方式,对本申请进行更详细的说明。In order to facilitate the understanding of the present application, the present application will be described in more detail below in conjunction with the accompanying drawings and specific implementation methods.
本申请提出一种与气雾产生装置一起使用的气雾产生制品,这种气雾产生制品包括气雾形成基体,该气雾形成基体当由气雾产生装置内部的加热元件加热时用来产生可吸入的气雾。The present application proposes an aerosol-generating article for use with an aerosol-generating device, the aerosol-generating article comprising an aerosol-forming substrate which, when heated by a heating element inside the aerosol-generating device, serves to generate Inhalable mist.
其中,基于通常用户抽吸使用的便利性,气雾产生制品整体外观呈纵长的圆柱形的构造。在申请的一个实施例中参见图1所示,气雾产生制品包括按同轴排列布置的三个元件:Among them, based on the convenience of general user's inhalation and use, the overall appearance of the aerosol-generating product has a vertically elongated cylindrical structure. In one embodiment of the application, see Figure 1, the aerosol-generating article comprises three elements arranged in a coaxial arrangement:
气雾形成基体10、冷却元件20、以及吸嘴30;这三个元件顺序地布置,并且由外部包裹件40限制,以形成气雾产生制品。An aerosol-forming substrate 10, a cooling element 20, and a mouthpiece 30; these three elements are arranged sequentially and are bounded by an outer wrapper 40 to form an aerosol-generating article.
进一步根据图1所示,气雾产生制品具有相对的近端41以及远端42,在使用期间用户将该近端41插入到嘴中进行抽吸,该远端42布置在气雾产生制品与该近端41相对的端部处。Further according to FIG. 1, the aerosol-generating article has an opposite proximal end 41 and a distal end 42. During use, the user inserts the proximal end 41 into the mouth for suction, and the distal end 42 is arranged between the aerosol-generating article and the distal end 42. The proximal end 41 is at the opposite end.
在使用中,空气由远端42通过气雾产生制品达到近端41。气雾产生制品的远端42也可以描述成气雾产生制品的上游端部,并且气雾产生制品的近端41也可以描述成气雾产生制品的下游端部。在近端41与远端42之间布置的气雾产生制品的各元件可描述成在近端41的上游,或者可选择地在远端42的下游。In use, air passes from the distal end 42 through the aerosol-generating article to the proximal end 41 . The distal end 42 of the aerosol-generating article may also be described as the upstream end of the aerosol-generating article, and the proximal end 41 of the aerosol-generating article may also be described as the downstream end of the aerosol-generating article. The elements of the aerosol-generating article disposed between the proximal end 41 and the distal end 42 may be described as upstream of the proximal end 41 , or alternatively downstream of the distal end 42 .
气雾产生制品的外观可以模仿常规可点燃后抽吸的香烟的外观。气雾产生制品可以具有在近似5毫米~12毫米之间(例如在近似6毫米~8毫米之间)的外径。The appearance of the aerosol-generating article can mimic that of a conventional smokeable cigarette. The aerosol-generating article may have an outer diameter of between approximately 5 mm and 12 mm, such as between approximately 6 mm and 8 mm.
气雾产生制品的总长度优选地为至少约35毫米。更优选地,气雾产生制品的总长度为至少约40毫米。甚至更优选地,气雾产生制品的总长度为至少约45毫米。另外或作为替代方案,气雾产生制品的总长度优选地小于约80毫米。更优选地,气雾产生制品的总长度小于约75毫米。甚至更优选地,气雾产生制品的总长度小于约70毫米。The overall length of the aerosol-generating article is preferably at least about 35 millimeters. More preferably, the aerosol-generating article has an overall length of at least about 40 millimeters. Even more preferably, the aerosol-generating article has an overall length of at least about 45 millimeters. Additionally or alternatively, the overall length of the aerosol-generating article is preferably less than about 80 millimeters. More preferably, the overall length of the aerosol-generating article is less than about 75 millimeters. Even more preferably, the total length of the aerosol-generating article is less than about 70 millimeters.
在优选的实施方案中,气雾产生制品的总长度为约35毫米至约80毫米,更优选地为约40毫米至约75毫米,甚至更优选地为约45毫米至约70毫米。In preferred embodiments, the aerosol-generating article has an overall length of from about 35 mm to about 80 mm, more preferably from about 40 mm to about 75 mm, even more preferably from about 45 mm to about 70 mm.
气雾形成基体10布置在气雾产生制品的远端42。The aerosol-forming substrate 10 is disposed at the distal end 42 of the aerosol-generating article.
气雾形成基体10可包括尼古丁。含尼古丁的气雾形成基体10可以包括尼古丁盐基质。气雾形成基体10可以包括植物基材料。气雾形成基体10优选地包括含烟草材料。气雾形成基体10可以包括均质化的烟草材料,均质化的烟草材料可以通过凝结颗粒烟草形成。替代地或另外,气雾形成基体10可以包括不含烟草的材料。气雾形成基体10可以包括 均化的植物基材料。The aerosol-forming substrate 10 may comprise nicotine. The nicotine-containing aerosol-forming substrate 10 may comprise a nicotine salt substrate. The aerosol-forming substrate 10 may comprise a plant-based material. The aerosol-forming substrate 10 preferably comprises a tobacco-containing material. The aerosol-forming substrate 10 may comprise a homogenized tobacco material, which may be formed by agglomerating particulate tobacco. Alternatively or additionally, the aerosol-forming substrate 10 may comprise a tobacco-free material. The aerosol-forming substrate 10 may comprise a homogenized plant-based material.
气雾形成基体10可以包括例如如下的一种或多种形式:粉末、颗粒、丸粒、碎片、丝条、条带或片材。气雾形成基体10可以包含如下的一种或多种材料:烟草叶、烟草叶脉片段、复原烟草、均质化烟草、挤出烟草、烟草浆料、流延叶烟草和膨胀烟草。The aerosol-forming substrate 10 may comprise, for example, one or more of the following forms: powder, granules, pellets, chips, strands, strips or sheets. The aerosol-forming substrate 10 may comprise one or more of the following materials: tobacco leaf, tobacco vein segments, reconstituted tobacco, homogenized tobacco, extruded tobacco, tobacco pulp, cast leaf tobacco, and expanded tobacco.
气雾形成基体10可以包含至少一种气雾形成剂。气雾形成剂用来描述任何适当的已知化合物或化合物的混合物,该任何适当的已知化合物或化合物的混合物在使用中促进气雾的形成,并且大体上耐受在气雾产生制品的操作温度下的热降解。适当的气雾形成剂在技术中是已知的,并且包括但不限于:多元醇,如丙二醇、三甘醇、1,3-丁二醇、以及甘油;多元醇的酯,如甘油单、二或三乙酸酯;以及单、二或多羧酸的脂族酯,如十二烷二酸二甲酯和十四烯二酸二甲酯。The aerosol-forming substrate 10 may comprise at least one aerosol-forming agent. Aerosol-forming agent is used to describe any suitable known compound or mixture of compounds which, in use, promotes the formation of Thermal degradation at temperature. Suitable aerosol formers are known in the art and include, but are not limited to: polyols such as propylene glycol, triethylene glycol, 1,3-butanediol, and glycerin; esters of polyols such as glycerol mono, di- or triacetate; and aliphatic esters of mono-, di-, or polycarboxylic acids, such as dimethyl dodecanedioate and dimethyl tetradecenoate.
气雾形成基体可包括任何合适量的气雾形成剂。例如,气雾形成剂的含量以干重计可等于或大于气溶胶形成基材的5%,并且优选地以干重计大于30%的重量。以干重计,气雾形成剂含量可小于约95%。优选地,气雾形成剂的含量高达约55%。The aerosol-forming substrate may comprise any suitable amount of an aerosol-forming agent. For example, the amount of aerosol-forming agent may be equal to or greater than 5% by dry weight of the aerosol-forming substrate, and preferably greater than 30% by weight by dry weight. The aerosol former may comprise less than about 95% by dry weight. Preferably, the aerosol former is present in an amount up to about 55%.
气雾形成基体10还可以包含烟草或无烟草易挥发调味化合物,这些烟草或无烟草易挥发调味化合物在气雾形成基体10的加热时释放。气雾形成基体10也可以包含一个或多个封壳,该一个或多个封壳例如包括另外的烟草易挥发调味化合物或无烟草易挥发调味化合物,并且这样的封壳在气雾形成基体10的加热期间可以熔化。The aerosol-forming substrate 10 may also contain tobacco or tobacco-free volatile flavoring compounds that are released upon heating of the aerosol-forming substrate 10 . The aerosol-forming substrate 10 may also comprise one or more capsules comprising, for example, additional tobacco volatile flavoring compounds or non-tobacco volatile flavoring compounds, and such capsules are formed on the aerosol-forming substrate 10. May melt during heating.
气雾形成基体10可以提供在热稳定载体上或嵌在热稳定载体中。此处使用的术语“热稳定载体”表示在气雾形成基体10通常被加热到的温度(例如,约150℃至约300℃)下基本上不降解的材料。载体可以采取粉末、颗粒、丸粒、碎片、丝条、条带或片材的形式。气雾形成基体10可以按例如薄片、泡沫、胶或浆的形式淀积在载体的表面上。气雾形成基体10可以淀积在载体的整个表面上,或者可选择地,可以按图案淀积,以便在使用期间提供非均匀味道输送。The aerosol-forming substrate 10 may be provided on or embedded in a thermally stable carrier. As used herein, the term "thermally stable carrier" means a material that does not substantially degrade at temperatures to which aerosol-forming substrate 10 is typically heated (eg, from about 150°C to about 300°C). The carrier may take the form of powder, granules, pellets, chips, strands, ribbons or sheets. The aerosol-forming substrate 10 may be deposited on the surface of the carrier in the form of, for example, a sheet, foam, glue or paste. The aerosol-forming substrate 10 may be deposited over the entire surface of the carrier, or alternatively, may be deposited in a pattern so as to provide non-uniform flavor delivery during use.
冷却元件20布置在气雾形成基体10的紧接下游,并且与气雾形成基体10邻接。在使用中,由气雾形成基体10被加热后释放易挥发物质沿冷却元件20朝向气雾产生制品的近端41通过,并且易挥发物质可以在冷却元件20内降温变凉,以形成由用户吸入的气雾。在图1中示出的优选实施例中,冷却元件20包括空腔,该空腔沿冷却元件20的长度方向延伸。通过以上轴向延伸的空腔,使得穿过冷却元件20的空气流是在沿纵向方向上,而没有相当大的径向偏离。冷却元件20可以借助 于热传递对被抽吸通过冷却元件20的气雾流束的温度起到冷却作用。气雾的成分将与冷却元件20内的空间相互作用,并且失去热能。The cooling element 20 is arranged immediately downstream of the aerosol-forming substrate 10 and adjoins the aerosol-forming substrate 10 . In use, after the aerosol-forming substrate 10 is heated, the volatile substances released pass along the cooling element 20 toward the proximal end 41 of the aerosol-generating article, and the volatile substances can cool down in the cooling element 20 to form Inhaled mist. In the preferred embodiment shown in FIG. 1 , the cooling element 20 comprises a cavity extending along the length of the cooling element 20 . Through the above axially extending cavity, the air flow through the cooling element 20 is in the longitudinal direction without considerable radial deviation. The cooling element 20 can cool the temperature of the aerosol stream drawn through the cooling element 20 by means of heat transfer. Components of the aerosol will interact with the space within the cooling element 20 and lose thermal energy.
在一些实施例中,气雾流束的温度随着它被抽吸通过冷却元件20可能降低多于10摄氏度。在一些实施例中,气雾流束的温度随着它被抽吸通过冷却元件20可能降低多于25摄氏度或多于30摄氏度。In some embodiments, the temperature of the aerosol stream may decrease by more than 10 degrees Celsius as it is drawn through the cooling element 20 . In some embodiments, the temperature of the aerosol stream may decrease by more than 25 degrees Celsius or by more than 30 degrees Celsius as it is drawn through the cooling element 20 .
吸嘴30布置在冷却元件20的紧接下游,并与冷却元件20邻接。在图1中示出的实施例中,吸嘴30可以是常规纤维素乙酸酯或聚丙烯丝束过滤嘴。The suction nozzle 30 is arranged immediately downstream of the cooling element 20 and adjoins the cooling element 20 . In the embodiment shown in Figure 1, the mouthpiece 30 may be a conventional cellulose acetate or polypropylene tow filter.
为了组装气雾产生制品,将以上描述的三个元件对准,并且紧紧地包裹在外部包裹件40内。在图1中示出的实施例中,外部包裹件40可以是常规烟纸。To assemble the aerosol-generating article, the three components described above are aligned and tightly wrapped within the outer wrapper 40 . In the embodiment shown in Figure 1, the outer wrapper 40 may be conventional cigarette paper.
在图1中示出的气雾产生制品设计成与包括加热元件的气雾产生装置相接合,以便由用户抽吸。在使用中,气雾产生装置的加热元件将气雾产生制品的气雾形成基体10加热到足够温度以产生气雾,该气雾穿过气雾产生制品被向下游抽吸,并且由用户吸入。The aerosol-generating article shown in Figure 1 is designed to be engaged with an aerosol-generating device comprising a heating element for inhalation by a user. In use, the heating element of the aerosol-generating device heats the aerosol-forming substrate 10 of the aerosol-generating article to a temperature sufficient to generate an aerosol that is drawn downstream through the aerosol-generating article and inhaled by the user. .
本申请的一个实施例还提出一种红外吸收材料,所述红外吸收材料被配置为吸收辐射加热气雾形成基体10的红外线。优选的实施中,所述红外吸收材料的吸收峰与所述气雾形成基体中水分的吸收峰是关联的。这样,通过红外吸收材料吸收辐射加热气雾形成基体10的红外线,使得蒸发雾化的水分呈一定比例的降低,避免含有热量较高的水蒸气使得抽吸者在抽吸时产生灼痛感,尤其是降低第一口抽吸气雾的温度,提升了用户的抽吸体验;同时,红外吸收材料的温度升高后,可一起加热并雾化气雾形成基体10,一定程度上提升了制品的加热效率。An embodiment of the present application also proposes an infrared absorbing material configured to absorb infrared rays that radiate to heat the aerosol-forming substrate 10 . In a preferred implementation, the absorption peak of the infrared absorbing material is correlated with the absorption peak of the moisture in the aerosol-forming substrate. In this way, the infrared absorbing material absorbs the infrared rays that radiate and heat the aerosol to form the substrate 10, so that the evaporated and atomized water is reduced in a certain proportion, and the water vapor with high heat content is avoided to cause the smoker to have a burning sensation when inhaling, especially It is to reduce the temperature of the first puff of aerosol, which improves the user's inhalation experience; at the same time, after the temperature of the infrared absorbing material rises, it can be heated together and atomized to form the matrix 10, which improves the quality of the product to a certain extent. Heating efficiency.
在一示例中,红外吸收材料的吸收峰的波长范围与气雾形成基体10中水分的吸收峰的波长范围至少部分重合。具体地,红外吸收材料的吸收峰的波长范围在气雾形成基体10中水分的吸收峰的波长范围之内;或者,气雾形成基体10中水分的吸收峰的波长范围在红外吸收材料的吸收峰的波长范围之内;或者,红外吸收材料的吸收峰的波长范围在气雾形成基体10中水分的吸收峰的波长范围部分重合;或者,红外吸收材料的吸收峰的波长范围在气雾形成基体10中水分的吸收峰的波长范围完全一样。In one example, the wavelength range of the absorption peak of the infrared absorbing material at least partially coincides with the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate 10 . Specifically, the wavelength range of the absorption peak of the infrared absorbing material is within the wavelength range of the absorption peak of the moisture in the aerosol forming substrate 10; or, the wavelength range of the absorption peak of the moisture in the aerosol forming substrate 10 is within the wavelength range of the absorption peak of the infrared absorbing material. within the wavelength range of the peak; or, the wavelength range of the absorption peak of the infrared absorbing material partially overlaps with the wavelength range of the absorption peak of the moisture in the aerosol forming substrate 10; or, the wavelength range of the absorption peak of the infrared absorbing material is in the aerosol formation The wavelength ranges of the absorption peaks of water in the matrix 10 are exactly the same.
在一示例中,红外吸收材料的吸收峰的波长范围介于3μm~5μm。In an example, the wavelength range of the absorption peak of the infrared absorbing material is between 3 μm˜5 μm.
在一示例中,红外吸收材料是至少一种以下形式:粉末、颗粒、丸粒、碎片、丝条、条带或片材。红外吸收材料可以设置在气雾形成基体10与外部包裹件40之间,例如,片材形状的红外吸收材料夹持在气雾 形成基体10与外部包裹件40之间;或者,红外吸收材料设置在气雾形成基体10内。In an example, the infrared absorbing material is in at least one of the following forms: powder, granules, pellets, chips, strands, ribbons, or sheets. The infrared absorbing material can be arranged between the aerosol-forming substrate 10 and the outer wrapping member 40, for example, a sheet-shaped infrared-absorbing material is sandwiched between the aerosol-forming substrate 10 and the outer wrapping member 40; Within the aerosol-forming substrate 10 .
以红外吸收材料为颗粒形式为例,如图1所示,图中的标号11表示颗粒状的气雾形成基体,标号12表示颗粒状的气雾形成基体中的水分,标号13表示颗粒状的红外吸收材料;颗粒状的红外吸收材料与颗粒状的气雾形成基体以及其水分混合在一起。制品被红外辐射加热时,颗粒状的红外吸收材料与水分一起吸收3μm~5μm的红外线;这样,蒸发雾化的水分呈一定比例的降低,避免含有热量较高的水蒸气使得抽吸者在抽吸时产生灼痛感,尤其是降低第一口抽吸气雾的温度。同时,颗粒状的红外吸收材料吸收辐射热量后温度升高,将与之相邻的颗粒状的气雾形成基体加热并雾化,一定程度上提升了制品的加热效率。Take the infrared absorbing material as an example in the form of particles, as shown in Figure 1, the numeral 11 in the figure represents the granular aerosol forming matrix, the numeral 12 represents the moisture in the granular aerosol forming matrix, and the numeral 13 represents the granular aerosol Infrared absorbing material; granular infrared absorbing material mixed with a granular aerosol-forming substrate and its moisture. When the product is heated by infrared radiation, the granular infrared-absorbing material and water absorb infrared rays of 3 μm to 5 μm together; in this way, the evaporated and atomized water is reduced in a certain proportion, avoiding the water vapor with high heat and causing the smoker to lose weight during the pumping process. Burning sensation when inhaled, especially lowering the temperature of the first puff of aerosol. At the same time, the temperature of the granular infrared absorbing material rises after absorbing radiant heat, heating and atomizing the adjacent granular aerosol forming substrate, which improves the heating efficiency of the product to a certain extent.
在一示例中,红外吸收材料包括金属、无机非金属、有机物、超吸收材料中的至少一种。例如,金属包括但不限于铜、镍;无机非金属包括但不限于碳化硅、石墨烯;有机物包括但不限于蔗糖、纤维;超吸收材料:通过调控物质表面微结构,使其只吸收3μm~5μm的红外线。In an example, the infrared absorbing material includes at least one of metals, inorganic non-metals, organics, and superabsorbing materials. For example, metals include but not limited to copper and nickel; inorganic non-metals include but not limited to silicon carbide and graphene; organic substances include but not limited to sucrose and fibers; 5μm infrared.
在一示例中,以气雾形成基体10和红外吸收材料的总质量计,红外吸收材料的质量分数介于2%~30%;优选的,介于2%~25%;进一步优选的,介于2%~20%;进一步优选的,介于2%~15%;进一步优选的,介于5%~15%。In one example, based on the total mass of the aerosol-forming substrate 10 and the infrared absorbing material, the mass fraction of the infrared absorbing material is between 2% and 30%; preferably, between 2% and 25%; more preferably, between Between 2% and 20%; more preferably, between 2% and 15%; more preferably, between 5% and 15%.
以上外部包裹件40,优选采用透红外线的材料制成。例如,采用无机纤维材料制备,具体包括羟基磷灰石纤维、碳化硅纤维、钛酸钡纤维中的一种或多种。The above outer wrapper 40 is preferably made of infrared-transmitting material. For example, it is prepared by using inorganic fiber materials, specifically including one or more of hydroxyapatite fibers, silicon carbide fibers, and barium titanate fibers.
以上羟基磷灰石纤维、碳化硅纤维、钛酸钡纤维是具有优良的可透红外线的材料,使得可以通过红外辐射的方式对气雾产生制品加热时,外部包裹件40大体是不吸收红外线的,从而有效地促进内部气雾形成基体10的加热效率。The above hydroxyapatite fiber, silicon carbide fiber, and barium titanate fiber are materials with excellent infrared permeability, so that when the aerosol-generating product can be heated by infrared radiation, the outer wrapper 40 generally does not absorb infrared rays , thereby effectively promoting the heating efficiency of the inner aerosol-forming substrate 10 .
进一步为了便于对采用以上红外吸收材料的气雾产生制品可实施性,以及制备的气雾产生制品在各项性能上的进步性进行验证,以下通过具体实施例对制备的气雾产生制品进行示例和测试结果说明。Further, in order to facilitate the verification of the feasibility of the aerosol-generating products using the above infrared absorbing materials and the progress of the prepared aerosol-generating products in various performances, the prepared aerosol-generating products are illustrated through specific examples below and description of the test results.
S11,制备气雾形成基体的植物基材料;例如:烟草材料。S11. A plant-based material for preparing an aerosol-forming substrate; eg, tobacco material.
S12,制备红外吸收材料。S12, preparing an infrared absorbing material.
可以采用碳化硅材料,其中碳化硅材料的质量分数为10%,粒度为24目。Silicon carbide material can be used, wherein the mass fraction of silicon carbide material is 10%, and the particle size is 24 mesh.
也可以采用石墨烯材料,其中石墨烯材料的质量分数为10%。Graphene material can also be used, wherein the mass fraction of graphene material is 10%.
其中步骤S11、步骤S12可以不分先后顺序。The steps S11 and S12 can be performed in any order.
S13,将植物基材料与红外吸收材料混合后,可以采用常规制品工艺进行制备,以得到气雾产生制品。S13, after mixing the plant-based material and the infrared absorbing material, it can be prepared by conventional product technology to obtain an aerosol-generating product.
可以采用颗粒制品工艺进行制备,以得到颗粒型的气雾产生制品。It can be prepared by adopting a granular product technology to obtain a granular aerosol-generating product.
也可以采用常规再造烟叶型制品工艺(例如造纸法、干法、稠浆法以及辊压法等等)进行制备,以得到再造烟叶型的气雾产品制品。It can also be prepared by conventional reconstituted tobacco leaf product technology (such as papermaking method, dry method, thick pulp method, rolling method, etc.) to obtain reconstituted tobacco leaf-type aerosol products.
上述制品工艺可参考现有技术,例如:“董高峰,田永峰,尚善斋,等.用于加热不燃烧(HnB)卷烟的再造烟叶生产工艺研究进展[J].中国烟草学报,2020,26(1)”,具体地在此不作赘述。The above-mentioned product technology can refer to the existing technology, for example: "Dong Gaofeng, Tian Yongfeng, Shang Shanzhai, etc. Research progress in the production process of reconstituted tobacco leaves for heat-not-burn (HnB) cigarettes [J]. Chinese Journal of Tobacco, 2020, 26(1)", the details will not be repeated here.
对以上实施例制备的气雾产生制品进行气雾温度测试和TPM值变化率测试,测试的内容均采用常规的加热不燃烧制品进行比对。The aerosol-generating products prepared in the above examples were tested for the aerosol temperature and the rate of change of the TPM value, and the contents of the tests were compared with conventional heat-not-burn products.
一、气雾温度测试1. Aerosol temperature test
测试目的:测试制品抽吸时的气雾温度Test purpose: to test the aerosol temperature of the product when inhaled
测试环境:环境温度:25℃,相对湿度:65RH%。Test environment: ambient temperature: 25°C, relative humidity: 65RH%.
测试仪器:温度传感器采用K型热电偶;温度记录仪:GRAPHTEC GL240;抽烟机:采用自有设备。Test instrument: K-type thermocouple is used for temperature sensor; temperature recorder: GRAPHTEC GL240; smoking machine: self-owned equipment is used.
测试工况:抽烟机工况设定:抽吸量55ml/3s,抽吸间隔时间:27s;气雾温度采集点设定:K型热电偶布置于制品吸嘴的端面中心;数据记录频率:10Hz,即100ms记录一次数据。Test working conditions: smoke machine working condition setting: suction volume 55ml/3s, suction interval: 27s; gas mist temperature collection point setting: K-type thermocouple is arranged at the center of the end face of the product suction nozzle; data recording frequency: 10Hz, that is, record data once every 100ms.
测试步骤:Test steps:
S31,将受测制品插入气雾产生装置中;其中,受测制品包括实施例1、实施例2制备的气雾产生制品以及常规的加热不燃烧制品;每次测试均采用同一个气雾产生装置,以保证制品的加热工况相同;同一种类的制品可测试多个制品,以保证测试结果;S31, inserting the tested product into the aerosol generating device; wherein, the tested product includes the aerosol generating product prepared in Example 1 and Example 2 and a conventional heat-not-burn product; each test uses the same aerosol generating device. device to ensure that the heating conditions of the products are the same; multiple products of the same type can be tested to ensure the test results;
S32,将K型热电偶布置于受测制品吸嘴的端面中心;S32, arrange the K-type thermocouple at the center of the end face of the suction nozzle of the product under test;
S33,连接K型热电偶与温度记录仪;S33, connect K-type thermocouple and temperature recorder;
S34,启动气雾产生装置对制品进行预热,同时开启抽烟机并记录温度数据;S34, start the aerosol generating device to preheat the product, and at the same time turn on the smoker and record the temperature data;
S35,预热结束后,通过抽烟机进行抽吸并记录抽吸时的温度数据。S35, after the preheating is finished, smoke through the smoke machine and record the temperature data during the smoke.
受测制品为常规的加热不燃烧制品,其测试结果可参考附图2所示;The tested product is a conventional heat-not-burn product, and its test results can be referred to as shown in Figure 2;
受测制品为采用碳化硅材料作为红外吸收材料,其中碳化硅材料的质量分数为10%,粒度为24目;通过采用颗粒制品工艺进行制备的颗粒型的气雾产生制品,其测试结果可参考附图3所示;The tested product uses silicon carbide material as the infrared absorbing material, wherein the mass fraction of silicon carbide material is 10%, and the particle size is 24 mesh; the granular aerosol generating product prepared by adopting the granular product process, the test results can refer to Shown in accompanying drawing 3;
受测制品为采用石墨烯材料作为红外吸收材料,其中石墨烯材料的质量分数为10%;采用常规再造烟叶型制品工艺进行制备的再造烟叶型的气雾产品制品,其测试结果可参考附图4所示。The tested product uses graphene material as the infrared absorbing material, and the mass fraction of graphene material is 10%; the reconstituted tobacco leaf-type aerosol product is prepared by the conventional reconstituted tobacco leaf-type product process, and the test results can refer to the accompanying drawings 4.
其中,图2-图4中的横坐标表示采集的时间,纵坐标表示对应的温度,且从图2-图4的测试结果可以看出,附图2所示的常规的加热不燃烧制品中,其第一口抽吸气雾的温度约为55℃,相对常规的加热不燃烧制品,附图3所示的气雾产生制品,其第一口抽吸气雾的温度约为50℃,降低约5℃;附图4所示的气雾产生制品,其第一口抽吸气雾的温度约为51℃,降低约4℃。很显然的,减少了用户抽吸第一口时会产生灼痛感的问题。Wherein, the abscissa in Fig. 2-Fig. 4 represents the time of collection, and the ordinate represents the corresponding temperature, and it can be seen from the test results in Fig. 2-Fig. 4 that in the conventional heat-not-burn products shown in Fig. 2 , the temperature of the first inhaled aerosol is about 55°C, compared with conventional heat-not-burn products, the aerosol generating product shown in Figure 3, the temperature of the first inhaled aerosol is about 50°C, Decrease by about 5°C; for the aerosol-generating product shown in Figure 4, the temperature of the first inhaled aerosol is about 51°C, which is about 4°C lower. Apparently, the problem of burning sensation when users take the first puff is reduced.
二、TPM值变化率测试2. TPM value change rate test
测试目的:测试气雾产品制品1和气雾产生制品2相对于常规的加热不燃烧制品的TPM值变化率。Test purpose: To test the change rate of TPM value of aerosol product product 1 and aerosol-generating product 2 relative to conventional heat-not-burn products.
其中气雾产品制品1为采用碳化硅材料作为红外吸收材料,其中碳化硅材料的质量分数为10%,粒度为24目;通过采用颗粒制品工艺进行制备的颗粒型的气雾产生制品;气雾产品制品2为采用石墨烯材料作为红外吸收材料,其中石墨烯材料的质量分数为10%;采用常规再造烟叶型制品工艺进行制备的再造烟叶型的气雾产品制品。Among them, aerosol product product 1 uses silicon carbide material as the infrared absorbing material, wherein the mass fraction of silicon carbide material is 10%, and the particle size is 24 meshes; a granular aerosol generating product prepared by adopting a granular product process; aerosol Product 2 is a reconstituted tobacco leaf-type aerosol product that uses graphene material as an infrared absorbing material, and the mass fraction of graphene material is 10%; it is prepared by a conventional reconstituted tobacco leaf-type product process.
测试步骤:Test steps:
S41,测试常规的加热不燃烧制品、气雾产生制品1和气雾产品制品2,在抽吸前后的质量,并计算出失重值,如下表格所示:S41, test the mass of conventional heat-not-burn products, aerosol-generating product 1 and aerosol product 2 before and after smoking, and calculate the weight loss value, as shown in the following table:
Figure PCTCN2022142490-appb-000001
Figure PCTCN2022142490-appb-000001
S42,根据常规的加热不燃烧制品、气雾产生制品1的TPM值,计 算得到气雾产生制品1的TPM值变化率,如下计算过程所示:S42, according to the TPM value of the conventional heat-not-burn product and the aerosol-generating product 1, calculate the rate of change of the TPM value of the aerosol-generating product 1, as shown in the following calculation process:
Figure PCTCN2022142490-appb-000002
Figure PCTCN2022142490-appb-000002
与此类似的,得到气雾产生制品2的TPM值变化率约为6.9%。Similarly, the change rate of the TPM value of the aerosol-generating article 2 is about 6.9%.
以上测试结果可以看出,相对常规的加热不燃烧制品,气雾产生制品1、以及气雾产生制品2,其TPM值变化率都有所提升,进而提升了用户的抽吸体验。From the above test results, it can be seen that, compared with conventional heat-not-burn products, the rate of change of TPM value of aerosol-generating product 1 and aerosol-generating product 2 has been improved, thereby improving the user's smoking experience.
进一步本申请还提出一种包括以上气雾产生制品和加热装置的气雾生成系统,在一个实施例中的构造参见图5所示;Further, the present application also proposes an aerosol generating system comprising the above aerosol generating product and a heating device, and the structure in one embodiment is shown in FIG. 5 ;
加热装置200包括加热元件210;The heating device 200 includes a heating element 210;
其中,加热元件210是管状的形状,其管状中空的至少一部分被构造成接收气雾产生制品100的腔室,该加热元件210通过向气雾产生制品100辐射红外线进而对气雾产生制品100进行加热。气雾产生制品100可参考前述内容,在此不作赘述。Wherein, the heating element 210 is in the shape of a tube, at least a part of which is configured to receive the chamber of the aerosol generating product 100, and the heating element 210 radiates infrared rays to the aerosol generating product 100 to further heat the aerosol generating product 100. heating. For the aerosol-generating article 100, reference may be made to the aforementioned content, and details are not repeated here.
采用以上红外辐射的加热元件210对进行加热时,气雾产生制品100内的红外吸收材料吸收辐射加热气雾形成基体的红外线,使得蒸发雾化的水分呈一定比例的降低,避免含有热量较高的水蒸气使得抽吸者在抽吸时很容易产生灼痛感,尤其是降低第一口抽吸气雾的温度,提升了用户的抽吸体验;同时,红外吸收材料的温度升高后,可一起加热并雾化气雾形成基体,一定程度上提升了制品的加热效率。When the above infrared radiation heating element 210 is used for heating, the infrared absorbing material in the gas mist generating product 100 absorbs the infrared rays of radiation heating the gas mist forming substrate, so that the evaporated and atomized water is reduced in a certain proportion, avoiding high heat content The water vapor in the smoke makes it easy for the smoker to have a burning sensation when smoking, especially reducing the temperature of the first puff of the mist, which improves the user's suction experience; at the same time, after the temperature of the infrared absorbing material rises, it can Heating together and atomizing the aerosol to form a matrix improves the heating efficiency of the product to a certain extent.
需要说明的是,本申请的说明书及其附图中给出了本申请的较佳的实施例,但并不限于本说明书所描述的实施例,进一步地,对本领域普通技术人员来说,可以根据上述说明加以改进或变换,而所有这些改进和变换都应属于本申请所附权利要求的保护范围。It should be noted that the preferred embodiments of the application are given in the description of the application and its drawings, but they are not limited to the embodiments described in the description. Further, for those of ordinary skill in the art, they can Improvements or transformations are made according to the above description, and all these improvements and transformations shall fall within the scope of protection of the appended claims of this application.

Claims (12)

  1. 一种气雾产生制品,其特征在于,包括外部包裹件,以及被限制于所述外部包裹件内的气雾形成基体和红外吸收材料;An aerosol-generating article comprising an outer wrapper, and an aerosol-forming substrate and an infrared absorbing material confined within said outer wrapper;
    所述气雾形成基体被配置为被加热时产生供吸食的气雾;the aerosol-forming substrate is configured to generate an aerosol for inhalation when heated;
    所述红外吸收材料被配置为吸收用于辐射加热所述气雾形成基体的红外线;the infrared absorbing material is configured to absorb infrared light for radiative heating of the aerosol-forming substrate;
    其中,所述红外吸收材料的吸收峰的波长范围与所述气雾形成基体中水分的吸收峰的波长范围至少部分重合。Wherein, the wavelength range of the absorption peak of the infrared absorbing material at least partially coincides with the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate.
  2. 如权利要求1所述的气雾产生制品,其特征在于,The aerosol-generating article of claim 1, wherein:
    所述红外吸收材料的吸收峰的波长范围在所述气雾形成基体中水分的吸收峰的波长范围之内;或者,The wavelength range of the absorption peak of the infrared absorbing material is within the wavelength range of the absorption peak of moisture in the aerosol-forming substrate; or,
    所述气雾形成基体中水分的吸收峰的波长范围在所述红外吸收材料的吸收峰的波长范围之内;或者,the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate is within the wavelength range of the absorption peak of the infrared absorbing material; or,
    所述红外吸收材料的吸收峰的波长范围与所述气雾形成基体中水分的吸收峰的波长范围部分重合;或者,The wavelength range of the absorption peak of the infrared absorbing material partially coincides with the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate; or,
    所述红外吸收材料的吸收峰的波长范围与所述气雾形成基体中水分的吸收峰的波长范围完全一样。The wavelength range of the absorption peak of the infrared absorbing material is exactly the same as the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate.
  3. 如权利要求1所述的气雾产生制品,其特征在于,所述红外吸收材料是至少一种以下形状:The aerosol-generating article of claim 1, wherein said infrared absorbing material is in at least one of the following shapes:
    粉末状、颗粒状、丸粒状、碎片状、丝条状、条带状或片状。Powder, granules, pellets, flakes, strands, ribbons or flakes.
  4. 如权利要求1所述的气雾产生制品,其特征在于,所述红外吸收材料设置在所述气雾形成基体与所述外部包裹件之间;或者,所述红外吸收材料设置在所述气雾形成基体内。The aerosol-generating article of claim 1, wherein said infrared absorbing material is disposed between said aerosol-forming substrate and said outer wrap; or, said infrared absorbing material is disposed between said aerosol-generating article. Fog is formed within the matrix.
  5. 如权利要求1所述的气雾产生制品,其特征在于,所述红外吸收材料结合在部分所述气雾形成基体上;其中,该部分所述气雾形成基体靠近所述气雾形成基体的下游端设置。The aerosol-generating article of claim 1, wherein said infrared absorbing material is bonded to a portion of said aerosol-forming substrate; wherein said portion of said aerosol-forming substrate is adjacent to said aerosol-forming substrate Downstream settings.
  6. 如权利要求1所述的气雾产生制品,其特征在于,所述红外吸收材料包括金属、无机非金属、有机物、超吸收材料中的至少一种。The aerosol-generating article according to claim 1, wherein the infrared absorbing material comprises at least one of metals, inorganic non-metals, organic substances, and superabsorbing materials.
  7. 如权利要求1所述的气雾产生制品,其特征在于,以所述气雾形成基体和所述红外吸收材料的总质量计,所述红外吸收材料的质量分数介于2%~30%;或者,介于2%~25%;或者,介于2%~20%;或者,介于2%~15%;或者,介于5%~15%。The aerosol-generating product according to claim 1, characterized in that, based on the total mass of the aerosol-forming substrate and the infrared-absorbing material, the mass fraction of the infrared-absorbing material is between 2% and 30%; Or, between 2%-25%; or, between 2%-20%; or, between 2%-15%; or, between 5%-15%.
  8. 如权利要求1所述的气雾产生制品,其特征在于,还包括被限 制于所述外部包裹件内的吸嘴,所述吸嘴布置在所述气雾形成基体的下游。The aerosol-generating article of claim 1, further comprising a mouthpiece confined within said outer wrapper, said mouthpiece being disposed downstream of said aerosol-forming substrate.
  9. 如权利要求8所述的气雾产生制品,其特征在于,还包括被限制于所述外部包裹件内的冷却元件,所述冷却元件布置在所述气雾形成基体与所述吸嘴之间。The aerosol-generating article of claim 8, further comprising a cooling element confined within said outer wrapper, said cooling element being disposed between said aerosol-generating substrate and said mouthpiece .
  10. 一种气雾产生制品,其特征在于,包括外部包裹件,以及被限制于所述外部包裹件内的气雾形成基体和红外吸收材料;An aerosol-generating article comprising an outer wrapper, and an aerosol-forming substrate and an infrared absorbing material confined within said outer wrapper;
    所述气雾形成基体被配置为被加热时产生供吸食的气雾;the aerosol-forming substrate is configured to generate an aerosol for inhalation when heated;
    所述红外吸收材料被配置为吸收用于辐射加热所述气雾形成基体的红外线;the infrared absorbing material is configured to absorb infrared light for radiative heating of the aerosol-forming substrate;
    其中,所述红外吸收材料的吸收峰的波长范围介于3μm~5μm。Wherein, the wavelength range of the absorption peak of the infrared absorbing material is between 3 μm and 5 μm.
  11. 一种气雾产生制品的制备方法,其特征在于,所述方法包括:A method for preparing an aerosol-generating product, characterized in that the method comprises:
    制备气雾形成基体;preparing an aerosol-forming substrate;
    制备红外吸收材料;Preparation of infrared absorbing materials;
    将所述气雾形成基体与所述红外吸收材料混合后,采用常规制品工艺进行制备,以得到所述气雾产生制品。After mixing the aerosol-forming substrate and the infrared-absorbing material, the aerosol-generating product is prepared by conventional product technology.
  12. 一种气雾产生系统,其特征在于,包括气雾产生装置、权利要求1-10任一所述的气雾产生制品,所述气雾产生装置被配置为辐射红外线加热所述气雾产生制品以产生供吸食的气雾。An aerosol generating system, characterized by comprising an aerosol generating device and the aerosol generating product according to any one of claims 1-10, the aerosol generating device is configured to radiate infrared rays to heat the aerosol generating product To produce aerosol for inhalation.
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