WO2021135417A1 - Filtering distillation apparatus for fine chemical organic synthesis - Google Patents

Filtering distillation apparatus for fine chemical organic synthesis Download PDF

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Publication number
WO2021135417A1
WO2021135417A1 PCT/CN2020/116557 CN2020116557W WO2021135417A1 WO 2021135417 A1 WO2021135417 A1 WO 2021135417A1 CN 2020116557 W CN2020116557 W CN 2020116557W WO 2021135417 A1 WO2021135417 A1 WO 2021135417A1
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Prior art keywords
filter
organic synthesis
fine chemical
respectively arranged
piston
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PCT/CN2020/116557
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French (fr)
Chinese (zh)
Inventor
刘雪静
韩迎
闫鹏
韩猛
曹晗
别福生
石义军
Original Assignee
枣庄学院
艾思特（苏州）医药有限公司
山东省鲁南煤化工工程技术研究院
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Publication of WO2021135417A1 publication Critical patent/WO2021135417A1/en

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/085—Funnel filters; Holders therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/50—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition
    • B01D29/56—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition in series connection
    • B01D29/58—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition in series connection arranged concentrically or coaxially

Definitions

  • the invention relates to the technical field of filtration distillation equipment, in particular to a filtration distillation equipment for fine chemical organic synthesis.
  • fine chemical industry is a general term for the fine chemical industry, referred to as "fine chemical industry".
  • fine chemical industry The meaning of fine chemicals is still under discussion abroad. All chemical products with the following characteristics are generally called fine chemicals, namely: a wide variety of products, fast replacement; small output, mostly produced in batches; functional or end-use; many of them are compound products, formulas and other technical decisions Product performance; high product quality requirements; strong commercial properties, most of which are sold under brand names; high technology intensive, requiring continuous technological development of new products and research on application technologies, focusing on technical services; small equipment investment; high added value rate.
  • Fine chemicals can be divided into fine organic chemical products, fine inorganic chemical products, fine biological chemical products and fine polymer chemical products.
  • Organic synthesis refers to the use of easily available raw materials to produce organic compounds with specific structures and functions through organic reactions.
  • Sucrose fatty acid ester is a kind of non-ionic surfactant, which is a simple substance or mixture formed by esterification reaction of sucrose and fatty acid. Its appearance is white to yellow powder, colorless to slightly yellow viscous liquid or soft solid. Because sucrose contains 8 -OH groups, various products from monoester to octaester can be produced after esterification.
  • the -OH group of sucrose is the hydrophilic group, and the carbon chain part of the fatty acid is the lipophilic group.
  • Higher fatty acids such as stearic acid, oleic acid and palmitic acid are commonly used (the product is in powder form), and lower grades such as acetic acid and isobutyric acid are also used. Fatty acid (the product is a viscous resin).
  • Sucrose fatty acid esters are mainly used in emulsifiers, preservatives, meat products, emulsified flavors, etc.
  • the purpose of the present invention is to solve the above-mentioned problems by designing a filtering distillation equipment for fine chemical organic synthesis, which solves the problem that the existing filtering and distillation devices are split, and the filtering and distillation tools are relatively scattered, which is not convenient for collection and storage. , Making the work surface more messy and easy to lose, when filtering and distilling sucrose fatty acid ester, it is not convenient for the staff to use, and the work efficiency is low.
  • a filter distillation equipment for fine chemical organic synthesis including a base, the base is provided with a first groove and a second groove, the base is installed with a filter structure and distillation structure;
  • the filtering structure includes: two support plates, a moving part, a first filter, a first funnel, a second filter, a second funnel, and a controller;
  • the two supporting plates are respectively arranged on the front and rear ends of the base, the two moving parts are respectively arranged on the two supporting plates, and the two ends of the first filter screen are respectively arranged on the two moving parts ,
  • the first funnel is arranged at the lower end of the first filter, the two ends of the second filter are respectively arranged on the moving part, the second funnel is arranged at the lower end of the second frame, and the controller is arranged on the base on.
  • the distillation structure includes: a container, a resistance wire, an air strut, a pneumatic gripper, and a diversion part;
  • the container is arranged at the first groove on the base, the resistance wire is arranged inside the container, the gas strut is arranged on one of the two supports, and the pneumatic clamping jaw is arranged on the On the telescopic end of the gas strut, the guide portion is movably arranged on the driving end of the pneumatic clamping jaw.
  • the moving part includes: two sliding rails, two bearing plates and four sliding plates;
  • the two sliding rails are respectively arranged on two brackets, the two bearing plates are respectively arranged on the two sliding rails, and the four sliding plates are respectively arranged on the two bearing plates.
  • the guide portion includes: a tank body, a first piston, a second piston, a condenser tube, a horn tube, and a bottle body;
  • the tank body is arranged on the driving end of the pneumatic clamping jaws, the first piston is screwed to the mouth of the upper end of the tank body by threads, the second piston is arranged on the tank body, and one end of the condenser tube is At the second piston, the horn tube is movably arranged at the other end of the condenser tube through the third piston, the lower end of the condenser tube is equipped with a support assembly, and the bottle body is movably arranged at the second groove on the base.
  • the supporting assembly includes: two supporting rods with the same structure and a fixing plate;
  • the two supporting rods are respectively arranged on the fixing seat, and the fixing plate is respectively arranged on the two supporting rods.
  • a shock-absorbing pad is attached to the driving end of the pneumatic clamping jaw.
  • the diameter of the can mouth at the upper end of the can body is larger than the diameter of the can body.
  • a branch pipe is installed on the tank body, the second piston is movably arranged on the branch pipe, and a first non-slip rubber pad is attached between the bottle body and the support seat.
  • a water outlet pipe is installed on the left side of the container, and a valve is installed on the water outlet pipe.
  • an arc-shaped groove is formed on the fixing plate, and a second anti-slip rubber pad is installed on the arc-shaped groove.
  • a filter distillation equipment for fine chemical organic synthesis made by the technical solution of the present invention has a simple structure and is easy to operate.
  • the filter structure and the distillation structure are integrated, which facilitates the collection and storage of the staff, and effectively solves the loss of parts It is easy to organize the work surface, easy to operate, easy to use by the staff, and improve the work efficiency of the staff.
  • Fig. 1 is a schematic diagram of the front sectional view of the filter distillation equipment for fine chemical organic synthesis according to the present invention.
  • Fig. 2 is a schematic side view of the sectional structure of the filtering distillation equipment for fine chemical organic synthesis according to the present invention.
  • Fig. 3 is a schematic top view of the structure of a filter distillation device for fine chemical organic synthesis according to the present invention.
  • FIG. 4 is a schematic diagram of the front sectional view of the arc groove and the second non-slip rubber pad of the filtering distillation equipment for fine chemical organic synthesis according to the present invention.
  • Fig. 5 is a schematic side view of the fixed plate of the filter distillation equipment for fine chemical organic synthesis according to the present invention.
  • a filter distillation equipment for fine chemical organic synthesis includes a base 1 on which a first groove and a second groove are opened.
  • the base 1 is equipped with a filter structure and a distillation structure;
  • the filter structure includes: two support plates 2, a moving part, a first filter 4, a first funnel 5, a second filter 6, and a second funnel 7 and the controller 17;
  • the two supporting plates 2 are respectively arranged on the front and rear ends of the base 1, the two moving parts are respectively arranged on the two supporting plates 2, and the first filter 4
  • the two ends are respectively arranged on the two moving parts, the first funnel 5 is arranged at the lower end of the first filter screen 4, the two ends of the second filter screen 6 are respectively arranged on the moving parts, the second funnel 7
  • the controller 17 is installed on the base 1 and is arranged at the lower end of the second frame.
  • the distillation structure includes: a container 8, a resistance wire 9, a gas strut 10, a pneumatic clamping jaw 11, and a diversion part; the container 8 is arranged at the first groove on the base 1, and the resistance wire 9 is arranged Inside the container 8, the gas strut 10 is placed on one of the two brackets, the pneumatic gripper 11 is placed on the telescopic end of the gas strut 10, and the guide part is movable
  • the moving part is arranged on the driving end of the pneumatic gripper 11, and the moving part includes: two sliding rails 12, two bearing plates 13 and four sliding plates 14; the two sliding rails 12 are respectively arranged on two supports, two The two bearing plates 13 are respectively arranged on the two sliding rails 12, and the four sliding plates 14 are respectively arranged on the two bearing plates 13.
  • the guide portion includes a tank body 15, a first piston 16, a second piston 22, a condenser tube 18, a horn tube 19, and a bottle body 21.
  • the tank body 15 is arranged on the driving end of the pneumatic gripper 11,
  • the first piston 16 is screwed to the mouth of the upper end of the tank body 15 through threads
  • the second piston 22 is arranged on the tank body 15, one end of the condenser tube 18 is located at the second piston 22, and the horn tube 19 is movably arranged at the other end of the condenser tube 18 through the third piston 23, the lower end of the condenser tube 18 is installed with a supporting assembly
  • the bottle body 21 is movably arranged in the second groove on the base 1.
  • the support assembly includes: two support rods 25 with the same structure and a fixing plate 26; the two support rods 25 are respectively arranged on a fixing seat, and the fixing plate 26 is respectively arranged on the two support rods 25
  • a shock-absorbing pad 27 is attached to the driving end of the pneumatic gripper 11, the diameter of the mouth at the upper end of the tank body 15 is larger than the diameter of the tank body, a branch pipe 24 is installed on the tank body 15, and the first
  • the two pistons 22 are movably arranged on the branch pipe 24, the first non-slip rubber pad 3 is attached between the bottle body 21 and the supporting seat, the water outlet pipe 28 is installed on the left side of the container 8, and the water outlet pipe 28 is installed There is a valve 29, an arc-shaped groove is opened on the fixed plate 26, and a second non-slip rubber pad 20 is installed on the arc-shaped groove.
  • the feature of this embodiment is that it includes a base 1, on which a first groove and a second groove are opened, and a filter structure and a distillation structure are installed on the base 1;
  • the filtering structure includes: two supporting plates 2, a moving part, a first filter screen 4, a first funnel 5, a second filter screen 6, a second funnel 7 and a controller 17;
  • the two supporting plates 2 are respectively arranged on the front and rear ends of the base 1, the two moving parts are respectively arranged on the two supporting plates 2, the two ends of the first filter screen 4 are respectively arranged on the two moving parts, the first funnel 5 It is arranged at the lower end of the first filter screen 4, the two ends of the second filter screen 6 are respectively arranged on the moving part, the second funnel 7 is arranged on the lower end of the second frame, and the controller 17 is arranged on the base 1.
  • the structure is simple and easy to operate.
  • the filter structure and the distillation structure are integrated, which is convenient for the staff to collect and store, effectively solve the loss of parts, and is convenient for the arrangement of the work table, convenient for operation, convenient for the use of the staff, and improved staff. Work efficiency.
  • connection and control sequence should refer to the following work
  • the electrical connection is completed in the order of the electrical components.
  • the detailed connection method is a well-known technology in the art. The following mainly introduces the working principle and process, and does not explain the electrical control.
  • Embodiment A filtering distillation equipment for fine chemical organic synthesis, comprising a base 1, a first groove and a second groove are opened on the base 1, and a filtering structure and a distillation structure are installed on the base 1;
  • the filter structure includes: two support plates 2, a moving part, a first filter 4, a first funnel 5, a second filter 6, and a second funnel 7 And the controller 17; the connection relationship is as follows:
  • the two supporting plates 2 are respectively arranged on the front and rear ends of the base 1, the two moving parts are respectively arranged on the two supporting plates 2, the two ends of the first filter screen 4 are respectively arranged on the two moving parts, the first funnel 5 It is arranged at the lower end of the first filter screen 4, the two ends of the second filter screen 6 are respectively arranged on the moving part, the second funnel 7 is arranged at the lower end of the second frame, and the controller 17 is arranged on the base 1.
  • the distillation structure preferably adopts the following structure, including: a container 8, a resistance wire 9, a gas strut 10, a pneumatic gripper 11, and a diversion part; the connection relationship is as follows:
  • the container 8 is placed at the first groove on the base 1, the resistance wire 9 is placed inside the container 8, the gas strut 10 is placed on one of the two brackets, and the pneumatic gripper 11 is placed on the air strut 10 On the telescopic end, the guide part is movably arranged on the driving end of the pneumatic clamping jaw 11.
  • the moving part includes: two sliding rails 12, two load-bearing plates 13, and four sliding plates 14; the connection relationship is as follows:
  • Two sliding rails 12 are respectively arranged on two brackets, two bearing plates 13 are respectively arranged on two sliding rails 12, and four sliding plates 14 are respectively arranged on two bearing plates 13.
  • the diversion part includes: a tank body 15, a first piston 16, a second piston 22, a condenser tube 18, a horn tube 19, and a bottle body 21.
  • the connection relationship is as follows:
  • the tank body 15 is arranged on the driving end of the pneumatic clamping jaw 11, the first piston 16 is screwed to the mouth of the upper end of the tank body 15, the second piston 22 is arranged on the tank body 15, and one end of the condenser tube 18 is second At the piston 22, the horn tube 19 is movably arranged at the other end of the condenser tube 18 through the third piston 23, the lower end of the condenser tube 18 is equipped with a supporting assembly, and the bottle body 21 is movably arranged at the second groove on the base 1.
  • the support assembly includes: two support rods 25 and a fixing plate 26 with the same structure; the connection relationship is as follows:
  • the two supporting rods 25 are respectively arranged on the fixing seat, and the fixing plate 26 is respectively arranged on the two supporting rods 25.
  • a shock-absorbing pad 27 is attached to the driving end of the pneumatic gripper 11, the diameter of the can mouth at the upper end of the can body 15 is larger than the diameter of the can body, and the diameter of the can mouth is larger than the body diameter to prevent the can body 15 from facing
  • the damping pad 27 is used for when the tank body 15 is boiling due to the solution in the container 8, and the tank body 15 is fluctuated.
  • the staff puts the first filter 4 and The second filter screen 6 moves upward through the slide rail 12, and after moving to the top of the slide rail 12,
  • the resistance wire 9 began to heat and heat the liquid to boiling. Since the bottom of the tank 15 is placed in the middle of the container 8, when the container 8 is When the liquid is boiling, the filtrate will boil with it, and then it will be distilled.
  • a branch pipe 24 is installed on the tank body 15, and the distilled solution flows into the condenser pipe 18 through the direct-flow pipe. At this time, the condenser pipe 18 is connected to the tap water pipe.
  • the distilled solution passes through the condensation process, The distilled solution is cooled, and the cooled distilled solution flows into the bottle body 21 through the horn tube 19, and the support and fixing plate 26 effectively support the condenser tube 18 to obtain the sucrose fatty acid ester product.
  • the equipment will be cleaned, the tap water pipe will be closed, and the tap water pipe will be disconnected from the condenser tube 18. Then the first filter 4 and the second filter 6 will be disassembled through the slide plate 14, and then the staff will hold the tank with their hands 15,
  • a branch pipe 24 is installed on the tank body 15, the second piston 22 is movably arranged on the branch pipe 24, the second piston 22 is moved toward the tank body 15, and then the condenser tube 18 is fixed along The plate 26 moves to the right, and then the condenser tube 18 is removed from the second piston 22, and then the pneumatic clamping jaw 11 is opened, and then the second gas strut 10 is used to remove the tank 15 from the pneumatic clamping jaw 11 , Clean the tank 15 and the condenser tube 18,
  • a water outlet pipe 28 is installed on the left side of the container 8, and a valve 29 is installed on the water outlet pipe 28.
  • the staff opens the valve 29, and then flows out the water outlet pipe 28 in the container 8, and sets the first piston 16 is removed through the thread, the tank 15 is cleaned, and then the staff lifts the condenser tube 18, and takes the sucrose fatty acid ester product of the bottle 21 to the designated place.
  • the fixing plate 26 is provided with an arc-shaped groove, and the second non-slip rubber pad 20 is installed on the arc-shaped groove, and then the condenser tube 18 is picked up and removed from the third piston 23, and then The condenser tube 18 and the horn tube 19 are cleaned, and the controller 17 adopts a programmable controller 17, which can control the resistance wire 9 and control the heating time of the resistance wire 9.
  • a shock-absorbing pad 27 is attached to the driving end of the pneumatic clamping jaw 11.
  • the diameter of the opening at the upper end of the can body 15 is larger than the diameter of the can body.
  • a branch pipe 24 is installed on the tank body 15, the second piston 22 is movably arranged on the branch pipe 24, and a first anti-slip rubber pad 3 is attached between the bottle body 21 and the support seat.
  • a water outlet pipe 28 is installed on the left side of the container 8, and a valve 29 is installed on the water outlet pipe 28.
  • the fixing plate 26 is provided with an arc-shaped groove, and the second non-slip rubber pad 20 is installed on the arc-shaped groove.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

A filtering distillation apparatus for fine chemical organic synthesis, the apparatus comprises a base (1), wherein the base (1) is provided with a first groove and a second groove, a filtering structure and a distillation structure are mounted on the base (1), the filtering structure comprises two supporting plates (2), two moving parts, a first filter screen (4), a first funnel (5), a second filter screen (6), a second funnel (7) and a controller (17), the two supporting plates (2) are arranged at the front and rear ends of the base (1) respectively, the two moving parts are arranged on the two supporting plates (2) respectively, two ends of the first filter screen (4) are arranged on the two moving parts respectively, the first funnel (5) is arranged at the lower end of the first filter screen (4), two ends of the second filter screen (6) are arranged on the moving parts respectively, the second funnel (7) is arranged at the lower end of the second filter screen (6), and the controller (17) is arranged on the base (1).

Description

一种精细化工有机合成用过滤蒸馏设备Filtering distillation equipment for fine chemical organic synthesis 技术领域Technical field
本发明涉及过滤蒸馏设备技术领域，特别是一种精细化工有机合成用过滤蒸馏设备。The invention relates to the technical field of filtration distillation equipment, in particular to a filtration distillation equipment for fine chemical organic synthesis.
背景技术Background technique
精细化学工业是生产精细化学品工业的通称，简称“精细化工”。精细化学品的含义，国外仍在讨论中。凡具有以下特点的化工产品通称为精细化学品，即：品种多，更新换代快；产量小，大多以间歇方式生产；具有功能性或最终使用性；许多为复配性产品，配方等技术决定产品性能；产品质量要求高；商品性强，多数以商品名销售；技术密集高，要求不断进行新产品的技术开发和应用技术的研究，重视技术服务；设备投资较小；附加价值率高等。精细化工可分为精细有机化工产品、精细无机化工产品、精细生物化工产品和精细高分子化工产品。The fine chemical industry is a general term for the fine chemical industry, referred to as "fine chemical industry". The meaning of fine chemicals is still under discussion abroad. All chemical products with the following characteristics are generally called fine chemicals, namely: a wide variety of products, fast replacement; small output, mostly produced in batches; functional or end-use; many of them are compound products, formulas and other technical decisions Product performance; high product quality requirements; strong commercial properties, most of which are sold under brand names; high technology intensive, requiring continuous technological development of new products and research on application technologies, focusing on technical services; small equipment investment; high added value rate. Fine chemicals can be divided into fine organic chemical products, fine inorganic chemical products, fine biological chemical products and fine polymer chemical products.
有机合成，是指利用简单易得的原料，通过有机反应，生成具有特定结构和功能的有机化合物。Organic synthesis refers to the use of easily available raw materials to produce organic compounds with specific structures and functions through organic reactions.
蔗糖脂肪酸酯是一种非离子表面活性剂，由蔗糖和脂肪酸经酯化反应生成的单质或混合物。其外观为白色至黄色的粉末、无色至微黄色的粘稠液体或软固体。因蔗糖含有8个—OH基，因此经酯化，从单酯到八酯的各种产物均可生成。以蔗糖的—OH基为亲水基，脂肪酸的碳链部分为亲油基，常用硬脂酸、油酸、棕榈酸等高级脂肪酸(产品为粉末状)，也用醋酸、异丁酸等低级脂肪酸(产品为粘稠树脂状)。蔗糖脂肪酸酯主要用于乳化剂、保鲜剂，肉制品、乳化香精等。Sucrose fatty acid ester is a kind of non-ionic surfactant, which is a simple substance or mixture formed by esterification reaction of sucrose and fatty acid. Its appearance is white to yellow powder, colorless to slightly yellow viscous liquid or soft solid. Because sucrose contains 8 -OH groups, various products from monoester to octaester can be produced after esterification. The -OH group of sucrose is the hydrophilic group, and the carbon chain part of the fatty acid is the lipophilic group. Higher fatty acids such as stearic acid, oleic acid and palmitic acid are commonly used (the product is in powder form), and lower grades such as acetic acid and isobutyric acid are also used. Fatty acid (the product is a viscous resin). Sucrose fatty acid esters are mainly used in emulsifiers, preservatives, meat products, emulsified flavors, etc.
然而在对蔗糖脂肪酸酯进行提纯的过程中，需要对蔗糖脂肪酸酯母液进行过滤以及蒸馏，然而现有的过滤以及蒸馏装置均为分体式，过滤以及蒸馏的工具较为零散，不便于收集以及收纳，使得工作台台面较为杂乱，且易丢失，当对蔗糖脂肪酸酯进行过滤以及蒸馏时，不便于工作人员的使用，且工作效率较低，鉴于此，针对上述问题深入研究，遂有本发明产生。However, in the process of purifying sucrose fatty acid esters, the mother liquor of sucrose fatty acid esters needs to be filtered and distilled. However, the existing filtration and distillation devices are all split types, and the tools for filtration and distillation are relatively fragmented and inconvenient to collect and distill. Storage makes the workbench surface more messy and easy to lose. When filtering and distilling sucrose fatty acid esters, it is inconvenient for the staff to use, and the work efficiency is low. In view of this, in-depth research on the above problems has provided the foundation Invention produced.
发明内容Summary of the invention
本发明的目的是为了解决上述问题，设计了一种精细化工有机合成用过滤蒸馏设备，解决了现有的过滤以及蒸馏装置均为分体式，过滤以及蒸馏的工具较为零散，不便于收集以及收纳，使得工作台台面较为杂乱，且易丢失，当对蔗糖脂肪酸酯进行过滤以及蒸馏时，不便于工作人员的使用，且工作效率较低的问题。The purpose of the present invention is to solve the above-mentioned problems by designing a filtering distillation equipment for fine chemical organic synthesis, which solves the problem that the existing filtering and distillation devices are split, and the filtering and distillation tools are relatively scattered, which is not convenient for collection and storage. , Making the work surface more messy and easy to lose, when filtering and distilling sucrose fatty acid ester, it is not convenient for the staff to use, and the work efficiency is low.
实现上述目的本发明的技术方案为：一种精细化工有机合成用过滤蒸馏设备，包括底座，所述底座上开设有第一凹槽以及第二凹槽，所述底座上安装有过滤结构以及蒸馏结构；The technical solution of the present invention to achieve the above objective is: a filter distillation equipment for fine chemical organic synthesis, including a base, the base is provided with a first groove and a second groove, the base is installed with a filter structure and distillation structure;
所述过滤结构，包括：两个支板、移动部、第一过滤网、第一漏斗、第二过滤网、第二漏斗以及控制器；The filtering structure includes: two support plates, a moving part, a first filter, a first funnel, a second filter, a second funnel, and a controller;
两个所述支板分别安置于底座的前后两端，两个所述移动部分别安置于两个所述支板上，所述第一过滤网的两端分别安置于两个所述移动部上，所述第一漏斗安置于第一过滤网下端，所述第二过滤网的两端分别安置于移动部上，所述第二漏斗安置于第二框架下端，所述控制器安置于底座上。The two supporting plates are respectively arranged on the front and rear ends of the base, the two moving parts are respectively arranged on the two supporting plates, and the two ends of the first filter screen are respectively arranged on the two moving parts , The first funnel is arranged at the lower end of the first filter, the two ends of the second filter are respectively arranged on the moving part, the second funnel is arranged at the lower end of the second frame, and the controller is arranged on the base on.
优选的，所述蒸馏结构，包括：容器、电阻丝、气撑杆、气动夹爪以及导流部；Preferably, the distillation structure includes: a container, a resistance wire, an air strut, a pneumatic gripper, and a diversion part;
所述容器安置于底座上的第一凹槽处，所述电阻丝安置于容器的内部，所述气撑杆安置于两个所述支架的其中一个支架上，所述气动夹爪安置于所述气撑杆的伸缩端上，所述导流部活动安置于气动夹爪的驱动端上。The container is arranged at the first groove on the base, the resistance wire is arranged inside the container, the gas strut is arranged on one of the two supports, and the pneumatic clamping jaw is arranged on the On the telescopic end of the gas strut, the guide portion is movably arranged on the driving end of the pneumatic clamping jaw.
优选的，所述移动部包括：两个滑轨、两个承载板以及四个滑板；Preferably, the moving part includes: two sliding rails, two bearing plates and four sliding plates;
两个所述滑轨分别安置于两个支架上，两个所述承载板分别安置于两个所述滑轨上，四个所述滑板分别安置于两个所述承载板上。The two sliding rails are respectively arranged on two brackets, the two bearing plates are respectively arranged on the two sliding rails, and the four sliding plates are respectively arranged on the two bearing plates.
优选的，所述导流部，包括：罐体、第一活塞、第二活塞、冷凝管、牛角管以及瓶体；Preferably, the guide portion includes: a tank body, a first piston, a second piston, a condenser tube, a horn tube, and a bottle body;
所述罐体安置于气动夹爪的驱动端上，所述第一活塞通过螺纹旋接于 罐体上端的罐口处，所述第二活塞安置于罐体上，所述冷凝管的一端第二活塞处，所述牛角管通过第三活塞活动安置于冷凝管的另一端，所述冷凝管的下端安装有支撑组件，所述瓶体活动安置于底座上的第二凹槽处。The tank body is arranged on the driving end of the pneumatic clamping jaws, the first piston is screwed to the mouth of the upper end of the tank body by threads, the second piston is arranged on the tank body, and one end of the condenser tube is At the second piston, the horn tube is movably arranged at the other end of the condenser tube through the third piston, the lower end of the condenser tube is equipped with a support assembly, and the bottle body is movably arranged at the second groove on the base.
优选的，所述支撑组件，包括：两个结构相同的支撑杆以及固定板；Preferably, the supporting assembly includes: two supporting rods with the same structure and a fixing plate;
两个所述支撑杆分别安置于固定座上，所述固定板分别安置于两个所述支撑杆上。The two supporting rods are respectively arranged on the fixing seat, and the fixing plate is respectively arranged on the two supporting rods.
优选的，所述气动夹爪的驱动端上贴合有减震垫。Preferably, a shock-absorbing pad is attached to the driving end of the pneumatic clamping jaw.
优选的，所述罐体上端的罐口处直径大于罐身直径。Preferably, the diameter of the can mouth at the upper end of the can body is larger than the diameter of the can body.
优选的，所述罐体上安装有支流管，所述第二活塞活动安置于支流管上，所述瓶体与支撑座之间贴合有第一防滑胶垫。Preferably, a branch pipe is installed on the tank body, the second piston is movably arranged on the branch pipe, and a first non-slip rubber pad is attached between the bottle body and the support seat.
优选的，所述容器左侧安装有出水管，所述出水管上安装有阀门。Preferably, a water outlet pipe is installed on the left side of the container, and a valve is installed on the water outlet pipe.
优选的，所述固定板上开设有弧形槽，所述弧形槽上安装有第二防滑胶垫。Preferably, an arc-shaped groove is formed on the fixing plate, and a second anti-slip rubber pad is installed on the arc-shaped groove.
利用本发明的技术方案制作的一种精细化工有机合成用过滤蒸馏设备，结构简单，便于操作，将过滤结构以及蒸馏结构设为一体式，便于工作人员的收集以及收纳，有效的解决了零件丢失的情况，以及便于工作台台面的整理，便于操作，便于工作人员的使用，提高了工作人员的工作效率。A filter distillation equipment for fine chemical organic synthesis made by the technical solution of the present invention has a simple structure and is easy to operate. The filter structure and the distillation structure are integrated, which facilitates the collection and storage of the staff, and effectively solves the loss of parts It is easy to organize the work surface, easy to operate, easy to use by the staff, and improve the work efficiency of the staff.
附图说明Description of the drawings
图1为本发明所述一种精细化工有机合成用过滤蒸馏设备的主视剖视结构示意图。Fig. 1 is a schematic diagram of the front sectional view of the filter distillation equipment for fine chemical organic synthesis according to the present invention.
图2为本发明所述一种精细化工有机合成用过滤蒸馏设备的侧视剖视结构示意图。Fig. 2 is a schematic side view of the sectional structure of the filtering distillation equipment for fine chemical organic synthesis according to the present invention.
图3为本发明所述一种精细化工有机合成用过滤蒸馏设备的俯视结构示意图。Fig. 3 is a schematic top view of the structure of a filter distillation device for fine chemical organic synthesis according to the present invention.
图4为本发明所述一种精细化工有机合成用过滤蒸馏设备的弧形槽以及第二防滑胶垫主视剖视结构示意图。4 is a schematic diagram of the front sectional view of the arc groove and the second non-slip rubber pad of the filtering distillation equipment for fine chemical organic synthesis according to the present invention.
图5为本发明所述一种精细化工有机合成用过滤蒸馏设备的固定板的侧视结构示意图。Fig. 5 is a schematic side view of the fixed plate of the filter distillation equipment for fine chemical organic synthesis according to the present invention.
图中：1、底座；2、支板；3、第一防滑胶垫；4、第一过滤网；5、第一漏斗；6第二过滤网；7、第二漏斗；8、容器；9、电阻丝；10、气撑杆；11、气动夹爪；12、滑轨；13、承载板；14、滑板；15、罐体；16、第一活塞；17、控制器；18、冷凝管；19、牛角管；20、第二防滑胶垫；21、瓶体；22、第二活塞；23、第三活塞；24、支流管；25、支撑杆；26、固定板；27、减震垫；28、出水管；29、阀门。In the figure: 1. Base; 2. Support plate; 3. First non-slip rubber pad; 4. First filter; 5. First funnel; 6 Second filter; 7. Second funnel; 8. Container; 9. , Resistance wire; 10, gas strut; 11, pneumatic gripper; 12, slide rail; 13, bearing plate; 14, slide plate; 15, tank body; 16, first piston; 17, controller; 18, condenser tube 19, horn tube; 20, second non-slip rubber pad; 21, bottle body; 22, second piston; 23, third piston; 24, branch pipe; 25, support rod; 26, fixed plate; 27, shock absorption Mat; 28, outlet pipe; 29, valve.
具体实施方式Detailed ways
下面结合附图对本发明进行具体描述，如图1-图5所示，一种精细化工有机合成用过滤蒸馏设备，包括底座1，所述底座1上开设有第一凹槽以及第二凹槽，所述底座1上安装有过滤结构以及蒸馏结构；所述过滤结构，包括：两个支板2、移动部、第一过滤网4、第一漏斗5、第二过滤网6、第二漏斗7以及控制器17；两个所述支板2分别安置于底座1的前后两端，两个所述移动部分别安置于两个所述支板2上，所述第一过滤网4的两端分别安置于两个所述移动部上，所述第一漏斗5安置于第一过滤网4下端，所述第二过滤网6的两端分别安置于移动部上，所述第二漏斗7安置于第二框架下端，所述控制器17安置于底座1上。The present invention will be described in detail below with reference to the accompanying drawings. As shown in Figures 1 to 5, a filter distillation equipment for fine chemical organic synthesis includes a base 1 on which a first groove and a second groove are opened. , The base 1 is equipped with a filter structure and a distillation structure; the filter structure includes: two support plates 2, a moving part, a first filter 4, a first funnel 5, a second filter 6, and a second funnel 7 and the controller 17; the two supporting plates 2 are respectively arranged on the front and rear ends of the base 1, the two moving parts are respectively arranged on the two supporting plates 2, and the first filter 4 The two ends are respectively arranged on the two moving parts, the first funnel 5 is arranged at the lower end of the first filter screen 4, the two ends of the second filter screen 6 are respectively arranged on the moving parts, the second funnel 7 The controller 17 is installed on the base 1 and is arranged at the lower end of the second frame.
所述蒸馏结构，包括：容器8、电阻丝9、气撑杆10、气动夹爪11以及导流部；所述容器8安置于底座1上的第一凹槽处，所述电阻丝9安置于容器8的内部，所述气撑杆10安置于两个所述支架的其中一个支架上，所述气动夹爪11安置于所述气撑杆10的伸缩端上，所述导流部活动安置于气动夹爪11的驱动端上，所述移动部包括：两个滑轨12、两个承载板13以及四个滑板14；两个所述滑轨12分别安置于两个支架上，两个所述承载板13分别安置于两个所述滑轨12上，四个所述滑板14分别安置于两个所述承载板13上。The distillation structure includes: a container 8, a resistance wire 9, a gas strut 10, a pneumatic clamping jaw 11, and a diversion part; the container 8 is arranged at the first groove on the base 1, and the resistance wire 9 is arranged Inside the container 8, the gas strut 10 is placed on one of the two brackets, the pneumatic gripper 11 is placed on the telescopic end of the gas strut 10, and the guide part is movable The moving part is arranged on the driving end of the pneumatic gripper 11, and the moving part includes: two sliding rails 12, two bearing plates 13 and four sliding plates 14; the two sliding rails 12 are respectively arranged on two supports, two The two bearing plates 13 are respectively arranged on the two sliding rails 12, and the four sliding plates 14 are respectively arranged on the two bearing plates 13.
所述导流部，包括：罐体15、第一活塞16、第二活塞22、冷凝管18、 牛角管19以及瓶体21，所述罐体15安置于气动夹爪11的驱动端上，所述第一活塞16通过螺纹旋接于罐体15上端的罐口处，所述第二活塞22安置于罐体15上，所述冷凝管18的一端第二活塞22处，所述牛角管19通过第三活塞23活动安置于冷凝管18的另一端，所述冷凝管18的下端安装有支撑组件，所述瓶体21活动安置于底座1上的第二凹槽处。The guide portion includes a tank body 15, a first piston 16, a second piston 22, a condenser tube 18, a horn tube 19, and a bottle body 21. The tank body 15 is arranged on the driving end of the pneumatic gripper 11, The first piston 16 is screwed to the mouth of the upper end of the tank body 15 through threads, the second piston 22 is arranged on the tank body 15, one end of the condenser tube 18 is located at the second piston 22, and the horn tube 19 is movably arranged at the other end of the condenser tube 18 through the third piston 23, the lower end of the condenser tube 18 is installed with a supporting assembly, and the bottle body 21 is movably arranged in the second groove on the base 1.
所述支撑组件，包括：两个结构相同的支撑杆25以及固定板26；两个所述支撑杆25分别安置于固定座上，所述固定板26分别安置于两个所述支撑杆25上，所述气动夹爪11的驱动端上贴合有减震垫27，所述罐体15上端的罐口处直径大于罐身直径，所述罐体15上安装有支流管24，所述第二活塞22活动安置于支流管24上，所述瓶体21与支撑座之间贴合有第一防滑胶垫3，所述容器8左侧安装有出水管28，所述出水管28上安装有阀门29，所述固定板26上开设有弧形槽，所述弧形槽上安装有第二防滑胶垫20。The support assembly includes: two support rods 25 with the same structure and a fixing plate 26; the two support rods 25 are respectively arranged on a fixing seat, and the fixing plate 26 is respectively arranged on the two support rods 25 A shock-absorbing pad 27 is attached to the driving end of the pneumatic gripper 11, the diameter of the mouth at the upper end of the tank body 15 is larger than the diameter of the tank body, a branch pipe 24 is installed on the tank body 15, and the first The two pistons 22 are movably arranged on the branch pipe 24, the first non-slip rubber pad 3 is attached between the bottle body 21 and the supporting seat, the water outlet pipe 28 is installed on the left side of the container 8, and the water outlet pipe 28 is installed There is a valve 29, an arc-shaped groove is opened on the fixed plate 26, and a second non-slip rubber pad 20 is installed on the arc-shaped groove.
本实施方案的特点为，包括底座1，底座1上开设有第一凹槽以及第二凹槽，底座1上安装有过滤结构以及蒸馏结构；The feature of this embodiment is that it includes a base 1, on which a first groove and a second groove are opened, and a filter structure and a distillation structure are installed on the base 1;
过滤结构，包括：两个支板2、移动部、第一过滤网4、第一漏斗5、第二过滤网6、第二漏斗7以及控制器17；The filtering structure includes: two supporting plates 2, a moving part, a first filter screen 4, a first funnel 5, a second filter screen 6, a second funnel 7 and a controller 17;
两个支板2分别安置于底座1的前后两端，两个移动部分别安置于两个支板2上，第一过滤网4的两端分别安置于两个移动部上，第一漏斗5安置于第一过滤网4下端，第二过滤网6的两端分别安置于移动部上，第二漏斗7安置于第二框架下端，控制器17安置于底座1上，结构简单，便于操作，将过滤结构以及蒸馏结构设为一体式，便于工作人员的收集以及收纳，有效的解决了零件丢失的情况，以及便于工作台台面的整理，便于操作，便于工作人员的使用，提高了工作人员的工作效率。The two supporting plates 2 are respectively arranged on the front and rear ends of the base 1, the two moving parts are respectively arranged on the two supporting plates 2, the two ends of the first filter screen 4 are respectively arranged on the two moving parts, the first funnel 5 It is arranged at the lower end of the first filter screen 4, the two ends of the second filter screen 6 are respectively arranged on the moving part, the second funnel 7 is arranged on the lower end of the second frame, and the controller 17 is arranged on the base 1. The structure is simple and easy to operate. The filter structure and the distillation structure are integrated, which is convenient for the staff to collect and store, effectively solve the loss of parts, and is convenient for the arrangement of the work table, convenient for operation, convenient for the use of the staff, and improved staff. Work efficiency.
通过本领域人员，将本发明中所有电气件与其适配的电源通过导线进行连接，并且应该根据实际情况，选择合适的控制器，以满足控制需求，具体连接以及控制顺序，应参考下述工作原理中，各电气件之间先后工作顺序完成电性连接，其详细连接手段，为本领域公知技术，下述主要介绍 工作原理以及过程，不在对电气控制做说明。Those skilled in the art should connect all the electrical components of the present invention and their adapted power supply through wires, and should select a suitable controller according to the actual situation to meet the control requirements. The specific connection and control sequence should refer to the following work In the principle, the electrical connection is completed in the order of the electrical components. The detailed connection method is a well-known technology in the art. The following mainly introduces the working principle and process, and does not explain the electrical control.
实施例：一种精细化工有机合成用过滤蒸馏设备，包括底座1，底座1上开设有第一凹槽以及第二凹槽，底座1上安装有过滤结构以及蒸馏结构；Embodiment: A filtering distillation equipment for fine chemical organic synthesis, comprising a base 1, a first groove and a second groove are opened on the base 1, and a filtering structure and a distillation structure are installed on the base 1;
在具体实施过程中，请参阅附图1-图5，过滤结构，包括：两个支板2、移动部、第一过滤网4、第一漏斗5、第二过滤网6、第二漏斗7以及控制器17；连接关系如下：In the specific implementation process, please refer to Figures 1 to 5, the filter structure includes: two support plates 2, a moving part, a first filter 4, a first funnel 5, a second filter 6, and a second funnel 7 And the controller 17; the connection relationship is as follows:
两个支板2分别安置于底座1的前后两端，两个移动部分别安置于两个支板2上，第一过滤网4的两端分别安置于两个移动部上，第一漏斗5安置于第一过滤网4下端，第二过滤网6的两端分别安置于移动部上，第二漏斗7安置于第二框架下端，控制器17安置于底座1上。The two supporting plates 2 are respectively arranged on the front and rear ends of the base 1, the two moving parts are respectively arranged on the two supporting plates 2, the two ends of the first filter screen 4 are respectively arranged on the two moving parts, the first funnel 5 It is arranged at the lower end of the first filter screen 4, the two ends of the second filter screen 6 are respectively arranged on the moving part, the second funnel 7 is arranged at the lower end of the second frame, and the controller 17 is arranged on the base 1.
在具体实施过程中，蒸馏结构优选采用以下结构，包括：容器8、电阻丝9、气撑杆10、气动夹爪11以及导流部；连接关系如下：In the specific implementation process, the distillation structure preferably adopts the following structure, including: a container 8, a resistance wire 9, a gas strut 10, a pneumatic gripper 11, and a diversion part; the connection relationship is as follows:
容器8安置于底座1上的第一凹槽处，电阻丝9安置于容器8的内部，气撑杆10安置于两个支架的其中一个支架上，气动夹爪11安置于气撑杆10的伸缩端上，导流部活动安置于气动夹爪11的驱动端上。The container 8 is placed at the first groove on the base 1, the resistance wire 9 is placed inside the container 8, the gas strut 10 is placed on one of the two brackets, and the pneumatic gripper 11 is placed on the air strut 10 On the telescopic end, the guide part is movably arranged on the driving end of the pneumatic clamping jaw 11.
在具体实施过程中，需要特殊说明的是，移动部包括：两个滑轨12、两个承载板13以及四个滑板14；连接关系如下：In the specific implementation process, it needs to be specially explained that the moving part includes: two sliding rails 12, two load-bearing plates 13, and four sliding plates 14; the connection relationship is as follows:
两个滑轨12分别安置于两个支架上，两个承载板13分别安置于两个滑轨12上，四个滑板14分别安置于两个承载板13上。Two sliding rails 12 are respectively arranged on two brackets, two bearing plates 13 are respectively arranged on two sliding rails 12, and four sliding plates 14 are respectively arranged on two bearing plates 13.
在具体实施过程中，需要特殊说明的是，导流部，包括：罐体15、第一活塞16、第二活塞22、冷凝管18、牛角管19以及瓶体21，连接关系如下：In the specific implementation process, it needs to be specially explained that the diversion part includes: a tank body 15, a first piston 16, a second piston 22, a condenser tube 18, a horn tube 19, and a bottle body 21. The connection relationship is as follows:
罐体15安置于气动夹爪11的驱动端上，第一活塞16通过螺纹旋接于罐体15上端的罐口处，第二活塞22安置于罐体15上，冷凝管18的一端第二活塞22处，牛角管19通过第三活塞23活动安置于冷凝管18的另一端，冷凝管18的下端安装有支撑组件，瓶体21活动安置于底座1上的第二凹槽处。The tank body 15 is arranged on the driving end of the pneumatic clamping jaw 11, the first piston 16 is screwed to the mouth of the upper end of the tank body 15, the second piston 22 is arranged on the tank body 15, and one end of the condenser tube 18 is second At the piston 22, the horn tube 19 is movably arranged at the other end of the condenser tube 18 through the third piston 23, the lower end of the condenser tube 18 is equipped with a supporting assembly, and the bottle body 21 is movably arranged at the second groove on the base 1.
在具体实施过程中，需要特殊说明的是，支撑组件，包括：两个结构相同的支撑杆25以及固定板26；连接关系如下：In the specific implementation process, it needs to be specially explained that the support assembly includes: two support rods 25 and a fixing plate 26 with the same structure; the connection relationship is as follows:
两个支撑杆25分别安置于固定座上，固定板26分别安置于两个支撑杆25上。The two supporting rods 25 are respectively arranged on the fixing seat, and the fixing plate 26 is respectively arranged on the two supporting rods 25.
通过上述总体情况可知：From the above general situation, we can know:
首先，将向蔗糖脂肪酸酯母液中加入C1～C3醇，静置,静置完成后，将混合物进行过滤，首先将混合物导入第一过滤网4，用第一过滤网4进行简单的过滤，然后通过第一漏斗5流到第二过滤网6上进行精细的过滤，精细过滤后的滤液由第二漏斗7流进罐体15内部，First, add C1-C3 alcohols to the mother liquor of sucrose fatty acid esters and let it stand. After the standing is completed, the mixture is filtered. First, the mixture is introduced into the first filter screen 4, and the first filter screen 4 is used for simple filtration. Then it flows through the first funnel 5 to the second filter screen 6 for fine filtration, and the filtrate after fine filtration flows into the tank 15 from the second funnel 7.
作为优选的，更进一步的，气动夹爪11的驱动端上贴合有减震垫27，罐体15上端的罐口处直径大于罐身直径，罐口直径大于瓶身直径防止罐体15向下脱落，减震垫27用于，当罐体15由于容器8内的溶液沸腾的时候，对罐体15产生波动，当滤液全部流入到罐体15后，工作人员将第一过滤网4以及第二过滤网6通过滑轨12向上进行移动，移动到滑轨12的最顶端后，Preferably, and further, a shock-absorbing pad 27 is attached to the driving end of the pneumatic gripper 11, the diameter of the can mouth at the upper end of the can body 15 is larger than the diameter of the can body, and the diameter of the can mouth is larger than the body diameter to prevent the can body 15 from facing The damping pad 27 is used for when the tank body 15 is boiling due to the solution in the container 8, and the tank body 15 is fluctuated. When all the filtrate flows into the tank body 15, the staff puts the first filter 4 and The second filter screen 6 moves upward through the slide rail 12, and after moving to the top of the slide rail 12,
工作人员将第一活塞16通过螺纹旋接在罐体15上，然后接通电源，电阻丝9开始进行加热，对液体加热至沸腾，由于罐体15底部放置于容器8中间，当容器8内的液体沸腾的时候，滤液随之沸腾，然后进行蒸馏，The worker screwed the first piston 16 to the tank 15 through a thread, and then turned on the power. The resistance wire 9 began to heat and heat the liquid to boiling. Since the bottom of the tank 15 is placed in the middle of the container 8, when the container 8 is When the liquid is boiling, the filtrate will boil with it, and then it will be distilled.
作为优选的，更进一步的，罐体15上安装有支流管24，蒸馏溶液通过直流管流进冷凝管18，此时，冷凝管18连接于自来水水管，在蒸馏溶液通过冷凝的过程中，对蒸馏溶液进行冷却，冷却后的蒸馏溶液通过牛角管19流进瓶体21内，支撑安以及固定板26对冷凝管18进行有效的支撑，得到蔗糖脂肪酸酯产品，当过滤以及蒸馏工艺完成后，将对设备进行清洗，将自来水水管关闭，并自来水水管与冷凝管18断开，随后将第一过滤网4以及第二过滤网6通过滑板14进行拆卸，然后工作人员用手握住罐体15，Preferably, and furthermore, a branch pipe 24 is installed on the tank body 15, and the distilled solution flows into the condenser pipe 18 through the direct-flow pipe. At this time, the condenser pipe 18 is connected to the tap water pipe. When the distilled solution passes through the condensation process, The distilled solution is cooled, and the cooled distilled solution flows into the bottle body 21 through the horn tube 19, and the support and fixing plate 26 effectively support the condenser tube 18 to obtain the sucrose fatty acid ester product. When the filtration and distillation process are completed , The equipment will be cleaned, the tap water pipe will be closed, and the tap water pipe will be disconnected from the condenser tube 18. Then the first filter 4 and the second filter 6 will be disassembled through the slide plate 14, and then the staff will hold the tank with their hands 15,
作为优选的，更进一步的，罐体15上安装有支流管24，第二活塞22活动安置于支流管24上，将第二活塞22向罐体15方向移动，然后将冷 凝管18顺着固定板26向右移动，随之将冷凝管18从第二活塞22上卸下，然后气动夹爪11进行张开，然后将第二气撑杆10将罐体15从气动夹爪11上取下，对罐体15以及冷凝管18进行清洗，Preferably, and furthermore, a branch pipe 24 is installed on the tank body 15, the second piston 22 is movably arranged on the branch pipe 24, the second piston 22 is moved toward the tank body 15, and then the condenser tube 18 is fixed along The plate 26 moves to the right, and then the condenser tube 18 is removed from the second piston 22, and then the pneumatic clamping jaw 11 is opened, and then the second gas strut 10 is used to remove the tank 15 from the pneumatic clamping jaw 11 , Clean the tank 15 and the condenser tube 18,
作为优选的，更进一步的，容器8左侧安装有出水管28，出水管28上安装有阀门29，工作人员将阀门29打开，然后将容器8内的有出水管28流出，将第一活塞16通过螺纹取下，对罐体15进行清洗，然后工作人员将冷凝管18抬起，将瓶体21的蔗糖脂肪酸酯产品拿到指定地点，Preferably, and further, a water outlet pipe 28 is installed on the left side of the container 8, and a valve 29 is installed on the water outlet pipe 28. The staff opens the valve 29, and then flows out the water outlet pipe 28 in the container 8, and sets the first piston 16 is removed through the thread, the tank 15 is cleaned, and then the staff lifts the condenser tube 18, and takes the sucrose fatty acid ester product of the bottle 21 to the designated place.
作为优选的，更进一步的，固定板26上开设有弧形槽，弧形槽上安装有第二防滑胶垫20，然后将冷凝管18拿起，从第三活塞23上抽离，随后对冷凝管18以及牛角管19进行清洗,控制器17采用可编程控制器17，可对电阻丝9进行控制，可控制电阻丝9发热的时长。Preferably, and further, the fixing plate 26 is provided with an arc-shaped groove, and the second non-slip rubber pad 20 is installed on the arc-shaped groove, and then the condenser tube 18 is picked up and removed from the third piston 23, and then The condenser tube 18 and the horn tube 19 are cleaned, and the controller 17 adopts a programmable controller 17, which can control the resistance wire 9 and control the heating time of the resistance wire 9.
作为优选的，更进一步的，气动夹爪11的驱动端上贴合有减震垫27。Preferably, and further, a shock-absorbing pad 27 is attached to the driving end of the pneumatic clamping jaw 11.
作为优选的，更进一步的，罐体15上端的罐口处直径大于罐身直径。Preferably, and further, the diameter of the opening at the upper end of the can body 15 is larger than the diameter of the can body.
作为优选的，更进一步的，罐体15上安装有支流管24，第二活塞22活动安置于支流管24上，瓶体21与支撑座之间贴合有第一防滑胶垫3。Preferably, and further, a branch pipe 24 is installed on the tank body 15, the second piston 22 is movably arranged on the branch pipe 24, and a first anti-slip rubber pad 3 is attached between the bottle body 21 and the support seat.
作为优选的，更进一步的，容器8左侧安装有出水管28，出水管28上安装有阀门29。Preferably, and further, a water outlet pipe 28 is installed on the left side of the container 8, and a valve 29 is installed on the water outlet pipe 28.
作为优选的，更进一步的，固定板26上开设有弧形槽，弧形槽上安装有第二防滑胶垫20。Preferably, and further, the fixing plate 26 is provided with an arc-shaped groove, and the second non-slip rubber pad 20 is installed on the arc-shaped groove.
上述技术方案仅体现了本发明技术方案的优选技术方案，本技术领域的技术人员对其中某些部分所可能做出的一些变动均体现了本发明的原理，属于本发明的保护范围之内。The above technical solutions only embody the preferred technical solutions of the present invention, and those skilled in the art may make some possible changes to some parts of them all embody the principles of the present invention and fall within the protection scope of the present invention.

Claims (10)

  1. 一种精细化工有机合成用过滤蒸馏设备，包括底座(1)，其特征在于，所述底座(1)上开设有第一凹槽以及第二凹槽，所述底座(1)上安装有过滤结构以及蒸馏结构；A filter distillation equipment for fine chemical organic synthesis, comprising a base (1), wherein the base (1) is provided with a first groove and a second groove, and a filter is installed on the base (1). Structure and distillation structure;
    所述过滤结构，包括：两个支板(2)、移动部、第一过滤网(4)、第一漏斗(5)、第二过滤网(6)、第二漏斗(7)以及控制器(17)；The filtering structure includes: two support plates (2), a moving part, a first filter screen (4), a first funnel (5), a second filter screen (6), a second funnel (7), and a controller (17);
    两个所述支板(2)分别安置于底座(1)的前后两端，两个所述移动部分别安置于两个所述支板(2)上，所述第一过滤网(4)的两端分别安置于两个所述移动部上，所述第一漏斗(5)安置于第一过滤网(4)下端，所述第二过滤网(6)的两端分别安置于移动部上，所述第二漏斗(7)安置于第二框架下端，所述控制器(17)安置于底座(1)上。The two supporting plates (2) are respectively arranged on the front and rear ends of the base (1), the two moving parts are respectively arranged on the two supporting plates (2), and the first filter screen (4) The two ends of the filter are respectively arranged on the two moving parts, the first funnel (5) is arranged at the lower end of the first filter screen (4), and the two ends of the second filter screen (6) are respectively arranged on the moving part Above, the second funnel (7) is arranged on the lower end of the second frame, and the controller (17) is arranged on the base (1).
  2. 根据权利要求1所述的一种精细化工有机合成用过滤蒸馏设备，其特征在于，所述蒸馏结构，包括：容器(8)、电阻丝(9)、气撑杆(10)、气动夹爪(11)以及导流部；The filter distillation equipment for fine chemical organic synthesis according to claim 1, wherein the distillation structure comprises: a container (8), a resistance wire (9), a gas strut (10), and a pneumatic gripper (11) and the diversion part;
    所述容器(8)安置于底座(1)上的第一凹槽处，所述电阻丝(9)安置于容器(8)的内部，所述气撑杆(10)安置于两个所述支架的其中一个支架上，所述气动夹爪(11)安置于所述气撑杆(10)的伸缩端上，所述导流部活动安置于气动夹爪(11)的驱动端上。The container (8) is arranged at the first groove on the base (1), the resistance wire (9) is arranged inside the container (8), and the gas struts (10) are arranged on the two On one of the brackets, the pneumatic clamping jaw (11) is arranged on the telescopic end of the air strut (10), and the guide part is movably arranged on the driving end of the pneumatic clamping jaw (11).
  3. 根据权利要求1所述的一种精细化工有机合成用过滤蒸馏设备，其特征在于，所述移动部包括：两个滑轨(12)、两个承载板(13)以及四个滑板(14)；The filter distillation equipment for fine chemical organic synthesis according to claim 1, characterized in that the moving part comprises: two sliding rails (12), two carrying plates (13) and four sliding plates (14) ；
    两个所述滑轨(12)分别安置于两个支架上，两个所述承载板(13)分别安置于两个所述滑轨(12)上，四个所述滑板(14)分别安置于两个所述承载板(13)上。The two sliding rails (12) are respectively arranged on two brackets, the two bearing plates (13) are respectively arranged on the two sliding rails (12), and the four sliding plates (14) are respectively arranged On the two bearing plates (13).
  4. 根据权利要求2所述的一种精细化工有机合成用过滤蒸馏设备，其特征在于，所述导流部，包括：罐体(15)、第一活塞(16)、第二活塞(22)、冷凝管(18)、牛角管(19)以及瓶体(21)；The filter distillation equipment for fine chemical organic synthesis according to claim 2, characterized in that, the diversion part comprises: a tank (15), a first piston (16), a second piston (22), Condensation tube (18), horn tube (19) and bottle body (21);
    所述罐体(15)安置于气动夹爪(11)的驱动端上，所述第一活塞(16)通过螺纹旋接于罐体(15)上端的罐口处，所述第二活塞(22)安置于罐体(15)上， 所述冷凝管(18)的一端第二活塞(22)处，所述牛角管(19)通过第三活塞(23)活动安置于冷凝管(18)的另一端，所述冷凝管(18)的下端安装有支撑组件，所述瓶体(21)活动安置于底座(1)上的第二凹槽处。The tank body (15) is arranged on the driving end of the pneumatic clamping jaw (11), the first piston (16) is screwed to the mouth of the tank body (15) at the upper end of the tank body (15), and the second piston ( 22) Placed on the tank (15), one end of the condenser tube (18) is at the second piston (22), and the horn tube (19) is movably placed on the condenser tube (18) through the third piston (23) At the other end of the condenser tube (18), a support assembly is installed at the lower end, and the bottle body (21) is movably arranged at the second groove on the base (1).
  5. 根据权利要求4所述的一种精细化工有机合成用过滤蒸馏设备，其特征在于，所述支撑组件，包括：两个结构相同的支撑杆(25)以及固定板(26)；The filter distillation equipment for fine chemical organic synthesis according to claim 4, characterized in that, the support assembly comprises: two support rods (25) with the same structure and a fixed plate (26);
    两个所述支撑杆(25)分别安置于固定座上，所述固定板(26)分别安置于两个所述支撑杆(25)上。The two supporting rods (25) are respectively arranged on the fixing seat, and the fixing plate (26) is respectively arranged on the two supporting rods (25).
  6. 根据权利要求2所述的一种精细化工有机合成用过滤蒸馏设备，其特征在于，所述气动夹爪(11)的驱动端上贴合有减震垫(27)。The filter distillation equipment for fine chemical organic synthesis according to claim 2, characterized in that, a shock-absorbing pad (27) is attached to the driving end of the pneumatic gripper (11).
  7. 根据权利要求4所述的一种精细化工有机合成用过滤蒸馏设备，其特征在于，所述罐体(15)上端的罐口处直径大于罐身直径。The filter distillation equipment for fine chemical organic synthesis according to claim 4, characterized in that the diameter of the mouth of the upper end of the tank body (15) is larger than the diameter of the tank body.
  8. 根据权利要求4所述的一种精细化工有机合成用过滤蒸馏设备，其特征在于，所述罐体(15)上安装有支流管(24)，所述第二活塞(22)活动安置于支流管(24)上，所述瓶体(21)与支撑座之间贴合有第一防滑胶垫(3)。The filter distillation equipment for fine chemical organic synthesis according to claim 4, characterized in that a branch pipe (24) is installed on the tank (15), and the second piston (22) is movably arranged on the branch. On the tube (24), a first non-slip rubber pad (3) is attached between the bottle body (21) and the support seat.
  9. 根据权利要求2所述的一种精细化工有机合成用过滤蒸馏设备，其特征在于，所述容器(8)左侧安装有出水管(28)，所述出水管(28)上安装有阀门(29)。The filter distillation equipment for fine chemical organic synthesis according to claim 2, characterized in that a water outlet pipe (28) is installed on the left side of the container (8), and a valve (28) is installed on the water outlet pipe (28). 29).
  10. 根据权利要求5所述的一种精细化工有机合成用过滤蒸馏设备，其特征在于，所述固定板(26)上开设有弧形槽，所述弧形槽上安装有第二防滑胶垫(20)。The filter distillation equipment for fine chemical organic synthesis according to claim 5, characterized in that the fixed plate (26) is provided with an arc-shaped groove, and a second non-slip rubber pad ( 20).
PCT/CN2020/116557 2019-12-31 2020-09-21 Filtering distillation apparatus for fine chemical organic synthesis WO2021135417A1 (en)

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CN111035950A (en) * 2019-12-31 2020-04-21 枣庄学院 Filtration distillation equipment for fine chemical organic synthesis
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