WO2023111632A1

WO2023111632A1 - Atmosphere furnace control

Info

Publication number: WO2023111632A1
Application number: PCT/IB2021/061686
Authority: WO
Inventors: Morvan PLUNIAN; Ahmed KHELASSI; Walter DAL'MAZ SILVA
Original assignee: Arcelormittal
Priority date: 2021-12-14
Filing date: 2021-12-14
Publication date: 2023-06-22
Also published as: WO2023111837A1

Abstract

The invention relates to a method for regulating an atmosphere A inside a furnace, wherein a steel strip having a composition and an exposed surface area A₁ is heat treated from a time T₀ to a time T_S1END and a steel strip, having a composition and an exposed surface area is heat treated from a time T_S2START to a time T_N, comprising the following steps: a data acquisition step, an optimisation step and an injection of H₂O.

Description

ATMOSPHERE FURNACE CONTROL The present invention relates to a regulating method of furnace atmosphere during the heat treatment of a steel strip. More particularly, the method can be used during an annealing of a steel strip. During the annealing of a steel strip, the latter is heated and then maintained above its recrystallisation temperature in order to increase its ductility and reduce its hardness. This is done in a furnace wherein the temperature and the dew point of its atmosphere are regulated. Controlling the atmosphere is key to ensure the strip quality. The tuning of the temperature is ensured by heating devices (radiant tubes, inductors, …) providing a desired quantity of heat. The tuning of the dew point is ensured by providing water, e.g. in the form of vapour, to the atmosphere. Each steel grade and format have preferred process conditions, including a preferred furnace atmosphere, i.e. ranges of temperature and dew point. So, for continuous production line manufacturing different grades and formats of steel strip, the furnace atmosphere needs to be adapted for each product. During a product transition, shorter is the time from one furnace atmosphere to another, better is the achievable quality of the product. In order to regulate the dewpoint, the existing system uses a Proportional Integral Derivative controller (PID controller) which is a part of the control loop mechanism coupled with a dew point measuring device and a system to inject water. In this system, as illustrated in Figure 1, the dew point of the atmosphere is measured (DP_MEASURED) and a targeted dew point (DP_TARGET) is defined. Then an error value, e.g. a difference between the measured dew point and the targeted dew point, is calculated. After that, a flow of H₂O to inject (H₂O_INJECT) is determined based on proportional, integral and derivative terms calculated by the PID controller. Ultimately, the determined flow of H₂O is injected into the furnace. This sequence is regularly repeated throughout the heat treatment. However, it is key to remember that an annealing furnace has usually an important volume compared to the flow of vapour that can be injected in the furnace. So, when two steels grades requiring different dew points in the furnace are sent consecutively in a short period of time, an optimal dew point cannot be achieved on time over the full coil length. It may lead to a yield decrease or a poor strip quality, especially for the tail of the first strip and head of the second one. The goal of the invention is to improve the regulation of the H₂O injected in a section of an annealing furnace. More particularly, the goal of the invention is to improve the transition management from a preferred annealing atmosphere A_TAR1 of a steel strip S₁ to a preferred annealing atmosphere A_TAR2 of a steel strip S₂, in a section of a furnace leading to an optimised quality of the final products. The preferred annealing atmosphere can comprise a range of values. This object is achieved by providing a method according to claim 1. The method can also comprise any characteristics of claims 2 to 7. Other characteristics and advantages of the invention will become apparent from the following detailed description of the invention. To illustrate the invention, various embodiment and trials of non-limiting example will be described, particularly with reference to the following figures: Figure 1 illustrates a regulation method as known in the prior art. Figure 2 illustrates an embodiment of the regulation system as per the present invention. Figure 3A illustrates the dew point regulation as known in the prior art. Figure 3B illustrates the steam injection regulation as known in the prior art Figure 4A illustrates the dew point regulation according to the invention. Figure 3B illustrates the steam injection regulation according to the invention The invention, as illustrated in Figure 2, relates to a method for regulating an atmosphere A, comprising H₂ and N₂, inside a furnace, wherein a steel strip S₁ having a composition range C₁ and an exposed surface area A_SURF1 is heat treated from a time T₀ to a time T_S1END and a steel strip S₂, having a composition range C₂ and an exposed surface area A_SURF2 is heat treated from a time T_S2START to a time T_N, comprising the following steps: A. A data acquisition step wherein : i. at a time T₀, the dew point, DP₀, of said atmosphere A is measured, ii. a target atmosphere, A_TAR1, for said steel strip S1 is retrieved, wherein said target atmosphere A_TAR1 comprises at least a dew point value, iii. a target atmosphere, A_TAR2, for said steel strip S₂ is retrieved, wherein said target atmosphere A_TAR2 comprises at least a dew point value, B. A tuning step comprising the steps of : i. defining N projected atmospheres, A_PRO-1 to A_PRO-N, corresponding at N times, T₁ to T_N, based on: a) said dew point, DP₀, of said atmosphere measured at the time T₀, b) the volume of said furnace, c) the composition ranges and the exposed surface areas of said steel strips S1 and S2 inside said furnace for each of said times T₁ to T_N, ii. an amount of H₂O to be injected, Q_H2O, at T₁ inside said furnace is estimated using a model predictive control controller using the following data : a) said projected atmospheres A_PRO-1 to A_PRO-N b) said target atmospheres A_TAR1 and A_TAR2 c) said volume and the renewal flow of N2 and H2 of said furnace, d) the composition range and the exposed surface area of said steel strip S1 at T₁, C. Injecting at T₁, said estimated amount of H₂O. The furnace comprises heating means. The heating means can be for example inductors and/or radiant elements such as tubes. The furnace can comprise several sections such as a pre-heating section, a heating section, a soaking section and a cooling section. The method can be applied to each and every section of a furnace. Preferably, the method is applied in the heating and/or in the soaking section. The heat treatment can be any type of heat treatment. The heat treatment is preferably an annealing treatment, and more particularly a recrystallisation annealing The steel strip S1 and the steel strip S2 can have the same composition or similar compositions corresponding to the same family of products. The steel strip S1 and the steel strip S2 can have different compositions. Preferably, the steel strip comprises, in weight percent, from 0.0001% to 0.50% of C, from 0.01% to 5.0% of Mn, from 0.001% to 5.0% of Si. The exposed surface area of a steel strip represents the surface of a steel strip inside the furnace and exposed to the furnace atmosphere. The exposed surface can be expressed per unit or per volume area. T_S1END is the first step at which the strip S₁ is not in the furnace. In other words, it is the first time at which A_SURF1 is equal to zero. T_S2START is the first step at which the strip S₂ is in the furnace, at least partly. In other words, it is the first time at which A_SURF2 is not equal to zero. In the first step, the data acquisition step, the dew point of the atmosphere is measured and the targeted dew point for each steel strips undergoing a heat treatment in any of the times T₁ to T_N are retrieved. The targeted dew point can also be a targeted range of dew point so the target atmospheres, A_TAR1 and/or A_TAR2, can comprise a range of dew point values. A target atmosphere of a steel strip permits to perform the continuous heat treatment ensuring a satisfying product quality. The dew point values or ranges depends on the steel composition. They can, for example, be retrieved from a database. In the second step, the tuning step, the goal is to estimate the atmosphere of the furnace at N times (T₁ to T_N), i.e. at N steps, which correspond to N projected atmospheres ( A_PRO-1 to A_PRO-N ) if no water is added inside the furnace (e.g. the atmosphere) while determining the required water injection flow rate at each step. Preferably, N is a positive integer from 2 to 100. Even more preferably, N is a positive integer from 5 to 50. Even more preferably, N is a positive integer from 10 to 30. Preferably, each of said times T₀ to T_N are spaced apart by 5 seconds to 1 minute. Even more preferably, each of the times T₀ to T_N are spaced apart by 15 seconds to 45 seconds. Preferably, each of the times T₀ to T_N are spaced from the same period of time. For example, if N=50 and that each of the times are spaced of 10 seconds : T₀ is at a time t=0 second, T₁ is at a time t=10 seconds, T₂ is at a time t=20 seconds and T_N=T₅₀ is at a time t=500 seconds. The definition of the projected atmospheres, A_PRO-1 to A_PRO-N, is done using the dew point measured in step A.i., the volume of the furnace, the composition and the exposed surface area of the steel strip inside said furnace for each of said times T₁ to T_N. Such estimation of projected atmospheres are well known by the skilled in the art. It is possible that at one or several steps, the strip S₁ and the strip S₂ are partly in the furnace at the same time, e.g; this is notably the case when two strips are welded one to another. In that case, T_S2START happens before T_S1END. In that case, the definition of the projected atmosphere is done using the compositions and the surface areas of each of the strip in the furnace. It is also possible that at one or several steps, no strip is in the furnace, e.g; this is notably the case when T_S2START happens after T_S1END. The definition of the projected atmospheres is preferably done assuming that the temperature and the pressure of said atmosphere are constant for the steps T₁ to T_N. Preferably, said target atmospheres, A_TAR1 and A_TAR2, comprises at least a minimum and a maximum for the H2 concentration, a maximum for the CO concentration. Even more preferably, said target atmospheres, comprises from 0.1 to 50% by volume of H2. Even more preferably, said target atmospheres, comprises from 1 to 50% by volume of H2. Then the amount of H₂O to inject at T₁ in the furnace, Q_H2O, is estimated. This is done by using a model predictive control (MPC) taking into account - the projected atmospheres determined in step B.i., - the target atmospheres retrieved in step A.ii., - the volume and the renewal flow of N₂ and H₂ of the furnace, - the composition range and the exposed surface area of the steel strip S1 at T1. Alternatively, in the step B. ii, a flow of H₂O, or steam, to be injected at T₁ inside said furnace can be estimated using a model predictive control controller using the following data : a) said projected atmospheres A_PRO-1 to A_PRO-N b) said target atmospheres A_TAR1 and A_TAR2 c) said volume and the renewal flow of N₂ and H₂ of said furnace, d) the composition range and the exposed surface area of the steel strip S1 at T₁. In the fifth step, the amount, or the flow, of H₂O defined in the step B.ii. is injected into the furnace. This injection can be done by directly injecting water into the furnace or by means of a porter gas. The present invention permits to have an atmosphere inside a furnace closer to the setpoint value. The present invention is particularly advantageous when there is a strip composition and/or set-point change in the furnace. The invention also relates to a method for regulating an atmosphere A, comprising H2 and N2, inside a furnace, wherein a steel strip S₁ having a composition range C₁ and an exposed surface area A1 is heat treated from a time T₀ to a time T_N, comprising the following steps: A. A data acquisition step wherein : i. at a time T₀, the dew point, DP₀, of said atmosphere A is measured, ii. a target atmosphere, A_TAR1, for said steel strip S1 is retrieved, wherein said target atmosphere A_TAR1 comprises at least a dew point value, B. An tuning step comprising the steps of : i. defining N projected atmospheres, A_PRO-1 to A_PRO-N, for n times, T₁ to T_N, based on: a) said dew point, DP₀, of said atmosphere measured at the time T₀, b) the volume of said furnace, c) the composition range and the exposed surface area of said steel strip S₁ inside said furnace for each of said times T₁ to T_N, ii. an amount of H₂O to be injected, Q_H2O, at T₁ inside said furnace is estimated using a model predictive control controller using the following data : a) said projected atmospheres A_PRO-1 to A_PRO-N b) said target atmosphere A_TAR1 c) said volume and the renewal flow of H2 and N2 of said furnace, d) the composition range and the exposed surface area of said steel strip S₁ inside said furnace at T₁, C. Injecting at T₁, said estimated amount of H₂O. EXPERIMENTAL RESULTS In order to assess the impact of the present method on a furnace atmosphere regulation, an atmosphere is modelled for a transition between an Interstitial Free steel, of the type sold by ArcelorMittal, and a Dual Phase 780 steel, of the type sold by ArcelorMittal, for two regulation methods. In a first simulation, the atmosphere is a regulated using a PID controller. In a second simulation, the atmosphere is regulated using the claimed method. In both simulations, the Interstitial Free steel strip requires a dew point of -30°C and is in the furnace from the minute 0 to the minute 9.5 whereas the Dual Phase 780 steel strip requires a dew point of -15°C and is in the furnace from the minute 9.5 to the minute 20. For each target dewpoint, there is a tolerance of 5.10^-4 of the molar fraction of H₂O. So, for the target dewpoint of 30°C, the tolerance is of ±8°C and for the target dewpoint of -15°C the tolerance is of ± 3°C. For both simulations, the measured dewpoint (continuous line), the targeted dewpoint (thick dash line) and the tolerances (thin dash lines) are plotted in Figure 3A, for the first simulation, and in Figure 4A, for the second simulation. Moreover, the steam injection is also plotted in Figure 3B, for the first simulation, and in Figure 4B, for the second simulation. In the first simulation, the time spent outside of the tolerance ranges is of 14% whereas in the second simulation, according to the claimed method, the time spent outside of the tolerance ranges is of only 4%. So, with the claimed method, the time spend outside of the tolerances ranges is divided by 3.5 in this example.

Claims

CLAIMS 1. A method for regulating an atmosphere A, comprising H₂ and N₂, inside a furnace, wherein a steel strip S₁ having a composition range C₁ and an exposed surface area A_SURF1 is heat treated from a time T₀ to a time T_S1END and a steel strip S₂, having a composition range C₂ and an exposed surface area A_SURF2 is heat treated from a time T_S2START to a time T_N, comprising the following steps: A. A data acquisition step wherein : i. at a time T₀, the dew point, DP₀, of said atmosphere A is measured, ii. a target atmosphere, A_TAR1, for said steel strip S1 is retrieved, wherein said target atmosphere A_TAR1 comprises at least a dew point value, iii. a target atmosphere, A_TAR2, for said steel strip S2 is retrieved, wherein said target atmosphere A_TAR2 comprises at least a dew point value, B. A tuning step comprising the steps of : i. defining N projected atmospheres, A_PRO-1 to A_PRO-N, corresponding at N times, T₁ to T_N, based on: a) said dew point, DP₀, of said atmosphere measured at the time T₀, b) the volume of said furnace, c) the composition ranges and the exposed surface areas of steel strips S1 and S2 inside said furnace for each of said times T₁ to T_N, ii. an amount of H₂O to be injected, Q_H2O, at T₁ inside said furnace is estimated using a model predictive control controller using the following data : a) said projected atmospheres A_PRO-1 to A_PRO-N b) said target atmospheres A_TAR1 and A_TAR2 c) said volume and the renewal flow of N2 and H2 of said furnace, d) the composition range and the exposed surface area of the steel strip S1 at T₁, C. Injecting at T₁, said estimated amount of H₂O.

2. Method according to claim 1, wherein said heat treatment is an annealing.

3. Method according to any one of claims 1 or 2, wherein said steel strip comprises, in weight percent, from 0.0001% to 0.50% of C, from 0.01% to 5.0% of Mn, from 0.001% to 5.0% of Si.

4. Method according to any one of claims 1 to 3 wherein, N is a positive integer from 2 to 100.

5. Method according to any one of claims 1 to 4, wherein each of said times T₀ to T_N are spaced from 5 seconds to 1 minute apart 6. Method according to any one of claims 1 to 5, wherein in step B.i., said definition is done assuming that the temperature and the pressure of said atmosphere are constant for the times T₁ to T_N. 7. A method for regulating an atmosphere A, comprising H2 and N2, inside a furnace, wherein a steel strip S₁ having a composition range C₁ and an exposed surface area A1 is heat treated from a time T₀ to a time T_N, comprising the following steps: D. A data acquisition step wherein : i. at a time T₀, the dew point, DP₀, of said atmosphere A is measured, ii. a target atmosphere, A_TAR1, for said steel strip S1 is retrieved, wherein said target atmosphere A_TAR1 comprises at least a dew point value, E. An tuning step comprising the steps of : i. defining n projected atmospheres, A_PRO-1 to A_PRO-N, for n times, T₁ to T_N, based on: d) said dew point, DP₀, of said atmosphere measured at the time T₀, e) the volume of said furnace, f) the composition range and the exposed surface area of said steel strip S₁ inside said furnace for each of said times T₁ to T_N, ii. a flow of H₂O to be injected, Q_H2O, at T₁ inside said furnace is estimated using a model predictive control controller using the following data : e) said projected atmospheres A_PRO-1 to A_PRO-N f) said target atmosphere A_TAR1 g) said volume and the renewal flow of H2 and N2 of said furnace, h) the composition range and the exposed surface area of said steel strip S₁ inside said furnace at T₁, F. Injecting at T₁, said estimated amount of H₂O.