CN116349928A - Aerosol generating product, preparation method thereof and aerosol generating system - Google Patents
Aerosol generating product, preparation method thereof and aerosol generating system Download PDFInfo
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- CN116349928A CN116349928A CN202111621279.1A CN202111621279A CN116349928A CN 116349928 A CN116349928 A CN 116349928A CN 202111621279 A CN202111621279 A CN 202111621279A CN 116349928 A CN116349928 A CN 116349928A
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- forming substrate
- absorbing material
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Images
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
- A24F40/40—Constructional details, e.g. connection of cartridges and battery parts
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
- A24F40/20—Devices using solid inhalable precursors
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
- A24F40/40—Constructional details, e.g. connection of cartridges and battery parts
- A24F40/46—Shape or structure of electric heating means
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
- A24F40/50—Control or monitoring
- A24F40/51—Arrangement of sensors
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
- A24F40/50—Control or monitoring
- A24F40/53—Monitoring, e.g. fault detection
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
- A24F40/50—Control or monitoring
- A24F40/57—Temperature control
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
- A24F40/70—Manufacture
Abstract
An aerosol-generating article, a method of making the same, an aerosol-generating system, the aerosol-generating article comprising an outer wrapper, and an aerosol-forming substrate and an infrared absorbing material confined within the outer wrapper; the infrared absorbing material is configured to absorb infrared light for radiating the heated aerosol-forming substrate; the wavelength range of the absorption peak of the infrared absorbing material at least partially coincides with the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate. When the aerosol generating product is heated, infrared absorption materials absorb infrared rays for radiating and heating the aerosol to form a matrix, compared with the conventional heating non-combustion product, the temperature of the aerosol is reduced, particularly the temperature of the aerosol sucked by a first port is reduced, and in addition, the change rate of TPM value is improved, so that the suction experience of a user is improved; meanwhile, after the temperature of the infrared absorption material is increased, the infrared absorption material can be heated and atomized to form a matrix, so that the heating efficiency of the product is improved to a certain extent.
Description
Technical Field
The embodiment of the application relates to the technical field of products, in particular to an aerosol generating product, a preparation method thereof and an aerosol generating system.
Background
Smoking articles (e.g., cigarettes, cigars, etc.) burn tobacco during use to produce tobacco smoke. Attempts have been made to replace these tobacco-burning smoking articles by making products that release the compounds without burning.
An example of such a product is a heating device that releases a compound by heating rather than burning a smokable material in the article. For example, the smokable material may be tobacco or other non-tobacco products, which may or may not contain nicotine. As another example, there are heating devices that heat an article by infrared radiation to release a compound to produce an aerosol.
Because the infrared rays have stronger penetrability, the infrared rays can penetrate through the periphery of the product to enter the interior, so that the internal and external heating of the product is more uniform. Disadvantageously, such uniform heating causes a substantial portion of the moisture in the product to be vaporized by heat, while the higher heat-containing water vapor makes the user more prone to burning when inhaling, especially when inhaling the first bite.
Disclosure of Invention
In order to solve the problem that the existing product is easy to cause a smoker to produce a burning sensation during smoking when being heated by infrared radiation, the embodiment of the application provides an aerosol generating product, a preparation method thereof and an aerosol generating system.
As used herein, the term 'aerosol-forming substrate' is used to describe a substrate that is capable of releasing volatile compounds upon heating, which may form an aerosol. The aerosol generated by the aerosol-forming substrate of the aerosol-generating article described herein may be visible or invisible and may comprise droplets of vapor (e.g., fine particles of a substance, which particles are in a gaseous state, which particles are typically liquid or solid at room temperature) as well as gases and condensed vapors.
As used herein, the terms 'upstream' and 'downstream' are used to describe the relative positions of elements, or portions of elements, of the aerosol-generating article with respect to the direction in which a user draws on the aerosol-generating article during its use.
As used herein, the term 'mass fraction' refers to the percentage of the mass of a substance in a mixture to the total mass.
As used herein, the term 'TPM (Total Particulate Matter)' refers to the total particulate matter.
The aerosol-generating article comprises two ends: a proximal end through which the aerosol exits the aerosol-generating article and is delivered to a user, and a distal end. In use, a user may draw on the proximal end in order to inhale the aerosol generated by the aerosol-generating article. In use, the proximal end may also be referred to as the downstream end, and downstream of the distal end. The distal end may also be referred to as the upstream end and upstream of the proximal end.
As used herein, the term 'cooling element' is used to describe an element having a relatively large surface area and low resistance to draw. In use, an aerosol formed from a volatile compound released from the aerosol-forming substrate passes over and is cooled by the cooling element prior to inhalation by a user. The cooling element has a low resistance to suction, as opposed to high resistance to suction filter nozzles and other mouthpieces.
Preferably, the aerosol-generating article is a smoking article that generates an aerosol that is directly inhalable into a user's lungs through the user's mouth. More preferably, the smoking article produces a nicotine-containing aerosol directly inhalable into a user's lungs through the user's mouth.
In a preferred embodiment, the aerosol-forming substrate is arranged at the upstream end of the aerosol-generating article.
In one embodiment, an aerosol-generating article for use with an aerosol-generating device comprises an outer wrapper, and an aerosol-forming substrate and an infrared absorbing material confined within the outer wrapper;
the aerosol-forming substrate being configured to produce an aerosol for inhalation when heated;
the infrared absorbing material is configured to absorb infrared light for radiation heating the aerosol-forming substrate;
wherein the wavelength range of the absorption peak of the infrared absorbing material at least partially coincides with the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate.
In a preferred embodiment, the infrared absorbing material has an absorption peak with a wavelength range within the wavelength range of the absorption peak of moisture in the aerosol-forming substrate; or alternatively, the process may be performed,
the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate is within the wavelength range of the absorption peak of the infrared absorbing material; or alternatively, the process may be performed,
the wavelength range of the absorption peak of the infrared absorbing material partially coincides with the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate; or alternatively, the process may be performed,
the wavelength range of the absorption peak of the infrared absorbing material is exactly the same as the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate.
In a preferred embodiment, the infrared absorbing material is at least one of the following shapes: powdery, granular, pellet, chip, wire, ribbon or sheet.
In a preferred embodiment, the infrared absorbing material is disposed between the aerosol-forming substrate and the outer wrapper; alternatively, the infrared absorbing material is disposed within the aerosol-forming substrate.
Wherein the infrared absorbing material is disposed within the aerosol-forming substrate, including when the infrared absorbing material is mixed with the aerosol-forming substrate.
In a preferred embodiment, the infrared absorbing material is bonded to a portion of the aerosol-forming substrate; wherein the portion of the aerosol-forming substrate is disposed proximate a downstream end of the aerosol-forming substrate.
Wherein the infrared absorbing material is bonded to a portion of the aerosol-forming substrate, including where the infrared absorbing material is disposed between a portion of the aerosol-forming substrate and the outer wrapper, where the infrared absorbing material is disposed within a portion of the aerosol-forming substrate, and the like.
Wherein a portion of the aerosol-forming substrate is disposed proximate a downstream end of the aerosol-forming substrate, including where a portion of the aerosol-forming substrate forms the downstream end of the aerosol-forming substrate.
In a preferred embodiment, the infrared absorbing material comprises at least one of a metal, an inorganic non-metal, an organic, a super absorbing material.
In a preferred embodiment, the mass fraction of the infrared absorbing material is between 2% and 30% based on the total mass of the aerosol-forming substrate and the infrared absorbing material; preferably, between 2% and 25%; further preferably, between 2% and 20%; further preferably, between 2% and 15%; more preferably, the content is 5 to 15%.
In a preferred embodiment, further comprising a mouthpiece confined within the outer wrapper, the mouthpiece being arranged downstream of the aerosol-forming substrate.
In a preferred embodiment, a cooling element is also included that is confined within the outer wrapper, the cooling element being disposed between the aerosol-forming substrate and the mouthpiece.
In other examples, the mouthpiece, the cooling element, and the aerosol-forming substrate may be constrained by different external wraps. For example, one outer wrapper may limit the aerosol-forming substrate and the other outer wrapper may limit the mouthpiece and the cooling element, the two outer wrappers may be made of the same or different materials.
One embodiment of the present application also contemplates an aerosol-generating article comprising an outer wrapper, and an aerosol-forming substrate and an infrared absorbing material confined within the outer wrapper;
the aerosol-forming substrate being configured to produce an aerosol for inhalation when heated;
the infrared absorbing material is configured to absorb infrared light for radiation heating the aerosol-forming substrate;
wherein the infrared absorbing material has an absorption peak wavelength ranging from 3 μm to 5 μm.
One embodiment of the present application also proposes a method of producing an aerosol-generating article, the method comprising:
preparing an aerosol-forming substrate;
preparing an infrared absorbing material;
the aerosol-forming substrate is mixed with the infrared absorbing material and then prepared using conventional manufacturing techniques to provide the aerosol-generating article.
It should be noted that the term "mixing" includes mixing of the aerosol-forming substrate and the infrared absorbing material after pulverization, for example: mixing the aerosol-forming substrate (in powder, granule, pellet, chip form) with the infrared absorbing material (in powder, granule, pellet, chip form); also included are combinations of lamination modes of the aerosol-forming substrate and the infrared absorbing material, such as: lamination of an aerosol-forming substrate (in the form of a strip, ribbon or sheet) with an infrared absorbing material (in the form of a strip, ribbon or sheet).
Yet another embodiment of the present application also proposes an aerosol-generating system comprising an aerosol-generating device, the aforementioned aerosol-generating article, the aerosol-generating device being configured to radiate infrared radiation to heat the aerosol-generating article to generate an aerosol for inhalation.
When the aerosol generating product is heated, infrared absorption materials absorb infrared rays for radiating and heating the aerosol to form a matrix, compared with the conventional heating non-combustion product, the temperature of the aerosol is reduced, particularly the temperature of the aerosol sucked by a first port is reduced, and in addition, the change rate of TPM value is improved, so that the suction experience of a user is improved; meanwhile, after the temperature of the infrared absorption material is increased, the infrared absorption material can be heated and atomized to form a matrix, so that the heating efficiency of the product is improved to a certain extent.
Drawings
One or more embodiments are illustrated by way of example and not limitation in the figures of the accompanying drawings, in which like references indicate similar elements, and in which the figures of the drawings are not to be taken in a limiting sense, unless otherwise indicated.
FIG. 1 is a schematic illustration of an aerosol-generating article provided in an embodiment of the present application;
FIG. 2 is a schematic diagram of the results of an aerosol temperature test of a conventional aerosol-generating article;
FIG. 3 is a schematic illustration of aerosol temperature test results of an aerosol-generating article prepared according to one example;
FIG. 4 is a schematic illustration of aerosol temperature test results of an aerosol-generating article prepared according to another embodiment;
fig. 5 is a schematic diagram of an aerosol-generating system according to an embodiment of the present application.
Detailed Description
In order to facilitate an understanding of the present application, the present application will be described in more detail below with reference to the accompanying drawings and detailed description.
An aerosol-generating article for use with an aerosol-generating device is presented, the aerosol-generating article comprising an aerosol-forming substrate for generating an inhalable aerosol when heated by a heating element inside the aerosol-generating device.
Wherein the aerosol-generating article has an overall appearance of a slim cylindrical configuration based on convenience of use by a typical user. In one embodiment of the application, referring to fig. 1, the aerosol-generating article comprises three elements arranged in a coaxial arrangement:
an aerosol-forming substrate 10, a cooling element 20, and a mouthpiece 30; these three elements are arranged in sequence and are constrained by an outer wrapper 40 to form an aerosol-generating article.
Further according to fig. 1, the aerosol-generating article has an opposite proximal end 41 and a distal end 42, the proximal end 41 being inserted into the mouth for suction by a user during use, the distal end 42 being arranged at the end of the aerosol-generating article opposite the proximal end 41.
In use, air passes from the distal end 42 through the aerosol-generating article to the proximal end 41. The distal end 42 of the aerosol-generating article may also be described as the upstream end of the aerosol-generating article, and the proximal end 41 of the aerosol-generating article may also be described as the downstream end of the aerosol-generating article. The elements of the aerosol-generating article disposed between the proximal end 41 and the distal end 42 may be described as being upstream of the proximal end 41, or alternatively downstream of the distal end 42.
The appearance of the aerosol-generating article may mimic the appearance of a conventional smokeable cigarette. The aerosol-generating article may have an outer diameter of between approximately 5 mm and 12 mm (e.g., between approximately 6 mm and 8 mm).
The total length of the aerosol-generating article is preferably at least about 35 millimeters. More preferably, the total length of the aerosol-generating article is at least about 40 millimeters. Even more preferably, the total length of the aerosol-generating article is at least about 45 millimeters. Additionally or alternatively, the overall length of the aerosol-generating article is preferably less than about 80 millimeters. More preferably, the total length of the aerosol-generating article is less than about 75 millimeters. Even more preferably, the total length of the aerosol-generating article is less than about 70 millimeters.
In a preferred embodiment, the total length of the aerosol-generating article is from about 35 mm to about 80 mm, more preferably from about 40 mm to about 75 mm, even more preferably from about 45 mm to about 70 mm.
The aerosol-forming substrate 10 is disposed at a distal end 42 of the aerosol-generating article.
The aerosol-forming substrate 10 may comprise nicotine. The nicotine-containing aerosol-forming substrate 10 may comprise a nicotine salt matrix. The aerosol-forming substrate 10 may comprise a plant-based material. The aerosol-forming substrate 10 preferably comprises a tobacco-containing material. The aerosol-forming substrate 10 may comprise a homogenized tobacco material, which may be formed by agglomerating particulate tobacco. Alternatively or additionally, the aerosol-forming substrate 10 may comprise a tobacco-free material. The aerosol-forming substrate 10 may comprise a homogenized plant-based material.
The aerosol-forming substrate 10 may comprise, for example, one or more of the following forms: powder, granules, pellets, chips, strands, ribbons or sheets. The aerosol-forming substrate 10 may comprise one or more of the following materials: tobacco leaves, tobacco vein segments, reconstituted tobacco, homogenized tobacco, extruded tobacco, tobacco slurry, cast leaf tobacco, and expanded tobacco.
The aerosol-forming substrate 10 may comprise at least one aerosol-forming agent. An aerosol-former is used to describe any suitable known compound or mixture of compounds that promotes the formation of an aerosol in use and is generally resistant to thermal degradation at the operating temperature of the aerosol-generating article. Suitable aerosol formers are known in the art and include, but are not limited to: polyols such as propylene glycol, triethylene glycol, 1, 3-butanediol, and glycerol; esters of polyhydric alcohols, such as glycerol mono-, di-or triacetate; and aliphatic esters of mono-, di-or polycarboxylic acids, such as dimethyl dodecanedioate and dimethyl tetradecenedioate.
The aerosol-forming substrate may comprise any suitable amount of aerosol-forming agent. For example, the content of aerosol-forming agent may be equal to or greater than 5% by dry weight of the aerosol-forming substrate, and preferably greater than 30% by weight on a dry weight basis. The aerosol former content may be less than about 95% on a dry weight basis. Preferably, the aerosol former is present in an amount up to about 55%.
The aerosol-forming substrate 10 may also comprise tobacco or smokeless volatile flavoring compounds that are released upon heating of the aerosol-forming substrate 10. The aerosol-forming substrate 10 may also comprise one or more capsules comprising, for example, additional tobacco or smokeless volatile flavoring compounds, and such capsules may melt during heating of the aerosol-forming substrate 10.
The aerosol-forming substrate 10 may be provided on or embedded in a thermally stable carrier. The term "thermally stable" as used herein refers to a material that does not substantially degrade at the temperature to which the aerosol-forming substrate 10 is typically heated (e.g., about 150 ℃ to about 300 ℃). The carrier may take the form of a powder, granules, pellets, chips, strands, ribbons, or sheets. The aerosol-forming substrate 10 may be deposited on the surface of the carrier in the form of, for example, a sheet, foam, gel or paste. The aerosol-forming substrate 10 may be deposited over the entire surface of the carrier or, alternatively, may be deposited in a pattern to provide non-uniform taste delivery during use.
The cooling element 20 is arranged immediately downstream of the aerosol-forming substrate 10 and is adjacent to the aerosol-forming substrate 10. In use, the volatile material released by the aerosol-forming substrate 10 after being heated passes along the cooling element 20 towards the proximal end 41 of the aerosol-generating article and may cool down within the cooling element 20 to form an aerosol for inhalation by a user. In the preferred embodiment shown in fig. 1, the cooling element 20 includes a cavity that extends along the length of the cooling element 20. By the above axially extending cavities, the air flow through the cooling element 20 is in the longitudinal direction without substantial radial deviation. The cooling element 20 may act to cool the temperature of the aerosol stream drawn through the cooling element 20 by means of heat transfer. The components of the aerosol will interact with the space within the cooling element 20 and lose thermal energy.
In some embodiments, the temperature of the aerosol stream may decrease by more than 10 degrees celsius as it is drawn through the cooling element 20. In some embodiments, the temperature of the aerosol stream may decrease by more than 25 degrees celsius or more than 30 degrees celsius as it is drawn through the cooling element 20.
The suction nozzle 30 is arranged immediately downstream of the cooling element 20 and abuts against the cooling element 20. In the embodiment shown in fig. 1, the mouthpiece 30 may be a conventional cellulose acetate or polypropylene tow filter.
To assemble the aerosol-generating article, the three elements described above are aligned and tightly wrapped within the outer wrapper 40. In the embodiment shown in fig. 1, the outer wrapper 40 may be conventional cigarette paper.
The aerosol-generating article shown in fig. 1 is designed to be engaged by an aerosol-generating device comprising a heating element for inhalation by a user. In use, the heating element of the aerosol-generating device heats the aerosol-forming substrate 10 of the aerosol-generating article to a temperature sufficient to generate an aerosol which is drawn downstream through the aerosol-generating article and inhaled by a user.
One embodiment of the present application also proposes an infrared absorbing material configured to absorb infrared radiation that heats the aerosol-forming substrate 10. In a preferred embodiment, the absorption peak of the infrared absorbing material is correlated to the absorption peak of moisture in the aerosol-forming substrate. In this way, the infrared absorption material absorbs radiation and heats the infrared rays of the aerosol forming substrate 10, so that the evaporated and atomized moisture is reduced in a certain proportion, the phenomenon that the smoker generates a burning sensation during smoking due to the fact that the vapor with higher heat is contained is avoided, and particularly, the temperature of the first-mouth smoking aerosol is reduced, and the smoking experience of a user is improved; meanwhile, after the temperature of the infrared absorbing material is increased, the infrared absorbing material can be heated and atomized together to form the matrix 10, so that the heating efficiency of the product is improved to a certain extent.
In one example, the wavelength range of the absorption peak of the infrared absorbing material at least partially coincides with the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate 10. Specifically, the wavelength range of the absorption peak of the infrared absorbing material is within the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate 10; alternatively, the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate 10 is within the wavelength range of the absorption peak of the infrared absorbing material; alternatively, the wavelength range of the absorption peak of the infrared absorbing material partially coincides with the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate 10; alternatively, the wavelength range of the absorption peak of the infrared absorbing material is exactly the same as the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate 10.
In one example, the infrared absorbing material has an absorption peak in the wavelength range of 3 μm to 5 μm.
In one example, the infrared absorbing material is in at least one of the following forms: powder, granules, pellets, chips, strands, ribbons or sheets. An infrared absorbing material may be disposed between the aerosol-forming substrate 10 and the outer wrapper 40, for example, a sheet-shaped infrared absorbing material is sandwiched between the aerosol-forming substrate 10 and the outer wrapper 40; alternatively, an infrared absorbing material is disposed within the aerosol-forming substrate 10.
Taking the infrared absorbing material as a particle form, as shown in fig. 1, 11 in the figure represents a particle-shaped aerosol-forming substrate, 12 represents moisture in the particle-shaped aerosol-forming substrate, and 13 represents the particle-shaped infrared absorbing material; the particulate infrared absorbing material is mixed with the particulate aerosol-forming substrate and its moisture. When the product is heated by infrared radiation, the granular infrared absorbing material absorbs infrared rays of 3-5 mu m together with moisture; in this way, the evaporation and atomization of the water is reduced in a certain proportion, so that the phenomenon that the water vapor with high heat content causes burning sensation to the user during sucking is avoided, and the temperature of the first sucking air fog is reduced. Meanwhile, the temperature of the granular infrared absorbing material is increased after the granular infrared absorbing material absorbs the radiant heat, and the granular aerosol forming substrate adjacent to the granular infrared absorbing material is heated and atomized, so that the heating efficiency of the product is improved to a certain extent.
In one example, the infrared absorbing material includes at least one of a metal, an inorganic non-metal, an organic, and a super-absorbing material. For example, metals include, but are not limited to, copper, nickel; inorganic nonmetallic materials include, but are not limited to, silicon carbide, graphene; organics include, but are not limited to, sucrose, fiber; superabsorbent material: the surface microstructure of the substance is regulated so that the substance only absorbs infrared rays of 3-5 mu m.
In one example, the mass fraction of infrared absorbing material is between 2% and 30% based on the total mass of the aerosol-forming substrate 10 and the infrared absorbing material; preferably, between 2% and 25%; further preferably, between 2% and 20%; further preferably, between 2% and 15%; more preferably, the content is 5 to 15%.
The above outer wrapper 40 is preferably made of an infrared transmitting material. For example, the inorganic fiber material is used for preparation, and specifically comprises one or more of hydroxyapatite fiber, silicon carbide fiber and barium titanate fiber.
The above hydroxyapatite fiber, silicon carbide fiber, barium titanate fiber are excellent infrared-transmitting materials so that the outer wrapper 40 is substantially non-infrared-absorbing when the aerosol-generating article is heated by means of infrared radiation, thereby effectively promoting the heating efficiency of the inner aerosol-forming substrate 10.
Further to facilitate verification of the feasibility of aerosol-generating articles employing the above infrared absorbing materials, and the advancement in properties of the produced aerosol-generating articles, the produced aerosol-generating articles are illustrated by the following specific examples and test results.
S11, preparing a plant-based material of an aerosol-forming substrate; for example: tobacco material.
S12, preparing an infrared absorption material.
Silicon carbide material may be used, wherein the mass fraction of the silicon carbide material is 10% and the particle size is 24 mesh.
Graphene materials may also be employed, wherein the mass fraction of the graphene material is 10%.
The steps S11 and S12 may be not sequential.
S13, after the plant-based material is mixed with the infrared absorbing material, the mixture can be prepared by adopting a conventional product technology to obtain an aerosol generating product.
The preparation can be carried out using a particulate product process to obtain a particulate aerosol generating article.
The product can also be prepared by adopting the conventional reconstituted tobacco type product technology (such as a paper making method, a dry method, a thick slurry method, a rolling method and the like) so as to obtain an aerosol product of reconstituted tobacco type.
The above-mentioned product processes can be referred to in the art, for example: dong Gaofeng, tian Yongfeng, shang Shanzhai, etc. the development of reconstituted tobacco production process for heating non-combustible (HnB) cigarettes [ J ]. Chinese journal of tobacco, 2020, 26 (1) ", are not described in detail herein.
The aerosol-generating articles prepared in the above examples were subjected to an aerosol temperature test and a TPM value change rate test, the contents of which were all compared using conventional heated non-flammable articles.
1. Aerosol temperature test
Test purpose: testing the aerosol temperature of the article upon suction
Test environment: ambient temperature: 25 ℃, relative humidity: 65RH%.
Test instrument: the temperature sensor adopts a K-type thermocouple; temperature recorder: GRAPHTEC GL240, 240; a smoke extractor: the self-contained device is used.
Testing working conditions: operating condition setting of the smoke extractor: suction volume 55ml/3s, suction interval time: 27s; setting an aerosol temperature acquisition point: the K-type thermocouple is arranged in the center of the end face of the product suction nozzle; data recording frequency: the data is recorded once at 10Hz, i.e. 100 ms.
The testing steps are as follows:
s31, inserting the tested product into the aerosol generating device; among them, the tested articles included the aerosol-generating articles prepared in example 1, example 2, and conventional heated non-combustible articles; the same aerosol generating device is adopted for each test to ensure that the heating working conditions of the products are the same; multiple products can be tested by the same product to ensure test results;
s32, arranging a K-type thermocouple in the center of the end face of the tested product suction nozzle;
s33, connecting a K-type thermocouple with a temperature recorder;
s34, starting an aerosol generating device to preheat the product, and simultaneously starting a smoke extractor and recording temperature data;
s35, after the preheating is finished, the smoke is sucked by the smoke extractor and temperature data at the time of suction is recorded.
The tested product is a conventional heating non-combustible product, and the test result can be referred to in fig. 2;
the tested product adopts silicon carbide material as infrared absorption material, wherein the mass fraction of the silicon carbide material is 10%, and the granularity is 24 meshes; the test results of the particulate aerosol-generating article prepared by the particulate article process are shown in fig. 3;
the tested product adopts graphene material as infrared absorption material, wherein the mass fraction of the graphene material is 10%; the test result of the aerosol product of the reconstituted tobacco type prepared by adopting the conventional reconstituted tobacco type product process can be referred to as figure 4.
As can be seen from the test results of fig. 2-4, the aerosol-generating article of fig. 3 has a first port of the aerosol-generating article reduced in temperature by about 5 ℃ relative to a conventional heated non-combustible article; the aerosol-generating article of fig. 4 shows a first oral aerosol-generating article having a temperature of about 4 c. It is apparent that the problem of burning pain when the user sucks on the first mouth is reduced.
2. TPM value change rate test
Test purpose: the rate of change of the TPM values of the aerosol product article 1 and the aerosol generating article 2 relative to conventional heated nonflammable articles was tested.
Wherein the aerosol product 1 adopts silicon carbide material as infrared absorption material, the mass fraction of the silicon carbide material is 10%, and the granularity is 24 meshes; a particulate aerosol-generating article prepared by employing a particulate article process; the aerosol product 2 adopts graphene material as infrared absorption material, wherein the mass fraction of the graphene material is 10%; the reconstituted tobacco type aerosol product is prepared by adopting a conventional reconstituted tobacco type product process.
The testing steps are as follows:
s41, testing the quality of the conventional heated non-combustible product, aerosol-generating product 1 and aerosol-generating product 2 before and after suction, and calculating the weight loss value, as shown in the following table:
s42, calculating the TPM value change rate of the aerosol generating product 1 according to the TPM values of the conventional heating non-combustion product and the aerosol generating product 1, wherein the TPM value change rate is calculated according to the following calculation process:
similarly, the TPM value change rate of the resulting aerosol-generating article 2 was about 6.9%.
As can be seen from the above test results, compared with the conventional heating non-combustible product, the TPM value change rate of the aerosol-generating product 1 and the aerosol-generating product 2 is improved, and thus the sucking experience of a user is improved.
Further presented herein is an aerosol-generating system comprising the above aerosol-generating article and a heating device, the configuration in one embodiment being shown with reference to fig. 5;
the heating device 200 includes a heating element 210;
wherein the heating element 210 is tubular in shape, at least a portion of which tubular hollow is configured as a chamber for receiving the aerosol-generating article 100, the heating element 210 heating the aerosol-generating article 100 by radiating infrared rays towards the aerosol-generating article 100. The aerosol-generating article 100 may be referred to in the foregoing and will not be described in detail herein.
When the heating element 210 using the above infrared radiation is used for heating, the infrared absorbing material in the aerosol generating product 100 absorbs the infrared radiation to heat the aerosol to form the matrix, so that the evaporated and atomized moisture is reduced in a certain proportion, the phenomenon that the user easily generates burning sensation during suction due to the fact that the water vapor with higher heat is avoided, particularly the temperature of the first-mouth suction aerosol is reduced, and the suction experience of the user is improved; meanwhile, after the temperature of the infrared absorption material is increased, the infrared absorption material can be heated and atomized to form a matrix, so that the heating efficiency of the product is improved to a certain extent.
It should be noted that the description and drawings of the present application show preferred embodiments of the present application, but are not limited to the embodiments described in the present application, and further, those skilled in the art can make modifications or changes according to the above description, and all such modifications and changes should fall within the scope of the appended claims.
Claims (12)
1. An aerosol-generating article comprising an outer wrapper, and an aerosol-forming substrate and an infrared absorbing material confined within the outer wrapper;
the aerosol-forming substrate being configured to produce an aerosol for inhalation when heated;
the infrared absorbing material is configured to absorb infrared light for radiation heating the aerosol-forming substrate;
wherein the wavelength range of the absorption peak of the infrared absorbing material at least partially coincides with the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate.
2. The aerosol-generating article of claim 1, wherein the aerosol-generating article comprises,
the wavelength range of the absorption peak of the infrared absorbing material is within the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate; or alternatively, the process may be performed,
the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate is within the wavelength range of the absorption peak of the infrared absorbing material; or alternatively, the process may be performed,
the wavelength range of the absorption peak of the infrared absorbing material partially coincides with the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate; or alternatively, the process may be performed,
the wavelength range of the absorption peak of the infrared absorbing material is exactly the same as the wavelength range of the absorption peak of the moisture in the aerosol-forming substrate.
3. The aerosol-generating article of claim 1, wherein the infrared absorbing material is at least one of the following shapes:
powdery, granular, pellet, chip, wire, ribbon or sheet.
4. The aerosol-generating article of claim 1, wherein the infrared absorbing material is disposed between the aerosol-forming substrate and the outer wrapper; alternatively, the infrared absorbing material is disposed within the aerosol-forming substrate.
5. The aerosol-generating article of claim 1, wherein the infrared absorbing material is bonded to a portion of the aerosol-forming substrate; wherein the portion of the aerosol-forming substrate is disposed proximate a downstream end of the aerosol-forming substrate.
6. The aerosol-generating article of claim 1, wherein the infrared absorbing material comprises at least one of a metal, an inorganic non-metal, an organic, and a superabsorbent material.
7. The aerosol-generating article of claim 1, wherein the infrared absorbing material comprises a mass fraction of from 2% to 30% based on the total mass of the aerosol-forming substrate and the infrared absorbing material; preferably, between 2% and 25%; further preferably, between 2% and 20%; further preferably, between 2% and 15%; more preferably, the content is 5 to 15%.
8. The aerosol-generating article according to claim 1, further comprising a mouthpiece confined within the outer wrapper, the mouthpiece being disposed downstream of the aerosol-forming substrate.
9. The aerosol-generating article according to claim 8, further comprising a cooling element confined within the outer wrapper, the cooling element being disposed between the aerosol-forming substrate and the mouthpiece.
10. An aerosol-generating article comprising an outer wrapper, and an aerosol-forming substrate and an infrared absorbing material confined within the outer wrapper;
the aerosol-forming substrate being configured to produce an aerosol for inhalation when heated;
the infrared absorbing material is configured to absorb infrared light for radiation heating the aerosol-forming substrate;
wherein the infrared absorbing material has an absorption peak wavelength ranging from 3 μm to 5 μm.
11. A method of making an aerosol-generating article, the method comprising:
preparing an aerosol-forming substrate;
preparing an infrared absorbing material;
the aerosol-forming substrate is mixed with the infrared absorbing material and then prepared using conventional manufacturing techniques to provide the aerosol-generating article.
12. An aerosol-generating system comprising an aerosol-generating device, the aerosol-generating article of any of claims 1 to 10, the aerosol-generating device being configured to radiate infrared radiation to heat the aerosol-generating article to generate an aerosol for inhalation.
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CN113100493A (en) * | 2020-01-13 | 2021-07-13 | 深圳市合元科技有限公司 | Smoking article |
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