WO2022021526A1 - 一种驱蚊抗菌织物制备方法 - Google Patents
一种驱蚊抗菌织物制备方法 Download PDFInfo
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- WO2022021526A1 WO2022021526A1 PCT/CN2020/112074 CN2020112074W WO2022021526A1 WO 2022021526 A1 WO2022021526 A1 WO 2022021526A1 CN 2020112074 W CN2020112074 W CN 2020112074W WO 2022021526 A1 WO2022021526 A1 WO 2022021526A1
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- Prior art keywords
- fabric
- mosquito repellent
- antibacterial
- extract
- treatment
- Prior art date
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- 239000004744 fabric Substances 0.000 title claims abstract description 82
- 239000000077 insect repellent Substances 0.000 title claims abstract description 54
- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 49
- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 30
- 239000007788 liquid Substances 0.000 claims abstract description 20
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims abstract description 18
- 235000017491 Bambusa tulda Nutrition 0.000 claims abstract description 18
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims abstract description 18
- 239000011425 bamboo Substances 0.000 claims abstract description 18
- 238000000227 grinding Methods 0.000 claims abstract description 15
- 238000010992 reflux Methods 0.000 claims abstract description 12
- 229920000742 Cotton Polymers 0.000 claims abstract description 11
- 238000002156 mixing Methods 0.000 claims abstract description 11
- 239000000843 powder Substances 0.000 claims abstract description 11
- 239000000835 fiber Substances 0.000 claims abstract description 10
- 239000003610 charcoal Substances 0.000 claims abstract description 9
- 235000006679 Mentha X verticillata Nutrition 0.000 claims description 14
- 235000002899 Mentha suaveolens Nutrition 0.000 claims description 14
- 235000001636 Mentha x rotundifolia Nutrition 0.000 claims description 14
- 108010059820 Polygalacturonase Proteins 0.000 claims description 14
- 108010093305 exopolygalacturonase Proteins 0.000 claims description 14
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 12
- 241000208152 Geranium Species 0.000 claims description 12
- 238000000034 method Methods 0.000 claims description 12
- 241000208720 Nepenthes Species 0.000 claims description 9
- 241000205585 Aquilegia canadensis Species 0.000 claims description 8
- 244000025254 Cannabis sativa Species 0.000 claims description 8
- 241000037740 Coptis chinensis Species 0.000 claims description 8
- 235000017089 Scutellaria baicalensis Nutrition 0.000 claims description 8
- 240000004534 Scutellaria baicalensis Species 0.000 claims description 8
- 239000007921 spray Substances 0.000 claims description 8
- 229910052757 nitrogen Inorganic materials 0.000 claims description 6
- 235000009051 Ambrosia paniculata var. peruviana Nutrition 0.000 claims description 4
- 235000003097 Artemisia absinthium Nutrition 0.000 claims description 4
- 240000001851 Artemisia dracunculus Species 0.000 claims description 4
- 235000017731 Artemisia dracunculus ssp. dracunculus Nutrition 0.000 claims description 4
- 235000003261 Artemisia vulgaris Nutrition 0.000 claims description 4
- 239000001138 artemisia absinthium Substances 0.000 claims description 4
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims description 4
- 241000208442 Sarracenia Species 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 3
- 239000007789 gas Substances 0.000 claims description 3
- 238000009832 plasma treatment Methods 0.000 claims description 3
- 230000008569 process Effects 0.000 claims description 3
- 244000082204 Phyllostachys viridis Species 0.000 claims 2
- 238000007598 dipping method Methods 0.000 claims 1
- 239000012530 fluid Substances 0.000 claims 1
- 241001330002 Bambuseae Species 0.000 abstract description 16
- 241000894006 Bacteria Species 0.000 abstract description 6
- 241000255925 Diptera Species 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 2
- 239000000686 essence Substances 0.000 abstract 3
- 235000010894 Artemisia argyi Nutrition 0.000 abstract 2
- 241001435059 Artemisia argyi Species 0.000 abstract 2
- 244000038458 Nepenthes mirabilis Species 0.000 abstract 2
- 244000270673 Pelargonium graveolens Species 0.000 abstract 2
- 235000017927 Pelargonium graveolens Nutrition 0.000 abstract 2
- 230000002265 prevention Effects 0.000 abstract 2
- 241000628997 Flos Species 0.000 abstract 1
- 241000238631 Hexapoda Species 0.000 abstract 1
- 238000009395 breeding Methods 0.000 abstract 1
- 230000001488 breeding effect Effects 0.000 abstract 1
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 238000007654 immersion Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- 206010011409 Cross infection Diseases 0.000 description 1
- 206010029803 Nosocomial infection Diseases 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 244000000010 microbial pathogen Species 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 230000003071 parasitic effect Effects 0.000 description 1
- 230000002940 repellent Effects 0.000 description 1
- 239000005871 repellent Substances 0.000 description 1
- 230000037380 skin damage Effects 0.000 description 1
- 208000017520 skin disease Diseases 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000002759 woven fabric Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
- D06M16/003—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic with enzymes or microorganisms
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
Definitions
- the invention relates to the technical field of antibacterial fabric preparation, in particular to a preparation method of mosquito repellent antibacterial fabric.
- the fabric is a flat soft piece formed by crossing, knotting, and connecting small flexible objects.
- the woven fabric is composed of yarns with a cross relationship
- the knitted fabric is composed of yarns with a kink relationship.
- the fabric is composed of yarns that have a connection relationship
- the third fabric is composed of yarns that have a cross/knot relationship. After many yarns form a stable relationship, a fabric is formed. Crossing, knotting and connection are yarns.
- the three stable structural relationships formed by the thread can keep the fabric in a stable shape and specific mechanical properties.
- Cotton fabric is porous, loose and easy to absorb various impurities. It is the carrier of reproduction and parasitic bacteria, so it has become one of the main carriers in many bacterial transmission routes. Bacteria and other pathogenic microorganisms are ubiquitous and have long been a threat to In view of human health, the bacteria growing on textiles will use the products of human metabolism - sweat, fat, dander, etc. - as nutrition and multiply rapidly. The existence of these bacteria will not only stain and damage the fabric, but also It increases the cross-infection rate in the public environment, and will cause discoloration, mildew, embrittlement and degradation of fiber products, and will also produce abnormal stimulation to human skin, and induce various skin diseases, affecting human health.
- the purpose of the present invention is to provide a method for preparing a mosquito repellent and antibacterial fabric, so as to solve the problems raised by the above-mentioned background technology.
- the present invention provides the following technical solutions: a preparation method of a mosquito repellent antibacterial fabric, the preparation method comprising the following steps:
- A at first 40% of bamboo fibers and 60% of cotton fibers are blended to make above-mentioned fabrics, honeysuckle, Coptis chinensis, Scutellaria baicalensis are mixed, add bamboo charcoal and grind evenly, then add ethanol solution and carry out reflux mixing, concentrated to obtain antibacterial liquid; Grass, Geranium geranium, Nepenthes and mint are ground into powder by a grinding machine, and PBS buffer is added to extract, and the extract is freeze-dried to obtain a mosquito repellent extract;
- the pretreated fabric is put into the pectinase solution for treatment, it is then immersed in the mosquito repellent extract for treatment, and dried after being taken out to obtain the mosquito repellent antibacterial fabric.
- the concentration of the ethanol solution in step A is 60-70wt%, and the reflux time of adding the ethanol solution is 0.5h-1h.
- step A wormwood, geranium geranium, pitcher plant and mint are added with an appropriate amount of liquid nitrogen during the grinding process to collect the fabric treatment solution.
- the pectinase solution is put into the pectinase solution for treatment and then plasma treatment is performed, the gas is nitrogen, the treatment power is 80-280W, the pressure is 50-60Pa, and the treatment time is 20-30min.
- the volume of the mosquito repellent extract in step C is controlled at 100ml-260ml, and the drying time by using a dryer after immersion is controlled at 1.5h-2h.
- the present invention mixes it with the fabric by grinding wormwood, geranium, nepenthes and mint into powder and extracting the essence therein, which can improve the repellent and insect-proof effect, and cooperate with the antibacterial fabric to have a better effect.
- Mosquito repellent and antibacterial properties can better resist external mosquitoes.
- the fabric is more comfortable to wear after wearing it, and it is not easy to breed bacteria inside when worn for a long time.
- mint can emit mint substances, which not only prevent mosquitoes, but also bring coolness. sense, increased wearing comfort.
- the present invention provides the following technical solutions: a preparation method of a mosquito repellent antibacterial fabric, the preparation method comprising the following steps:
- A at first 40% of bamboo fibers and 60% of cotton fibers are blended to make above-mentioned fabrics, honeysuckle, Coptis chinensis, Scutellaria baicalensis are mixed, add bamboo charcoal and grind evenly, then add ethanol solution and carry out reflux mixing, concentrated to obtain antibacterial liquid; Grass, Geranium geranium, Nepenthes and mint are ground into powder by a grinding machine, and PBS buffer is added to extract, and the extract is freeze-dried to obtain a mosquito repellent extract;
- the pretreated fabric is put into the pectinase solution for treatment, it is then immersed in the mosquito repellent extract for treatment, and dried after being taken out to obtain the mosquito repellent antibacterial fabric.
- a preparation method of mosquito repellent antibacterial fabric comprises the following steps:
- A at first 40% of bamboo fibers and 60% of cotton fibers are blended to make above-mentioned fabrics, honeysuckle, Coptis chinensis, Scutellaria baicalensis are mixed, add bamboo charcoal and grind evenly, then add ethanol solution and carry out reflux mixing, concentrated to obtain antibacterial liquid; Grass, Geranium geranium, Nepenthes and mint are ground into powder by a grinding machine, and PBS buffer is added to extract, and the extract is freeze-dried to obtain a mosquito repellent extract;
- the pretreated fabric is put into the pectinase solution for treatment, it is then immersed in the mosquito repellent extract for treatment, and dried after being taken out to obtain the mosquito repellent antibacterial fabric.
- Embodiment 2 is a diagrammatic representation of Embodiment 1:
- step A the concentration of the ethanol solution is 60-70wt%, and the reflux time of adding the ethanol solution is 0.5h-1h.
- a preparation method of mosquito repellent antibacterial fabric comprises the following steps:
- A at first 40% of bamboo fibers and 60% of cotton fibers are blended to make above-mentioned fabrics, honeysuckle, Coptis chinensis, Scutellaria baicalensis are mixed, add bamboo charcoal and grind evenly, then add ethanol solution and carry out reflux mixing, concentrated to obtain antibacterial liquid; Grass, Geranium geranium, Nepenthes and mint are ground into powder by a grinding machine, and PBS buffer is added to extract, and the extract is freeze-dried to obtain a mosquito repellent extract;
- the pretreated fabric is put into the pectinase solution for treatment, it is then immersed in the mosquito repellent extract for treatment, and dried after being taken out to obtain the mosquito repellent antibacterial fabric.
- step A wormwood, geranium geranium, pitcher plant and mint are added with an appropriate amount of liquid nitrogen during the grinding process to collect the fabric treatment solution.
- a preparation method of mosquito repellent antibacterial fabric comprises the following steps:
- A at first 40% of bamboo fibers and 60% of cotton fibers are blended to make above-mentioned fabrics, honeysuckle, Coptis chinensis, Scutellaria baicalensis are mixed, add bamboo charcoal and grind evenly, then add ethanol solution and carry out reflux mixing, concentrated to obtain antibacterial liquid; Grass, Geranium geranium, Nepenthes and mint are ground into powder by a grinding machine, and PBS buffer is added to extract, and the extract is freeze-dried to obtain a mosquito repellent extract;
- the pretreated fabric is put into the pectinase solution for treatment, it is then immersed in the mosquito repellent extract for treatment, and dried after being taken out to obtain the mosquito repellent antibacterial fabric.
- Embodiment 4 is a diagrammatic representation of Embodiment 4:
- step C the pectinase solution is put into the pectinase solution for treatment and then plasma treatment is carried out.
- the gas is nitrogen
- the treatment power is 80-280W
- the pressure is 50-60Pa
- the treatment time is 20-30min.
- a preparation method of mosquito repellent antibacterial fabric comprises the following steps:
- A at first 40% of bamboo fibers and 60% of cotton fibers are blended to make above-mentioned fabrics, honeysuckle, Coptis chinensis, Scutellaria baicalensis are mixed, add bamboo charcoal and grind evenly, then add ethanol solution and carry out reflux mixing, concentrated to obtain antibacterial liquid; Grass, Geranium geranium, Nepenthes and mint are ground into powder by a grinding machine, and PBS buffer is added to extract, and the extract is freeze-dried to obtain a mosquito repellent extract;
- the pretreated fabric is put into the pectinase solution for treatment, it is then immersed in the mosquito repellent extract for treatment, and dried after being taken out to obtain the mosquito repellent antibacterial fabric.
- Embodiment 5 is a diagrammatic representation of Embodiment 5:
- step C the capacity of the mosquito repellent extract is controlled at 100ml-260ml, and the drying time using a dryer after immersion is controlled at 1.5h-2h.
- a preparation method of mosquito repellent antibacterial fabric comprises the following steps:
- A at first 40% of bamboo fibers and 60% of cotton fibers are blended to make above-mentioned fabrics, honeysuckle, Coptis chinensis, Scutellaria baicalensis are mixed, add bamboo charcoal and grind evenly, then add ethanol solution and carry out reflux mixing, concentrated to obtain antibacterial liquid; Grass, Geranium geranium, Nepenthes and mint are ground into powder by a grinding machine, and PBS buffer is added to extract, and the extract is freeze-dried to obtain a mosquito repellent extract;
- the pretreated fabric is put into the pectinase solution for treatment, it is then immersed in the mosquito repellent extract for treatment, and dried after being taken out to obtain the mosquito repellent antibacterial fabric.
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Biochemistry (AREA)
- Microbiology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
本发明公开了一种驱蚊抗菌织物制备方法,其制备方法包括以下步骤:首先将40%的竹纤维与60%的棉纤维混纺制成上述织物,将金银花、黄连、黄芩混合,加入竹炭研磨均匀,随后加入乙醇溶液进行回流混合,浓缩得到抗菌液;并将艾草、香叶天竺葵、猪笼草和薄荷利用研磨机研磨成粉状。本发明通过将艾草、香叶天竺葵、猪笼草和薄荷研磨成粉状并提取其中的精华将其与织物混合,可以提高驱蚊防虫效果,而且与抗菌织物相互配合具有较好的驱蚊抗菌性能,更好的抵御外部的蚊虫,该织物制成衣物穿戴后舒适性较高,长时间穿戴内部不易滋生细菌,同时薄荷可以散发薄荷物质,不仅防蚊,还能带来清凉之感,增加了穿着的舒适性。
Description
本发明涉及抗菌织物制备技术领域,具体为一种驱蚊抗菌织物制备方法。
织物是由细小柔长物通过交叉,绕结,连接构成的平软片块物,机织物是由存在交叉关系的纱线构成的,针织物是由存在绕结关系的纱线构成的,无纺织物是由存在连接关系的纱线构成的,第三织物是由存在交叉/绕结关系的纱线构成的,众多纱线构成稳定的关系后就形成了织物,交叉,绕结和连接是纱线能构成的三种稳定结构关系,使织物保持稳定的形态和特定力学性能,分析织物中的纱线组及其运行方向、运行规律和形成的关系,可以清晰地认识各种织物。
棉织物具有多孔、疏松,容易吸附各种杂质的特点,是繁殖、寄生细菌的载体,因而成为众多的细菌传播途径中主要的载体之一,细菌等致病微生物无处不在,长期以来一直威胁着人类的健康,纺织品上滋生的细菌,会以人体新陈代谢的产物-汗水、脂肪质、皮屑等-为营养,迅速繁殖,这些细菌的存在不仅使织物被沾污、损伤,更主要的是提高了公共环境的交叉感染率,且会使纤维制品变色、发霉、脆化降解等,而且还会对人体皮肤产生异常的刺激,并诱发各种皮肤疾病,影响人体健康,近年来,国内外纺织行业对抗菌棉织物的研究及应用非常重视,新技术、新产品不断问世,应用范围不断拓展,而抗菌织物作为现在常用的面料应用极为广泛,由于抗菌织物在使用时不具有驱蚊功能,且长时间洗涤会造成织物表面皮损,影响抗菌织物的使用寿命。
本发明的目的在于提供一种驱蚊抗菌织物制备方法,以解决上述背景技术提出的问题。
为实现上述目的,本发明提供如下技术方案:一种驱蚊抗菌织物制备方法,其制备方法包括以下步骤:
A、首先将40%的竹纤维与60%的棉纤维混纺制成上述织物,将金银花、黄连、黄芩混合,加入竹炭研磨均匀,随后加入乙醇溶液进行回流混合,浓缩得到抗菌液;并将艾草、香叶天竺葵、猪笼草和薄荷利用研磨机研磨成粉状,加入PBS缓冲液浸提,浸提液冻干后制得驱蚊提取液;
B、将抗菌液和驱蚊提取液均匀喷洒在织物上,并进行烘干得到预处理织物;
C、将预处理织物放入果胶酶溶液中进行处理后,然后浸渍在驱蚊提取液中处理,取出后烘干,得到驱蚊抗菌织物。
优选的,所述在步骤A中乙醇溶液的浓度为60-70wt%,加入乙醇溶液回流时间为0.5h-1h。
优选的,所述在步骤A中艾草、香叶天竺葵、猪笼草和薄荷在研磨过程中适量添加液氮,收集得到织物处理液。
优选的,所述在步骤C中放入果胶酶溶液中进行处理再进行等离子处理,气体采用氮气,处理功率为80~280W,压强为50~60Pa,处理时间为20~30min。
优选的,所述在步骤C中驱蚊提取液的容量控制在100ml-260ml,而浸渍后利用烘干机烘干时间控制在1.5h-2h。
与现有技术相比,本发明的有益效果如下:
1、本发明通过将艾草、香叶天竺葵、猪笼草和薄荷研磨成粉状并提取其中的精华将其与织物混合,可以提高驱蚊防虫效果,而且与抗菌织物相互配合具有较好的驱蚊抗菌性能,更好的抵御外部的蚊虫,该织物制成衣物穿戴后舒适性较高,长时间穿戴内部不易滋生细菌,同时薄荷可以散发薄荷物质,不仅防蚊,还能带来清凉之感,增加了穿着的舒适性。
下面将结合本发明实施例中,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。
为实现上述目的,本发明提供如下技术方案:一种驱蚊抗菌织物制备方法,其制备方法包括以下步骤:
A、首先将40%的竹纤维与60%的棉纤维混纺制成上述织物,将金银花、黄连、黄芩混合,加入竹炭研磨均匀,随后加入乙醇溶液进行回流混合,浓缩得到抗菌液;并将艾草、香叶天竺葵、猪笼草和薄荷利用研磨机研磨成粉状,加入PBS缓冲液浸提,浸提液冻干后制得驱蚊提取液;
B、将抗菌液和驱蚊提取液均匀喷洒在织物上,并进行烘干得到预处理织物;
C、将预处理织物放入果胶酶溶液中进行处理后,然后浸渍在驱蚊提取液中处理,取出后烘干,得到驱蚊抗菌织物。
实施例一:
一种驱蚊抗菌织物制备方法,其制备方法包括以下步骤:
A、首先将40%的竹纤维与60%的棉纤维混纺制成上述织物,将金银花、黄连、黄芩混合,加入竹炭研磨均匀,随后加入乙醇溶液进行回流混合,浓缩得到抗菌液;并将艾草、香叶天竺葵、猪笼草和薄荷利用研磨机研磨成粉状,加入PBS缓冲液浸提,浸提液冻干后制得驱蚊提取液;
B、将抗菌液和驱蚊提取液均匀喷洒在织物上,并进行烘干得到预处理织物;
C、将预处理织物放入果胶酶溶液中进行处理后,然后浸渍在驱蚊提取液中处理,取出后烘干,得到驱蚊抗菌织物。
实施例二:
在实施例一中,再加上下述工序:
在步骤A中乙醇溶液的浓度为60-70wt%,加入乙醇溶液回流时间为0.5h-1h。
一种驱蚊抗菌织物制备方法,其制备方法包括以下步骤:
A、首先将40%的竹纤维与60%的棉纤维混纺制成上述织物,将金银花、黄连、黄芩混合,加入竹炭研磨均匀,随后加入乙醇溶液进行回流混合,浓缩得到抗菌液;并将艾草、香叶天竺葵、猪笼草和薄荷利用研磨机研磨成粉状,加入PBS缓冲液浸提,浸提液冻干后制得驱蚊提取液;
B、将抗菌液和驱蚊提取液均匀喷洒在织物上,并进行烘干得到预处理织物;
C、将预处理织物放入果胶酶溶液中进行处理后,然后浸渍在驱蚊提取液中处理,取出后烘干,得到驱蚊抗菌织物。
实施例三:
在实施例二中,再加上下述工序:
在步骤A中艾草、香叶天竺葵、猪笼草和薄荷在研磨过程中适量添加液氮,收集得到织物处理液。
一种驱蚊抗菌织物制备方法,其制备方法包括以下步骤:
A、首先将40%的竹纤维与60%的棉纤维混纺制成上述织物,将金银花、黄连、黄芩混合,加入竹炭研磨均匀,随后加入乙醇溶液进行回流混合,浓缩得到抗菌液;并将艾草、香叶天竺葵、猪笼草和薄荷利用研磨机研磨成粉状,加入PBS缓冲液浸提,浸提液冻干后制得驱蚊提取液;
B、将抗菌液和驱蚊提取液均匀喷洒在织物上,并进行烘干得到预处理织物;
C、将预处理织物放入果胶酶溶液中进行处理后,然后浸渍在驱蚊提取液中处理,取出后烘干,得到驱蚊抗菌织物。
实施例四:
在实施例三中,再加上下述工序:
在步骤C中放入果胶酶溶液中进行处理再进行等离子处理,气体采用氮气,处理功率为80~280W,压强为50~60Pa,处理时间为20~30min。
一种驱蚊抗菌织物制备方法,其制备方法包括以下步骤:
A、首先将40%的竹纤维与60%的棉纤维混纺制成上述织物,将金银花、黄连、黄芩混合,加入竹炭研磨均匀,随后加入乙醇溶液进行回流混合,浓缩得到抗菌液;并将艾草、香叶天竺葵、猪笼草和薄荷利用研磨机研磨成粉状,加入PBS缓冲液浸提,浸提液冻干后制得驱蚊提取液;
B、将抗菌液和驱蚊提取液均匀喷洒在织物上,并进行烘干得到预处理织物;
C、将预处理织物放入果胶酶溶液中进行处理后,然后浸渍在驱蚊提取液中处理,取出后烘干,得到驱蚊抗菌织物。
实施例五:
在实施例四中,再加上下述工序:
在步骤C中驱蚊提取液的容量控制在100ml-260ml,而浸渍后利用烘干机烘干时间控制在1.5h-2h。
一种驱蚊抗菌织物制备方法,其制备方法包括以下步骤:
A、首先将40%的竹纤维与60%的棉纤维混纺制成上述织物,将金银花、黄连、黄芩混合,加入竹炭研磨均匀,随后加入乙醇溶液进行回流混合,浓缩得到抗菌液;并将艾草、香叶天竺葵、猪笼草和薄荷利用研磨机研磨成粉状,加入PBS缓冲液浸提,浸提液冻干后制得驱蚊提取液;
B、将抗菌液和驱蚊提取液均匀喷洒在织物上,并进行烘干得到预处理织物;
C、将预处理织物放入果胶酶溶液中进行处理后,然后浸渍在驱蚊提取液中处理,取出后烘干,得到驱蚊抗菌织物。
尽管已经示出和描述了本发明的实施例,对于本领域的普通技术人员而言,可以理解在不脱离本发明的原理和精神的情况下可以对这些实施例进行多种变化、修改、替换和变型,本发明的范围由所附权利要求及其等同物限定。
Claims (5)
- 一种驱蚊抗菌织物制备方法,其特征在于:其制备方法包括以下步骤:A、首先将40%的竹纤维与60%的棉纤维混纺制成上述织物,将金银花、黄连、黄芩混合,加入竹炭研磨均匀,随后加入乙醇溶液进行回流混合,浓缩得到抗菌液;并将艾草、香叶天竺葵、猪笼草和薄荷利用研磨机研磨成粉状,加入PBS缓冲液浸提,浸提液冻干后制得驱蚊提取液;B、将抗菌液和驱蚊提取液均匀喷洒在织物上,并进行烘干得到预处理织物;C、将预处理织物放入果胶酶溶液中进行处理后,然后浸渍在驱蚊提取液中处理,取出后烘干,得到驱蚊抗菌织物。
- 根据权利要求1所述的一种驱蚊抗菌织物制备方法,其特征在于:所述在步骤A中乙醇溶液的浓度为60-70wt%,加入乙醇溶液回流时间为0.5h-1h。
- 根据权利要求1所述的一种驱蚊抗菌织物制备方法,其特征在于:所述在步骤A中艾草、香叶天竺葵、猪笼草和薄荷在研磨过程中适量添加液氮,收集得到织物处理液。
- 根据权利要求1所述的一种驱蚊抗菌织物制备方法,其特征在于:所述在步骤C中放入果胶酶溶液中进行处理再进行等离子处理,气体采用氮气,处理功率为80~280W,压强为50~60Pa,处理时间为20~30min。
- 根据权利要求1所述的一种驱蚊抗菌织物制备方法,其特征在于:所述在步骤C中驱蚊提取液的容量控制在100ml-260ml,而浸渍后利用烘干机烘干时间控制在1.5h-2h。
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