WO2019025670A1 - System for harvesting microalgae and microalga exudates from culture water loaded with same, comprising tangential flow on a membrane filter - Google Patents

System for harvesting microalgae and microalga exudates from culture water loaded with same, comprising tangential flow on a membrane filter Download PDF

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Publication number
WO2019025670A1
WO2019025670A1 PCT/FR2018/000203 FR2018000203W WO2019025670A1 WO 2019025670 A1 WO2019025670 A1 WO 2019025670A1 FR 2018000203 W FR2018000203 W FR 2018000203W WO 2019025670 A1 WO2019025670 A1 WO 2019025670A1
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WIPO (PCT)
Prior art keywords
plate
water
filtered water
channel
circulation
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PCT/FR2018/000203
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French (fr)
Inventor
René-Jean GUILLARD
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Skyworld International Overseas Limited
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Publication of WO2019025670A1 publication Critical patent/WO2019025670A1/en

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D63/00Apparatus in general for separation processes using semi-permeable membranes
    • B01D63/08Flat membrane modules
    • B01D63/082Flat membrane modules comprising a stack of flat membranes
    • B01D63/0822Plate-and-frame devices
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D63/00Apparatus in general for separation processes using semi-permeable membranes
    • B01D63/08Flat membrane modules
    • B01D63/082Flat membrane modules comprising a stack of flat membranes
    • B01D63/084Flat membrane modules comprising a stack of flat membranes at least one flow duct intersecting the membranes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2313/00Details relating to membrane modules or apparatus
    • B01D2313/08Flow guidance means within the module or the apparatus
    • B01D2313/086Meandering flow path over the membrane
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2313/00Details relating to membrane modules or apparatus
    • B01D2313/10Specific supply elements
    • B01D2313/105Supply manifolds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2313/00Details relating to membrane modules or apparatus
    • B01D2313/12Specific discharge elements
    • B01D2313/125Discharge manifolds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2315/00Details relating to the membrane module operation
    • B01D2315/10Cross-flow filtration
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14Ultrafiltration; Microfiltration
    • B01D61/18Apparatus therefor

Definitions

  • the present invention relates to a system for harvesting micro-algae contained in a charged culture water, as well as a method of harvesting these micro-algae. It also relates to a harvesting system and a process for harvesting exudates of microalgae which, when they are placed in very particular situations, in particular stress, have been released into the environment. Moreover, in this respect, the applicants of the present patent application file the same day a patent application which sets out the means they propose to precisely put certain microalgae in these very particular situations so that then they secrete a large quantity of exudates into the medium containing the microalgae. It is then the medium thus loaded which is treated in the aforementioned harvesting system, and this in order to simultaneously allow the recovery of exudates which are found to have been released into the medium.
  • micro-algae The cultivation of micro-algae is an activity more and more widespread around the world.
  • the transparent tubes are superimposed in greenhouses so as to form batteries of rows arranged parallel to one another.
  • the water contained in the culture tubes is kept at temperature by the greenhouse effect, and by an exchanger fed by a hot water circuit.
  • microalgae chosen have a rapid growth, which can give a doubling of biomass in a day, and they are also rich in oils and valuable elements. Very high yields per hectare are obtained, which can be more than a hundred times higher than the yields of plants grown in the soil.
  • micro-algae is processed in a concentration and packaging station, to be delivered in liquid phase in drums. This produces a product presented in limited volumes and masses, which reduces at the same time: transport costs, energy consumption and pollution.
  • microalgae is selected and the parameters of the hydroponic culture are adjusted to obtain specific growths rich in desired elements according to the applications, intended in particular for the pharmaceutical, cosmetic and food markets.
  • concentrated micro-algae are used in particular in the fields of: cosmetics, with lipid extracts, protein extracts and so-called molecules anti-aging ; from the pharmacy, with omega 3/6; food, with human or animal nutritional supplements; from industry, with bio-plastics and dyes; and energy with oil extractions to replace fossil fuels or biomass methaniza- tion.
  • the size of the cells can be very small, usually a few microns, and the structure of these cells is extremely fragile, which makes their harvest difficult.
  • the concentration of biomass in the culture water is generally very low, it is necessary to treat a large amount of water to, in fact, harvest only a few grams of biomass. Thus, for this meager harvest, it is nevertheless still necessary to recycle in parallel a significant amount of water, which implies significant costs.
  • the so-called reverse osmosis technique is not very satisfactory because, since, by transfer through a semi-selective membrane, it is necessary to separate under the effect of a pressure gradient a liquid product called permeate. , which passes through the filter membrane, and a solid product said concentrate or retentate, which does not pass through the membrane, it is understood that, in this case, the biomass, which is structurally very fragile, would be deteriorated. In addition, the clogging of the pores of the filters is often irreversible, thus requiring the rapid change of the latter.
  • the system in question comprises a filter membrane having porosities water filter loaded in holding micro-algae, a water distribution plate charge which is applied against the face of the filtering membrane situated on the side of the arrival of the charged water and which has at least one tangential circulation channel of charged water, and a circulation plate of the filtered water which is applied against the opposite face of the filter membrane and which comprises at least one filtered water circulation channel, the harvesting system comprising at least one subassembly, successively comprising a charged water distribution plate, a first filter membrane, a filter plate, flow of the filtered water and a second filter membrane which is applied against the face of the filtered water circulation plate which is located on the side opposite to that of the In the first diaphragm, the assembly consisting of the distribution
  • the filtered water circulation channel of the filtered water circulation plate consists of several concentric circular channels, some of which are connected by a radial channel.
  • This system has the disadvantage that, because of the arrangement of the latter channel, the filtration efficiency through the membrane is not optimal.
  • the aforementioned document relates to the filtration of very diverse fluids, in particular macromolecular solutions, without aiming more particularly at the culture of microalgae.
  • both the tangential circulation channel of water loaded with the plate of The distribution and the filtered water circulation channel of the circulation plate are channels extending rectilinearly between their inlet and outlet.
  • the declogging possibly necessary is therefore carried out by reverse scanning.
  • the present invention is intended in particular to avoid the various disadvantages mentioned above in connection with the prior art and it is more particularly aimed at improving the efficiency of membrane filtration.
  • An advantage of this harvesting system is that the tangential flow channel or channels impose on the charged water a circulation which is tangent on the surface of the membrane. filter and which is carried out with a certain speed depending on the flow and the section of these channels, which has the effect of carrying micro-algae by distributing them along the channels, that is to say avoiding a local accumulation.
  • the biomass can be harvested without risk of deterioration of the cells.
  • micro-algae harvest By “charged water,” one will understand indifferently water loaded with micro-algae or water loaded with exudates of micro-algae.
  • the harvesting system according to the invention may additionally comprise one or more of the following characteristics, which may be combined with each other.
  • the or each subassembly has bores passing through each subassembly and comprising a piercing of charged water supply practiced in isolation in each filtering membrane and in each circulation plate of the filtered water opposite from the supply inlet of the channel of each distribution plate, a microalgae harvest piercing connected to the collection outlet of the channel.
  • each distribution plate and the hole corresponding thereto pierced opposite in the filter membrane glued under said plate and in each water circulation plate filtered a filtered water bore connected to the collection outlet of each filtered water circulation plate and the corresponding orifice pierced opposite in the filter membrane located under said filtered water circulation plate and a through hole for injecting compressed air pierced in the filtered water circulation plate.
  • the upstream or inlet end of the filtered water circulation channel of the filtered water circulation plate is located close to but slightly away from the projection, on said filtered water circulation plate. , the supply of the distribution plate and that the other end of the filtered water circulation channel opens into an outlet which is distinct from the projection, on said filtered water circulation plate, of the collection exit.
  • the first filter membrane is glued under the distribution plate.
  • the pressurized air line crosses the subset from bottom to top, forming a succession of bends at the level of the filtered water collecting plates, the pressurized air duct opening into the filtered water circulation channel cut from each filtered water collection plate and, conversely, does not open into any charged water circulation channel cut in each distribution plate.
  • each filter membrane has a coating of a material having an extremely low coefficient of friction, the face thus coated being the upper face with respect to the filtering membrane bonded to the distribution plate and the underside for the filter membrane glued to the circulation plate of the filtered water.
  • the arrival of charged water is connected to a water column having at its top a float.
  • the harvesting system comprises a return of a small portion of filtered water at the top of the column.
  • the harvesting system according to the invention comprises means for treating the filtered water with ultraviolet rays.
  • each membrane has a face having an extremely low coefficient of friction, such as polytetrafluoroethylene, and a rough face consisting of polyvinylidene fluoride.
  • the second object of the invention is a process for harvesting micro-algae and micro-algae exudates contained in charged culture water, said method using a filter membrane having porosities filtering the water loaded with water. retaining said micro-algae, said method being characterized in that it consists in circulating tangentially the water charged on the upper face of this filter membrane located on the side of the arrival of this charged water, in at least one channel of circulation, and to evacuate the collection of micro-algae through a collection outlet located at the other end of said circulation channel.
  • the harvesting method according to the invention uses a filter membrane having pores filtering the charged water retaining these microalgae, at least one circulation channel, a charged water inlet located at one end of the circulation channel, a crop outlet located at the other end of the circulation channel and a filtered water outlet, such a method is remarkable in that it comprises a harvest cycle of circulating tangentially the water loaded on the the filter membrane located on the side of the charged water inlet, in the circulation channel, by closing the crop outlet and by opening the filtered water outlet, to automatically detect a rise in pressure of charged water due to a progressive clogging of the filtering membrane, to be closed the filtered water outlet and open the crop outlet, to inject compressed air from the filtered water outlet to the loaded water inlet so as to detach the micro-algae deposited and to return to the beginning cycle by closing the crop outlet and opening the filtered water outlet.
  • a pure water flow rate is controlled, which flow of pure water causes, by tangential effect, the micro-algae detached from the channel thus providing a concentrate at the crop outlet. ..
  • the injection of compressed air is at very low pressure.
  • the harvest cycle takes place under very low pressure.
  • FIG. 1 is an exploded view of a stack of a harvest system according to the invention, having a single subset of membranes and distribution and circulation plates disposed between two clamping plates;
  • FIGS. 2 and 3 are front views of the circulation plates of this stack, namely a distribution plate and a permeate circulation plate for, respectively, the charged water and the filtered water, comprising circulation each forming a spiral;
  • FIG. 4 is a front view of each filter membrane of this stack.
  • FIG. 5 is a view of a harvest system forming a complete installation.
  • FIG. 1 illustrates, for the harvesting system according to the invention, a subassembly 12 comprising a stack of rectangular flat panels, having a first filter membrane 2 receiving, glued above, a plate 4 for distributing the water loaded microalgae and, glued below, a plate 6 for collecting the filtered water.
  • the subassembly 12 also includes a second filter membrane 2, which is glued below the filtered water collection plate 6.
  • the complete stack of the harvesting system according to the invention comprises a succession of such superposed identical subassemblies 12, said superposition of subassemblies 12 being clamped between two thick and rigid end clamping plates 8.
  • Each clamping plate 8 comprises, in the vicinity of its periphery, a series of bores 10 fitted on corresponding bores made in the filtering membranes 2 and in the distribution and collecting plates 6, which bores 10 receive clamping screws passing through the together.
  • the thick clamping plates distribute the pressure of the clamping screws evenly over the entire surface of the various components of the stack.
  • FIG. 2 shows a view from above of the plate 4 for dispensing charged water, which plate is cut in its thickness so as to produce a channel of constant width 20 drawn in a spiral having an external beginning or end 22 forming an inlet of charged water, disposed near an angle of said plate 4, then five turns tapering progressively towards the center of this plate and ending with an end or inner end 24 constituting a harvesting outlet concentrated microalgae schematically by the arrow 28.
  • the free part in the center of the spiral formed by the channel 20 further comprises a circular bore 26 independent of this channel, this drilling being intended to allow the vertical passage of the filtered water which is shown schematically in Figure 1 by the arrow SI .
  • Figure 3 shows in top view the filtered water collection plate 6, which is similarly cut in its thickness so as to achieve a similar channel 38 for collecting filtered water forming the same spiral.
  • the inner end 34 of the channel 38 is also slightly offset from that 24 of the distribution plate 4, and it is very precisely aligned with the circular bore 26 of said distribution plate to allow in turn the vertical passage SI of filtered water.
  • a circular bore 36 independent of the channel 38, is aligned with the inner end 24 constituting the crop outlet of the concentrated microalgae of the distribution plate 4, to form a means for the vertical passage of harvest.
  • the holes 10 of the clamping screws are arranged on the outer contour of these plates, as well as in their center and in the vicinity of this center, so as to obtain the best distribution of the clamping pressure. while avoiding crossing the channels 20, 38.
  • FIG. 4 shows a top view of the filtering membrane
  • the filter membrane 2 is formed of a porous material which retains particles whose size is greater than the diameters of its porosities in the channel 20 of the distribution plate 4, which size may be for example of the order of one micron, porous material which instead allows the filtered liquid to pass on the other side to the channel 38 of the filtered water collection plate 6.
  • the two distribution plates 4 and collection 6 are bonded to the porous membrane 2 ⁇ , on both sides of it.
  • the surface of the porous membrane 2 ⁇ which faces the channel 20 of the distribution plate 4, that is to say the upper face, is made of a non-stick material such as "Teflon", in order to obtain the best possible slip of the microalgae harvested on this upper surface.
  • a variable number of modular subassemblies 12 are arranged between the two clamping plates 8, thus forming for each subassembly a filtration circuit arranged in parallel.
  • each subassembly 12 will comprise a second porous membrane 2B identical to the first, this second membrane being bonded under the collection plate 6.
  • this variant with two membranes , 2B which is glued under the collection plate 6 will be by its side does not include the release material.
  • the upper clamping plate 8 comprises a common feed of charged water E which is aligned with the vertical feed bores 22 and 32, and which therefore feeds all the distribution plates 4 and passes only through all the collecting plates 6 and the filtering membranes 2.
  • the lower clamping plate 8 has a common harvesting outlet S2 aligned with the vertical harvesting holes 24 and 36, which is fed by all, the distribution plates 4, and a common filtered water outlet SI which is aligned with the vertical bores of filtered water 26 and 34, and which is therefore fed by all the collection plates 6.
  • the water distribution plate 4 loaded with microalgae, the plate 6 for collecting the filtered water and the membrane 2, or both membranes 2 of each subassembly 12 is pierced in the vicinity of one of their angles with a through hole, respectively 27 for the plate 4, 37 for the plate 6 and 47 for each membrane 2.
  • the holes 27 and 37 are substantially aligned on the entire height of the harvesting system, to the extent that the hole 37 passing through the plate 6 is tangent, or even opens slightly into the channel 38 while the hole 27 passing through the plate 4 is slightly offset towards the center of this plate so as to However, the holes 27 and 47 which pass through the plates 4 and respectively the membranes 2 are perfectly aligned.
  • micro-algae-laden water is circulated in the stack of the subassemblies 12, from the upper subassembly, the crop outlet S2 being closed and the filtered water outlet SI being however open.
  • All the channels 20 of the distribution plates 4 have identical flow rates, thanks to the parallel arrangement of all these plates and a construction carried out identically between all these plates 4.
  • the biomass harvesting cycle is done by closing the filtered water outlet SI, by opening the crop outlet S2, and injecting compressed air at very low pressure, for example 50 gr / cm 2 , into the through hole 47 of the membrane 2B (or in the through hole 37 of the collection plate 6) of the subset 12 of the lowest harvesting system.
  • compressed air at very low pressure, for example 50 gr / cm 2
  • a passage of micro-bubbles of air is obtained through all the filtering membranes 2, in the opposite direction of the passage of the filtered water, that is to say from bottom to top, by circulating first in the channel 38 then in the channel 20, and these micro-bubbles repel and thus detach the micro-algae deposited on the walls of the channels 20 of the filter membranes 2 which are glued under the distribution plates 4.
  • the microalgae have been detached from the filtering membranes 2 and are in suspension in the space between the two teflon surfaces facing each other on the said membranes 2 which surround the membrane. plate 4 concerned.
  • An exemplary embodiment of the micro system ⁇ harvesting algae described above is to use plates 4 and 6 which are made of metal or plastics, for example Plexiglas or polypropylene.
  • the filter membranes may be of the type marketed under the name ML-2F by the Chinese company Minglie, which is headquartered in Shanghai.
  • the face having an extremely low coefficient of friction is composed of polytetrafluoroethylene (PTFE) and the rough side is made of polyvinylidene fluoride (PVDF).
  • PTFE polytetrafluoroethylene
  • PVDF polyvinylidene fluoride
  • the porosity of such membranes can be chosen in a range from 0.05 ⁇ to 1 ⁇ .
  • FIG. 5 represents an example of an installation making it possible to implement the invention, this installation comprising a chassis 40 forming a cage made of aluminum profiles, placed on rollers 42 and having above four lifting rings 44 .
  • the stack of subassemblies of panels 12 arranged between the two clamping plates 8 is fixed inside the frame 40, on a tank 52 for recovering the filtered water which oozes outside this stack, in particular by the edges lateral filter membranes after crossing their thicknesses.
  • the chassis 40 comprises a mast 48 supporting a water column 46 connected to the inlet of charged water coming from the photo-bioreactors, comprising an equivalent level of water, column which is equipped at its top with a float 50 framed by two upper and lower level witnesses.
  • this water column 46 forming an expansion vessel, it firstly obtains a protection against any excess pressure that may damage the filter membranes 2.
  • Filtered water is continuously returned to the photo bioreactors for recycling and limiting outside water consumption.
  • ultraviolet treatment of the stream of filtered water is carried out at the outlet of the harvesting system, which, with filtration by the membranes, maintains an acceptable sanitary level of the culture medium by reducing the concentration of bacteria or micro-organisms. -organisms that can colonize the fluid circuits.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)

Abstract

The present invention relates to a system for harvesting microalgae from culture water loaded with same, said system comprising at least one sub-assembly (12) having a plate (4) for distributing the loaded water, provided with a loaded water tangential flow channel (20), a first membrane filter (2A) filtering the water by retaining the microalgae, a plate (6) for the flow of the filtered water, having at least one filtered water flow channel (38), and a second membrane filter (2B), wherein the assembly consisting of the plate (4) and of the first membrane (2A) has a feed inlet (22) at one end of the channel (20) and a collecting outlet (24) at the other end of the channel (20). The system is characterised in that it comprises a means for blowing a pressurised air stream in order to clean the surface of each membrane (2A), and in that the channel (38) is disposed substantially opposite the channel (20).

Description

SYSTÈME DE RÉCOLTE DE MICRO-ALGUES ET D'EXSUDATS DE MICROALGUES DANS UNE EAU DE CULTURE CHARGÉE, COMPORTANT UNE  MICRO-ALGAE HARVESTING SYSTEM AND MICROALGAE EXUDATES IN CHARGED CULTURE WATER, COMPRISING A
CIRCULATION TANGENTIELLE SUR UNE MEMBRANE FILTRANTE DOMAINE TECHNIQUE DE L' INVENTION  TANGENTIAL CIRCULATION ON A FILTERING MEMBRANE TECHNICAL FIELD OF THE INVENTION
La présente invention concerne un système de récolte de micro-algues contenues dans une eau de culture chargée, ainsi qu'un procédé de récolte de ces micro-algues. Elle a également trait à un système de récolte et à un procédé de récolte des exsudats de micro-algues qui, lorsque ces dernières sont placées dans des situations bien particulières, notamment de stress, ont été libérés dans le milieu. D'ailleurs, à cet égard, les déposants de la présente demande de brevet déposent ce même jour une demande de brevet qui expose les moyens qu' ils proposent pour, précisément, mettre certaines micro-algues dans ces situations bien particulières afin qu' alors elles sécrètent une quantité importante d' exsudats dans le milieu contenant les micro-algues. C'est alors le milieu ainsi chargé qui est traité dans le système de récolte précité, et ce afin de permettre simultanément la récupération d' exsudats qui se trouvent avoir été relargués dans le milieu. The present invention relates to a system for harvesting micro-algae contained in a charged culture water, as well as a method of harvesting these micro-algae. It also relates to a harvesting system and a process for harvesting exudates of microalgae which, when they are placed in very particular situations, in particular stress, have been released into the environment. Moreover, in this respect, the applicants of the present patent application file the same day a patent application which sets out the means they propose to precisely put certain microalgae in these very particular situations so that then they secrete a large quantity of exudates into the medium containing the microalgae. It is then the medium thus loaded which is treated in the aforementioned harvesting system, and this in order to simultaneously allow the recovery of exudates which are found to have been released into the medium.
ARRIÈRE PLAN TECHNOLOGIQUE DE L' INVENTION BACKGROUND OF THE INVENTION
La culture de micro-algues est une activité de plus en plus répandue à travers le monde. The cultivation of micro-algae is an activity more and more widespread around the world.
A ce propos, il est connu de réaliser des cultures dites hydroponiques , c'est-à-dire hors-sol, de. micro-algues sélectionnées qui se développent dans des tubes transparents appelés photo-bioréacteurs ou encore "PBR" par abréviation, ces tubes recevant une solution liquide contenant des éléments nutritifs NPK ainsi que du dioxyde de carbone dissous dans cette solution liquide afin de synthétiser de manière rapide la biomasse. Avantageusement, les tubes transparents sont superposés dans des serres afin de former des batteries de rangées disposées parallèlement les unes aux autres. L'eau contenue dans les tubes de culture est maintenue à température par l'effet de serre, et par un échangeur alimenté par un circuit d'eau chaude. In this respect, it is known to produce so-called hydroponic, that is to say, above-ground, cultures. selected micro-algae that develop in transparent tubes called photo-bioreactors or "PBR" by abbreviation, these tubes receiving a liquid solution containing NPK nutrients as well as carbon dioxide dissolved in this liquid solution to synthesize fast biomass. Advantageously, the transparent tubes are superimposed in greenhouses so as to form batteries of rows arranged parallel to one another. The water contained in the culture tubes is kept at temperature by the greenhouse effect, and by an exchanger fed by a hot water circuit.
Pour ces cultures hors-sol, on peut en particulier utiliser des résidus organiques venant d'une unité de méthanisation de déchets agricoles ou d'effluents d'élevages. On peut aussi utiliser le gaz produit par cette unité de méthanisation pour alimenter une unité de cogénération qui délivre la chaleur et l'électricité nécessaire pour les cultures.  For these crops above ground, it is possible in particular to use organic residues from a methanization unit of agricultural waste or livestock effluents. The gas produced by this methanation unit can also be used to supply a cogeneration unit that delivers the heat and electricity required for the crops.
Il est également connu de cultiver les micro-algues en bassins ouverts, ou fermés sous serre, suivant un mode de culture appelé " raceway ".  It is also known to cultivate micro-algae in open ponds, or closed under greenhouse, according to a mode of culture called "raceway".
Les variétés de micro-algues choisies présentent une croissance rapide, qui peut donner un doublement de la biomasse en une journée, et elles sont en outre riches en huiles et en éléments valorisables . On obtient des rendements à l'hectare très élevés, qui peuvent être plus de cent fois supérieurs aux rendements des plantes cultivées en terre.  The varieties of microalgae chosen have a rapid growth, which can give a doubling of biomass in a day, and they are also rich in oils and valuable elements. Very high yields per hectare are obtained, which can be more than a hundred times higher than the yields of plants grown in the soil.
La production de micro-algues est traitée dans un poste de concentration et de conditionnement, pour être livrée en phase liquide dans des fûts. On obtient ainsi un produit présenté selon des volumes et des masses limités, ce qui permet de réduire tout à la fois : les coûts des transports, la consommation d'énergie et la pollution.  The production of micro-algae is processed in a concentration and packaging station, to be delivered in liquid phase in drums. This produces a product presented in limited volumes and masses, which reduces at the same time: transport costs, energy consumption and pollution.
On choisit le type de micro-algues et on ajuste les paramètres de la culture hydroponique pour obtenir des croissances spécifiques riches en éléments recherchés suivant les applications, destinés notamment aux marchés pharmaceutiques, cosmétiques et alimentaires.  The type of microalgae is selected and the parameters of the hydroponic culture are adjusted to obtain specific growths rich in desired elements according to the applications, intended in particular for the pharmaceutical, cosmetic and food markets.
Pour exemples, les micro-algues concentrées sont utilisées en particulier dans les domaines : de la cosmétique, avec des extraits lipidiques, protéiniques ainsi que des molécules dites anti-âge ; de la pharmacie, avec les oméga 3/6 ; de l'alimentation, avec des compléments nutrit ionnels humains ou animaux ; de l'industrie, avec les bio-plastiques et les colorants ; et de l'énergie avec des extractions d'huile pour remplacer les énergies fossiles ou la méthanisat ion de la biomasse . For example, concentrated micro-algae are used in particular in the fields of: cosmetics, with lipid extracts, protein extracts and so-called molecules anti-aging ; from the pharmacy, with omega 3/6; food, with human or animal nutritional supplements; from industry, with bio-plastics and dyes; and energy with oil extractions to replace fossil fuels or biomass methaniza- tion.
Cela étant, la récolte d'une telle biomasse arrivée à maturité, c'est-à-dire la séparation des micro-algues de leur milieu de culture, pose différents problèmes techniques et financiers.  However, the harvesting of such a mature biomass, ie the separation of micro-algae from their culture medium, poses different technical and financial problems.
En effet, la taille des cellules peut être très réduite, en général de quelques microns, et la structure de ces cellules est extrêmement fragile, ce qui rend leur récolte délicate. En outre, dès lors que la concentration de la biomasse dans l'eau de culture est généralement très faible, il faut nécessairement traiter une grande quantité d'eau pour, dans les faits, ne récolter que seulement quelques grammes de biomasse. Ainsi, pour cette maigre récolte, il faut néanmoins toujours recycler en parallèle une quantité importante d'eau, ce qui implique des coûts importants.  Indeed, the size of the cells can be very small, usually a few microns, and the structure of these cells is extremely fragile, which makes their harvest difficult. In addition, since the concentration of biomass in the culture water is generally very low, it is necessary to treat a large amount of water to, in fact, harvest only a few grams of biomass. Thus, for this meager harvest, it is nevertheless still necessary to recycle in parallel a significant amount of water, which implies significant costs.
Différents systèmes de filtration de l'eau permettant de réaliser les récoltes sont connus. Ces systèmes sont cependant toujours dérivés de procédés utilisés pour d'autres activités, et ils nécessitent donc des compromis. Ils sont souvent mal adaptés. De plus, ils peuvent consommer une grande quantité d'énergie pour maintenir la circulation de l'eau, ce qui augmente les coûts de récolte.  Various water filtration systems for harvesting are known. However, these systems are still derived from processes used for other activities, and therefore require compromise. They are often poorly adapted. In addition, they can consume a large amount of energy to maintain the flow of water, which increases the costs of harvesting.
Pour exemple, la technique dite de l'osmose inverse n'est guère satisfaisante car, dès lors que, par transfert à travers une membrane semi-sélective, il faut séparer sous l'effet d'un gradient de pression un produit liquide dit perméat, qui passe à travers la membrane filtrante, et un produit solide dit concentrât ou rétentat, qui ne passe pas à travers la membrane, on comprend que, dans le cas présent, la biomasse, qui est structurellement très fragile, serait détériorée. Au surplus, le colmatage des pores des filtres est souvent irréversible, nécessitant en conséquence le changement rapide de ces derniers. For example, the so-called reverse osmosis technique is not very satisfactory because, since, by transfer through a semi-selective membrane, it is necessary to separate under the effect of a pressure gradient a liquid product called permeate. , which passes through the filter membrane, and a solid product said concentrate or retentate, which does not pass through the membrane, it is understood that, in this case, the biomass, which is structurally very fragile, would be deteriorated. In addition, the clogging of the pores of the filters is often irreversible, thus requiring the rapid change of the latter.
Parmi les systèmes de filtration de fluides liquides chargés indiqués ci-dessus, on connaît plus particulièrement, par exemple par le brevet US 3.560.377, un système de récolte de macromolécules par ultrafiltration selon un trajet en spirale. Par extrapolation à l'invention, il est possible de considérer que le système en question comprend une membrane filtrante présentant des porosités filtrant l'eau chargée en retenant des micro-algues, une plaque de distribution de l'eau chargée qui' est appliquée contre la face de la membrane filtrante située du côté de l'arrivée de l'eau chargée et qui présente au moins un canal de circulation tangentielle d'eau chargée, et une plaque de circulation de l'eau filtrée qui est appliquée contre la face opposée de la membrane filtrante et qui comprend au moins un canal de circulation d'eau filtrée, le système de récolte comportant au moins un sous-ensemble, comprenant successivement une plaque de distribution de l'eau chargée, une première membrane filtrante, une plaque de circulation de l'eau filtrée et une deuxième membrane filtrante qui est appliquée contre la face de la plaque de circulation de l'eau filtrée qui est située du côté opposé à celui de la première membrane, l'ensemble constitué de la plaque de distribution et de la première membrane filtrante comporte une entrée d'alimentation se trouvant à une extrémité du canal ou des canaux de circulation tangentielle d'eau chargée et une sortie de collecte se trouvant à l'autre extrémité du canal ou de ces canaux d'eau chargée, le ou chaque sous-ensemble présentant des perçages traversant l'ensemble et comprenant un perçage d'alimentation en eau chargée et un perçage de sortie d'eau filtrée. Among the charged liquid fluid filtration systems indicated above, there is more particularly known, for example from US Pat. No. 3,560,377, a system for harvesting macromolecules by ultrafiltration in a spiral path. By extrapolation with the invention, it is possible to consider that the system in question comprises a filter membrane having porosities water filter loaded in holding micro-algae, a water distribution plate charge which is applied against the face of the filtering membrane situated on the side of the arrival of the charged water and which has at least one tangential circulation channel of charged water, and a circulation plate of the filtered water which is applied against the opposite face of the filter membrane and which comprises at least one filtered water circulation channel, the harvesting system comprising at least one subassembly, successively comprising a charged water distribution plate, a first filter membrane, a filter plate, flow of the filtered water and a second filter membrane which is applied against the face of the filtered water circulation plate which is located on the side opposite to that of the In the first diaphragm, the assembly consisting of the distribution plate and the first filter membrane has a feed inlet at one end of the channel or tangential circulation channels of charged water and a collection outlet at Another end of the channel or channels of charged water, wherein the or each subassembly has bores passing through the assembly and including a filled water supply bore and a filtered water outlet bore.
Toutefois, dans ce système, le canal de circulation d'eau filtrée de la plaque de circulation de l'eau filtrée est constitué de plusieurs canaux circulaires concentriques dont certains sont reliés par un canal radial. Ce système présente l'inconvénient que, du fait de l'agencement de ce dernier canal, l'efficacité de filtration à travers la membrane n'est pas optimale. However, in this system, the filtered water circulation channel of the filtered water circulation plate consists of several concentric circular channels, some of which are connected by a radial channel. This system has the disadvantage that, because of the arrangement of the latter channel, the filtration efficiency through the membrane is not optimal.
Par ailleurs, il n'est en aucun cas prévu l'introduction d'impulsions d'air. Le décolmatage éventuellement nécessaire s'effectue par balayage inverse.  Moreover, it is in no case provided the introduction of air pulses. The declogging possibly necessary is carried out by reverse scanning.
Le document précité concerne la filtration de fluides très divers, en particulier de solutions macromoléculaires, sans viser plus particulièrement la culture de micro-algues.  The aforementioned document relates to the filtration of very diverse fluids, in particular macromolecular solutions, without aiming more particularly at the culture of microalgae.
On connaît également, par exemple par la demande de brevet It is also known, for example by the patent application
US 201 /0.238.235 , un système de filtration du même type, mais dans lequel, d'une manière encore moins efficace concernant la filtration à travers la membrane, à la fois le canal de circulation tangentielle d'eau chargée de la plaque de distribution et le canal de circulation d'eau filtrée de la plaque de circulation sont des canaux s ' étendant d'une manière rectiligne entre leur entrée et leur sortie. US 201 / 0,238,235, a filtration system of the same type, but in which, even less effectively concerning the filtration through the membrane, both the tangential circulation channel of water loaded with the plate of The distribution and the filtered water circulation channel of the circulation plate are channels extending rectilinearly between their inlet and outlet.
Ce document mentionne en particulier la filtration de culture de micro-algues.  This document mentions in particular the culture filtration of micro-algae.
On remarque qu'il est mentionné dans ce document l'introduction d'impulsions d'air dans le canal de circulation de la plaque de distribution, mais cela n'est prévu qu'au cours d'un test effectué pour faire fluctuer de manière importante la pression dans ce canal à des fins de vérification, alors qu'il est par ailleurs précisé que la pression normale est stable sans introduction d'air.  Note that it is mentioned in this document the introduction of air pulses in the distribution channel of the distribution plate, but this is only expected during a test performed to fluctuate so the pressure in this channel for verification purposes, while it is also stated that the normal pressure is stable without introduction of air.
Le décolmatage éventuellement nécessaire s'effectue donc par balayage inverse.  The declogging possibly necessary is therefore carried out by reverse scanning.
On connaît encore, par exemple par la publication de la demande de brevet allemand DE 37.31.864, un système du type précité, mais dans lequel il n'est pas prévu de sous-ensemble comportant une deuxième membrane filtrante, de sorte que la filtration est encore moins efficace que dans les deux cas précités. Il ne s'agit que d'un système de test, il concerne une culture de cellules d'une manière générale et il n'est prévu aucun moyen de décolmatage. Le canal de la plaque de distribution a une forme générale présentant un changement de direction afin de réduire l'usure de la membrane. It is also known, for example from the publication of the German patent application DE 37.31.864, a system of the aforementioned type, but in which there is no provision for a subassembly comprising a second filter membrane, so that the filtration is even less effective than in the two cases mentioned above. It's just a test system, it's about a cell culture in general and no means of declogging is provided. The distribution plate channel has a general shape with a change of direction to reduce the wear of the membrane.
On connaît enfin, par exemple par la demande de brevet britannique GB 2.360.958, un autre système de récolte qui ne présente pas non plus de sous-ensemble comportant une deuxième membrane. Bien que présentant des « méandres » pour réduire le colmatage, le système fait partie d'un agencement de récolte très différent.  Finally, there is known, for example from British patent application GB 2,360,958, another harvesting system which does not have either a subassembly comprising a second membrane. Although having "meanders" to reduce clogging, the system is part of a very different harvesting arrangement.
DESCRIPTION GÉNÉRALE DE L ' INVENTION GENERAL DESCRIPTION OF THE INVENTION
La présente invention a notamment pour but d'éviter les divers inconvénients mentionnés ci-dessus à propos de la technique antérieure et elle vise plus particulièrement à améliorer l'efficacité de la filtration des membranes. The present invention is intended in particular to avoid the various disadvantages mentioned above in connection with the prior art and it is more particularly aimed at improving the efficiency of membrane filtration.
Elle propose à cet effet un système de récolte du type enseigné pour partie par le brevet US 3.560.377, ledit système étant caractérisé en ce qu' il comprend en outre un moyen pour insuffler un flux d'air sous pression à travers le canal de circulation d'eau filtrée de chaque plaque de collecte de l'eau filtrée, à travers la membrane filtrante, afin de décoller les micro-algues et de décolmater la surface de chaque membrane filtrante sur laquelle lesdites micro-algues se sont accumulées, en ce qu'au moins un canal de circulation tangentielle d'eau chargée et au moins le canal de circulation d'eau filtrée qui lui fait face forment chacun une spirale, et en ce que le ou les canaux de circulation d' eau filtrée sont sensiblement disposés en face du canal ou, respectivement, en face du ou des canaux de circulation tangentielle d'eau chargée.  It proposes for this purpose a harvesting system of the type taught in part by US Pat. No. 3,560,377, said system being characterized in that it further comprises means for blowing a flow of air under pressure through the channel of circulating filtered water from each filtered water collecting plate, through the filter membrane, in order to detach the micro-algae and to decolour the surface of each filter membrane on which said micro-algae have accumulated, in that at least one tangential circulation channel of charged water and at least the filtered water circulation channel which faces it each form a spiral, and in that the channel (s) for circulating filtered water are substantially arranged in front of the channel or, respectively, in front of the tangential flow channel or channels of charged water.
Un avantage de ce système de récolte est que le ou les canaux de circulation tangentielle imposent à l'eau chargée une circulation qui est tangente sur la surface de la membrane filtrante et qui est réalisée avec une certaine vitesse dépendant du débit et de la section de ces canaux, ce qui a pour effet d'emporter les micro-algues en les répartissant le long des canaux, c'est-à-dire en évitant une accumulation locale. An advantage of this harvesting system is that the tangential flow channel or channels impose on the charged water a circulation which is tangent on the surface of the membrane. filter and which is carried out with a certain speed depending on the flow and the section of these channels, which has the effect of carrying micro-algae by distributing them along the channels, that is to say avoiding a local accumulation.
On obtient ainsi une dépose sensiblement constante des micro¬ algues sur la longueur des canaux, dépose qui donc limite l'obstruction locale de la membrane filtrante et donne un bon débit au travers de cette membrane en permettant d'utiliser avec le meilleur rendement l'ensemble de sa surface et d'espacer les ramassages dans le système de récolte. La consommation d'énergie est réduite, ainsi que les coûts de production. This results in a substantially constant removal of micro ¬ algae along the length of the channels, which therefore limits the local obstruction of the filter membrane and gives a good flow through this membrane allowing to use with the best performance the all of its surface and to space the pick-ups in the harvesting system. Energy consumption is reduced as well as production costs.
Au surplus, puisque le système selon l'invention fonctionne sous très basse pression, la biomasse peut être récoltée sans risque de détérioration des cellules.  In addition, since the system according to the invention operates under very low pressure, the biomass can be harvested without risk of deterioration of the cells.
Bien que l'invention s'applique aussi bien à la récolte de micro-algues qu'à celle d' exsudats de micro-algues, ces deux applications, dans toute la suite de la description ainsi que dans les revendications, seront dans un souci de simplification réunies sous l'expression « récolte de micro-algues ». Par « eau chargée, » on comprendra ainsi indifféremment une eau chargée en micro-algues ou une eau chargée en exsudats de micro-algues.  Although the invention applies both to the harvest of microalgae and that of exudates of micro-algae, these two applications, throughout the remainder of the description as well as in the claims, will be in a concern. simplification under the term "micro-algae harvest". By "charged water," one will understand indifferently water loaded with micro-algae or water loaded with exudates of micro-algae.
Le système de récolte selon l'invention peut de surcroît comporter une ou plusieurs des caractéristiques suivantes, qui peuvent être combinées entre elles.  The harvesting system according to the invention may additionally comprise one or more of the following characteristics, which may be combined with each other.
Selon une construction préférentielle, le ou chaque sous- ensemble présente des perçages traversant chaque sous-ensemble et comprenant un perçage d' alimentation en eau chargée pratiqué de façon isolée dans chaque membrane filtrante et dans chaque plaque de circulation de l'eau filtrée en regard de l'entrée d'alimentation du canal de chaque plaque de distribution, un perçage de récolte de micro-algues relié à la sortie de collecte du canal de. chaque plaque de distribution et à l'orifice qui lui correspond percé en regard dans la membrane filtrante collée sous ladite plaque et dans chaque plaque de circulation de l'eau filtrée, un perçage d'eau filtrée relié à la sortie de collecte de chaque plaque de circulation de l'eau filtrée et à l'orifice qui lui correspond percé en regard dans la membrane filtrante située sous ladite plaque de circulation de l'eau filtrée et un trou traversant d'injection d'air comprimé percé dans la plaque de circulation d'eau filtrée. According to a preferred construction, the or each subassembly has bores passing through each subassembly and comprising a piercing of charged water supply practiced in isolation in each filtering membrane and in each circulation plate of the filtered water opposite from the supply inlet of the channel of each distribution plate, a microalgae harvest piercing connected to the collection outlet of the channel. each distribution plate and the hole corresponding thereto pierced opposite in the filter membrane glued under said plate and in each water circulation plate filtered, a filtered water bore connected to the collection outlet of each filtered water circulation plate and the corresponding orifice pierced opposite in the filter membrane located under said filtered water circulation plate and a through hole for injecting compressed air pierced in the filtered water circulation plate.
De manière avantageuse, l'extrémité amont ou entrée du canal de circulation d'eau filtrée de la plaque de circulation de l'eau filtrée est située à proximité mais légèrement en retrait de la projection, sur ladite plaque de circulation de l'eau filtrée, de l'alimentation de la plaque de distribution et en ce que l'autre extrémité du canal de circulation d'eau filtrée débouche dans une sortie qui est distincte de la projection, sur ladite plaque de circulation de l'eau filtrée, de la sortie de collecte.  Advantageously, the upstream or inlet end of the filtered water circulation channel of the filtered water circulation plate is located close to but slightly away from the projection, on said filtered water circulation plate. , the supply of the distribution plate and that the other end of the filtered water circulation channel opens into an outlet which is distinct from the projection, on said filtered water circulation plate, of the collection exit.
Selon un mode de réalisation préféré, la première membrane filtrante est collée sous la plaque de distribution.  According to a preferred embodiment, the first filter membrane is glued under the distribution plate.
Selon une autre construction préférentielle, la conduite d'air sous pression traverse de bas en haut le sous-ensemble, en formant une succession de coudes au niveau des plaques de collecte de l'eau filtrée, la conduite d'air sous pression débouchant dans le canal de circulation d'eau filtrée découpé dans chaque plaque de collecte de l'eau filtrée et, à l'inverse, ne débouchant dans aucun canal de circulation d' eau chargée découpé dans chaque plaque de distribution.  According to another preferred construction, the pressurized air line crosses the subset from bottom to top, forming a succession of bends at the level of the filtered water collecting plates, the pressurized air duct opening into the filtered water circulation channel cut from each filtered water collection plate and, conversely, does not open into any charged water circulation channel cut in each distribution plate.
De préférence encore, au moins une face de chaque membrane filtrante présente un revêtement d'un matériau présentant un coefficient de frottement extrêmement faible, la face ainsi revêtue étant la face supérieure pour ce qui est de la membrane filtrante collée à la plaque de distribution et la face inférieure pour ce qui est de la membrane filtrante collée à la plaque de circulation de l'eau filtrée.  More preferably, at least one face of each filter membrane has a coating of a material having an extremely low coefficient of friction, the face thus coated being the upper face with respect to the filtering membrane bonded to the distribution plate and the underside for the filter membrane glued to the circulation plate of the filtered water.
Toujours avantageusement, l'arrivée d'eau chargée est reliée à une colonne d'eau comportant à son sommet un flotteur. Dans cette construction, le système de récolte comporte un renvoi d'une petite partie d'eau filtrée en haut de la colonne. Still advantageously, the arrival of charged water is connected to a water column having at its top a float. In this construction, the harvesting system comprises a return of a small portion of filtered water at the top of the column.
De préférence encore, le système de récolte selon l'invention comporte des moyens permettant de traiter l'eau filtrée aux rayons ultraviolets.  More preferably, the harvesting system according to the invention comprises means for treating the filtered water with ultraviolet rays.
Selon encore une autre forme de réalisation particulièrement avantageuse, chaque membrane comporte une face présentant un coefficient de frottement extrêmement faible, tel que du polytétrafluoroéthylène , et une face rugueuse constituée de polyfluorure de vinylidène.  According to yet another particularly advantageous embodiment, each membrane has a face having an extremely low coefficient of friction, such as polytetrafluoroethylene, and a rough face consisting of polyvinylidene fluoride.
L'invention a pour second objet un procédé de récolte de micro-algues et d' exsudats de micro-algues contenu (e) s dans une eau de culture chargée, ledit procédé utilisant une membrane filtrante présentant des porosités filtrant l'eau chargée en retenant ces micro-algues, ledit procédé étant caractérisé en ce qu'il consiste à faire circuler tangentiellement l'eau chargée sur la face supérieure de cette membrane filtrante située du côté de l'arrivée de cette eau chargée, dans au moins un canal de circulation, et à évacuer la collecte de micro-algues à travers une sortie de collecte située à l'autre extrémité dudit canal de circulation.  The second object of the invention is a process for harvesting micro-algae and micro-algae exudates contained in charged culture water, said method using a filter membrane having porosities filtering the water loaded with water. retaining said micro-algae, said method being characterized in that it consists in circulating tangentially the water charged on the upper face of this filter membrane located on the side of the arrival of this charged water, in at least one channel of circulation, and to evacuate the collection of micro-algae through a collection outlet located at the other end of said circulation channel.
Lorsque le procédé de récolte selon l'invention utilise une membrane filtrante présentant des porosités filtrant l'eau chargée en retenant ces micro-algues, au moins un canal de circulation, une arrivée d' eau chargée située à une extrémité du canal de circulation, une sortie de récolte située à l'autre extrémité du canal de circulation et une sortie d'eau filtrée, un tel procédé est remarquable en ce qu' il comprend un cycle de récolte consistant à faire circuler tangentiellement l'eau chargée sur la face de la membrane filtrante située du côté de l'arrivée d'eau chargée, dans le canal de circulation, en fermant la sortie de récolte et en ouvrant la sortie d'eau filtrée, à détecter automatiquement une montée en pression d'eau chargée due à un colmatage progressif de la membrane filtrante, à fermer la sortie d'eau filtrée et à ouvrir la sortie de récolte, à injecter de l'air comprimé de la sortie d'eau filtrée vers l'arrivée d'eau chargée de façon à détacher les micro-algues déposées et à revenir au début du cycle en fermant la sortie de récolte et en ouvrant la sortie d'eau filtrée. When the harvesting method according to the invention uses a filter membrane having pores filtering the charged water retaining these microalgae, at least one circulation channel, a charged water inlet located at one end of the circulation channel, a crop outlet located at the other end of the circulation channel and a filtered water outlet, such a method is remarkable in that it comprises a harvest cycle of circulating tangentially the water loaded on the the filter membrane located on the side of the charged water inlet, in the circulation channel, by closing the crop outlet and by opening the filtered water outlet, to automatically detect a rise in pressure of charged water due to a progressive clogging of the filtering membrane, to be closed the filtered water outlet and open the crop outlet, to inject compressed air from the filtered water outlet to the loaded water inlet so as to detach the micro-algae deposited and to return to the beginning cycle by closing the crop outlet and opening the filtered water outlet.
De préférence, en même temps que l'injection d'air comprimé, on commande un débit d'eau pure, lequel débit d'eau pure entraine par effet tangentiel des micro-algues décollées du canal fournissant ainsi un concentrât à la sortie de récolte..  Preferably, at the same time as the injection of compressed air, a pure water flow rate is controlled, which flow of pure water causes, by tangential effect, the micro-algae detached from the channel thus providing a concentrate at the crop outlet. ..
De préférence également, l'injection d'air comprimé est à très basse pression.  Also preferably, the injection of compressed air is at very low pressure.
De préférence encore, le cycle de récolte a lieu sous très basse pression. BRÈVE DESCRIPTION DES DESSINS  More preferably, the harvest cycle takes place under very low pressure. BRIEF DESCRIPTION OF THE DRAWINGS
L' invention sera mieux comprise et d' autres caractéristiques et avantages apparaîtront plus clairement à la lecture de la description ci-après donnée à titre d'exemple, en référence aux dessins annexés dans lesquels : The invention will be better understood and other features and advantages will appear more clearly on reading the following description given by way of example, with reference to the appended drawings in which:
- la figure 1 est une vue éclatée d'un empilement d'un système de récolte suivant l'invention, présentant un seul sous-ensemble de membranes et de plaques de distribution et de circulation disposé entre deux plaques de serrage ;  - Figure 1 is an exploded view of a stack of a harvest system according to the invention, having a single subset of membranes and distribution and circulation plates disposed between two clamping plates;
- les figures 2 et 3 sont des vues de face des plaques de circulation de cet empilement, à savoir une plaque de distribution et une plaque de circulation du perméat pour, respectivement, l'eau chargée et l'eau filtrée, comportant des canaux de circulation formant chacun une spirale ;  FIGS. 2 and 3 are front views of the circulation plates of this stack, namely a distribution plate and a permeate circulation plate for, respectively, the charged water and the filtered water, comprising circulation each forming a spiral;
- La figure 4 est une vue de face de chaque membrane filtrante de cet empilement ; et  FIG. 4 is a front view of each filter membrane of this stack; and
- la figure 5 est une vue d'un système de récolte formant une installation complète. DESCRIPTION D ' UN MODE DE RÉALISATION PRÉFÉRÉ DE L ' INVENTION - Figure 5 is a view of a harvest system forming a complete installation. DESCRIPTION OF A PREFERRED EMBODIMENT OF THE INVENTION
La figure 1 illustre, pour le système de récolte selon l'invention, un sous-ensemble 12 comprenant un empilement de panneaux plats rectangulaires, présentant une première membrane filtrante 2 recevant, collée au-dessus, une plaque 4 de distribution de l'eau chargée en micro-algues et, collée en- dessous, une plaque 6 de collecte de l'eau filtrée. Le sous- ensemble 12 comporte aussi une deuxième membrane filtrante 2, qui est collée en-dessous de la plaque de collecte de l'eau filtrée 6. FIG. 1 illustrates, for the harvesting system according to the invention, a subassembly 12 comprising a stack of rectangular flat panels, having a first filter membrane 2 receiving, glued above, a plate 4 for distributing the water loaded microalgae and, glued below, a plate 6 for collecting the filtered water. The subassembly 12 also includes a second filter membrane 2, which is glued below the filtered water collection plate 6.
L'empilement complet du système de récolte selon l'invention comporte une succession de tels sous-ensembles 12 identiques superposés, ladite superposition de sous-ensembles 12 étant serrée entre deux plaques de serrage d'extrémité, épaisses et rigides 8.  The complete stack of the harvesting system according to the invention comprises a succession of such superposed identical subassemblies 12, said superposition of subassemblies 12 being clamped between two thick and rigid end clamping plates 8.
Chaque plaque de serrage 8 comporte au voisinage de sa périphérie une série de perçages 10 ajustés sur des perçages correspondant réalisés dans les membranes filtrantes 2 et dans les plaques de distribution 4 et de collecte 6, lesquels perçages 10 reçoivent des vis de serrage traversant l'ensemble. Les plaques de serrage épaisses permettent de répartir uniformément la pression des vis de serrage sur toute la surface des différents composants de l'empilement.  Each clamping plate 8 comprises, in the vicinity of its periphery, a series of bores 10 fitted on corresponding bores made in the filtering membranes 2 and in the distribution and collecting plates 6, which bores 10 receive clamping screws passing through the together. The thick clamping plates distribute the pressure of the clamping screws evenly over the entire surface of the various components of the stack.
La figure 2 présente en vue de dessus la plaque 4 de distribution d'eau chargée, plaque qui est découpée dans son épaisseur de sorte à réaliser un canal de largeur constante 20 dessiné suivant une spirale présentant un début ou extrémité extérieure 22 formant une entrée d'eau chargée, disposée près d'un angle de ladite plaque 4, puis cinq tours se resserrant progressivement en direction du centre de cette plaque et se terminant par une fin ou extrémité intérieure 24 constituant une sortie de récolte des micro-algues concentrées schématisée par la flèche 28. La partie libre au centre de la spirale que forme le canal 20 comporte en outre un perçage circulaire 26 indépendant de ce canal, ce perçage étant destiné à permettre le passage vertical de l'eau filtrée qui est schématisé à la figure 1 par la flèche SI. FIG. 2 shows a view from above of the plate 4 for dispensing charged water, which plate is cut in its thickness so as to produce a channel of constant width 20 drawn in a spiral having an external beginning or end 22 forming an inlet of charged water, disposed near an angle of said plate 4, then five turns tapering progressively towards the center of this plate and ending with an end or inner end 24 constituting a harvesting outlet concentrated microalgae schematically by the arrow 28. The free part in the center of the spiral formed by the channel 20 further comprises a circular bore 26 independent of this channel, this drilling being intended to allow the vertical passage of the filtered water which is shown schematically in Figure 1 by the arrow SI .
La figure 3 présente en vue de dessus la plaque 6 de collecte d'eau filtrée, qui est, de la même manière, découpée dans son épaisseur de sorte à réaliser un canal similaire 38 de collecte d'eau filtrée formant la même spirale.  Figure 3 shows in top view the filtered water collection plate 6, which is similarly cut in its thickness so as to achieve a similar channel 38 for collecting filtered water forming the same spiral.
Le début ou extrémité extérieure 30 de ce canal de collecte The beginning or outer end 30 of this collection channel
38 est un peu décalé de celui 22 de la plaque de distribution 4, un perçage circulaire 32, voisin mais totalement indépendant de ce canal 38, destiné à permettre le passage vertical de l'eau chargée, étant en revanche aligné avec l'extrémité extérieure 22 du canal 20 de ladite plaque de distribution. 38 is slightly offset from that 22 of the distribution plate 4, a circular bore 32, adjacent but totally independent of this channel 38, intended to allow the vertical passage of the charged water, being on the other hand aligned with the outer end 22 of the channel 20 of said distribution plate.
L'extrémité intérieure 34 du canal 38 est aussi un peu décalée de celle 24 de la plaque de distribution 4, et elle est très précisément alignée avec le perçage circulaire 26 de ladite plaque de distribution afin de permettre à son tour le passage vertical SI de l'eau filtrée.  The inner end 34 of the channel 38 is also slightly offset from that 24 of the distribution plate 4, and it is very precisely aligned with the circular bore 26 of said distribution plate to allow in turn the vertical passage SI of filtered water.
Un perçage circulaire 36, indépendant du canal 38, est aligné sur l'extrémité intérieure 24 constituant la sortie de récolte des micro-algues concentrées de la plaque de distribution 4, en vue de former un moyen permettant le passage vertical de récolte.  A circular bore 36, independent of the channel 38, is aligned with the inner end 24 constituting the crop outlet of the concentrated microalgae of the distribution plate 4, to form a means for the vertical passage of harvest.
Sur ces deux plaques 4 et 6, les perçages 10 des vis de serrage sont disposés sur le contour extérieur de ces plaques, ainsi qu'en leur centre et au voisinage de ce centre, de manière à obtenir la meilleure répartition de la pression de serrage tout en évitant de traverser les canaux 20, 38.  On these two plates 4 and 6, the holes 10 of the clamping screws are arranged on the outer contour of these plates, as well as in their center and in the vicinity of this center, so as to obtain the best distribution of the clamping pressure. while avoiding crossing the channels 20, 38.
La figure 4 présente en vue de dessus la membrane filtrante FIG. 4 shows a top view of the filtering membrane
2, laquelle comprend trois perçages circulaires alignés sur ceux des plaques de distribution 4 et de collecte 6, à savoir un premier perçage extérieur 32 destiné à permettre le passage vertical de l'eau chargée, un deuxième perçage intérieur 26 destiné à permettre le passage vertical de l'eau filtrée et un troisième perçage intérieur 36 destiné à permettre le passage vertical de récolte. 2, which comprises three circular holes aligned with those of the distribution and collection plates 4 and 6, namely a first external bore 32 intended to allow the vertical passage of the charged water, a second internal bore 26 intended to allow the vertical passage of the filtered water and a third internal bore 36 for allowing the vertical passage of harvest.
La membrane filtrante 2 est formée d' une matière poreuse qui retient les particules dont la dimension est supérieure aux diamètres de ses porosités dans le canal 20 de la plaque de distribution 4, dimension qui peut être par exemple de l'ordre de un micron, matière poreuse qui en revanche laisse le liquide filtré passer de l'autre côté vers le canal 38 de la plaque de collecte de l'eau filtrée 6.  The filter membrane 2 is formed of a porous material which retains particles whose size is greater than the diameters of its porosities in the channel 20 of the distribution plate 4, which size may be for example of the order of one micron, porous material which instead allows the filtered liquid to pass on the other side to the channel 38 of the filtered water collection plate 6.
Les deux plaques de distribution 4 et de collecte 6 sont collées sur la membrane poreuse 2Ά, de part et d' autre de celle- ci . Avantageusement, la surface de la membrane poreuse 2Δ qui fait face au canal 20 de la plaque de distribution 4, c'est-à- dire la face supérieure, est constituée d'un matériau antiadhésif tel que du « Téflon », et ce afin d'obtenir le meilleur glissement possible des micro-algues récoltées sur cette face supérieure .  The two distribution plates 4 and collection 6 are bonded to the porous membrane 2Ά, on both sides of it. Advantageously, the surface of the porous membrane 2Δ which faces the channel 20 of the distribution plate 4, that is to say the upper face, is made of a non-stick material such as "Teflon", in order to to obtain the best possible slip of the microalgae harvested on this upper surface.
On dispose un nombre variable de sous-ensembles modulaires 12 entre les deux plaques de serrage 8, formant ainsi pour chaque sous-ensemble un circuit de filtration disposé en parallèle.  A variable number of modular subassemblies 12 are arranged between the two clamping plates 8, thus forming for each subassembly a filtration circuit arranged in parallel.
Avantageusement, ainsi qu'il a été représenté à la figure 1, chaque sous-ensemble 12 comportera une deuxième membrane poreuse 2B identique à la première, cette deuxième membrane étant collée sous la plaque de collecte 6. Toutefois, dans cette variante à deux membranes, celle 2B qui est collée sous la plaque de collecte 6 le sera par sa face ne comportant pas le matériau antiadhésif.  Advantageously, as shown in FIG. 1, each subassembly 12 will comprise a second porous membrane 2B identical to the first, this second membrane being bonded under the collection plate 6. However, in this variant with two membranes , 2B which is glued under the collection plate 6 will be by its side does not include the release material.
Autrement dit, dans cette construction, ce sont les faces les plus rugueuses des deux membranes 2 qui seront disposées en vis- à-vis, en encadrant la plaque de collecte 6.  In other words, in this construction, it is the roughest faces of the two membranes 2 which will be arranged facing each other, framing the collecting plate 6.
La plaque supérieure 8 de serrage comporte une alimentation commune en eau chargée E qui est alignée sur les perçages verticaux d'alimentation 22 et 32, et qui alimente donc toutes les plaques de distribution 4 et ne fait que traverser toutes les plaques de collecte 6 et les membranes filtrantes 2. La plaque inférieure 8 de serrage comporte une sortie commune de récolte S2 alignée sur les perçages verticaux de récolte 24 et 36, qui est alimentée par toutes, les plaques de distribution 4, ainsi qu'une sortie commune d'eau filtrée SI qui est alignée sur les perçages verticaux d'eau filtrée 26 et 34, et qui est donc alimentée par toutes les plaques de collecte 6. The upper clamping plate 8 comprises a common feed of charged water E which is aligned with the vertical feed bores 22 and 32, and which therefore feeds all the distribution plates 4 and passes only through all the collecting plates 6 and the filtering membranes 2. The lower clamping plate 8 has a common harvesting outlet S2 aligned with the vertical harvesting holes 24 and 36, which is fed by all, the distribution plates 4, and a common filtered water outlet SI which is aligned with the vertical bores of filtered water 26 and 34, and which is therefore fed by all the collection plates 6.
Enfin, dans un but bien précis qui sera exposé ci-après, la plaque 4 de distribution de l'eau chargée en micro-algues, la plaque 6 de collecte de l'eau filtrée et la membrane 2, voire les deux membranes 2 de chaque sous-ensemble 12 sont percées au voisinage de l'un de leurs angles d'un trou traversant, respectivement 27 pour la plaque 4, 37 pour la plaque 6 et 47 pour chaque membrane 2. Les trous 27 et 37 sont sensiblement alignés sur toute la hauteur du système de récolte, à la nuance près que le trou 37 traversant la plaque 6 est tangent, voire débouche légèrement dans le canal 38 alors que le trou 27 traversant la plaque 4 est légèrement décalé vers le centre de cette plaque afin d'être éloigné du canal 20. En revanche, les trous 27 et 47 qui traversent les plaques 4 et respectivement les membranes 2 sont parfaitement alignés.  Finally, for a specific purpose which will be explained below, the water distribution plate 4 loaded with microalgae, the plate 6 for collecting the filtered water and the membrane 2, or both membranes 2 of each subassembly 12 is pierced in the vicinity of one of their angles with a through hole, respectively 27 for the plate 4, 37 for the plate 6 and 47 for each membrane 2. The holes 27 and 37 are substantially aligned on the entire height of the harvesting system, to the extent that the hole 37 passing through the plate 6 is tangent, or even opens slightly into the channel 38 while the hole 27 passing through the plate 4 is slightly offset towards the center of this plate so as to However, the holes 27 and 47 which pass through the plates 4 and respectively the membranes 2 are perfectly aligned.
En choisissant le nombre de sous-ensembles modulaires 12, on peut ainsi réaliser un circuit de filtration comprenant une surface de filtre variable et une capacité de récolte qui est ainsi facilement ajustable.  By choosing the number of modular sub-assemblies 12, it is thus possible to produce a filtration circuit comprising a variable filter surface and a harvesting capacity which is thus easily adjustable.
Le fonctionnement du système de récolte décrit ci-dessus est le suivant.  The operation of the harvesting system described above is as follows.
On fait circuler l'eau chargée en micro-algues dans l'empilement des sous-ensembles 12, à partir du sous-ensemble supérieur, la sortie de récolte S2 étant fermée et la sortie d'eau filtrée SI étant en revanche ouverte. Tous les canaux 20 des plaques de distribution 4 présentent des débits identiques, grâce à la disposition en parallèle de toutes ces plaques et d'une construction réalisée à l'identique entre toutes ces plaques 4. The micro-algae-laden water is circulated in the stack of the subassemblies 12, from the upper subassembly, the crop outlet S2 being closed and the filtered water outlet SI being however open. All the channels 20 of the distribution plates 4 have identical flow rates, thanks to the parallel arrangement of all these plates and a construction carried out identically between all these plates 4.
L'eau chargée avançant dans chaque canal 20 de plaque de distribution 4, on obtient tout au long de ces canaux un débit d'eau filtrée au travers des membranes filtrantes 2 disposées sous chaque plaque 4 et, simultanément, un dépôt des micro-algues sur les surfaces de ces membranes.  With the charged water advancing in each channel 20 of distribution plate 4, a flow of water filtered through the filtering membranes 2 placed under each plate 4 and simultaneously a deposit of the micro-algae is obtained along these channels. on the surfaces of these membranes.
Il se produit alors progressivement un colmatage des surfaces des membranes filtrantes 2 qui se traduit par une réduction du débit et une montée en pression de l'eau chargée. Cette montée en pression est détectée automatiquement, pour déclencher un cycle de récolte de la biomasse.  There is then gradually a clogging of the surfaces of the filtering membranes 2 which results in a reduction of the flow rate and a rise in pressure of the charged water. This rise in pressure is detected automatically, to trigger a cycle of harvesting biomass.
Le cycle de récolte de la biomasse se fait en fermant la sortie d'eau filtrée SI, en ouvrant la sortie de récolte S2, et en injectant de l'air comprimé à très basse pression, par exemple 50 gr/cm2 , dans le trou traversant 47 de la membrane 2B (ou dans le trou traversant 37 de la plaque de collecte 6) du sous-ensemble 12 le plus bas du système de récolte. On obtient un passage de micro-bulles d'air au travers de toutes les membranes filtrantes 2, dans le sens inverse de passage de l'eau filtrée, c'est-à- dire de bas en haut, en circulant d'abord dans le canal 38 puis dans le canal 20, et ces micro-bulles repoussent et détachent ainsi les micro-algues déposées sur les parois des canaux 20 des membranes filtrantes 2 qui sont collées sous les plaques 4 de distribution. The biomass harvesting cycle is done by closing the filtered water outlet SI, by opening the crop outlet S2, and injecting compressed air at very low pressure, for example 50 gr / cm 2 , into the through hole 47 of the membrane 2B (or in the through hole 37 of the collection plate 6) of the subset 12 of the lowest harvesting system. A passage of micro-bubbles of air is obtained through all the filtering membranes 2, in the opposite direction of the passage of the filtered water, that is to say from bottom to top, by circulating first in the channel 38 then in the channel 20, and these micro-bubbles repel and thus detach the micro-algae deposited on the walls of the channels 20 of the filter membranes 2 which are glued under the distribution plates 4.
Ainsi, au niveau de chaque plaque 4, les micro-algues ont été détachées des membranes filtrantes 2 et se trouvent en suspension dans l'espace situé entre les deux surfaces téflonées en vis-à- vis présentes sur les dites membranes 2 qui encadrent la plaque 4 concernée.  Thus, at each plate 4, the microalgae have been detached from the filtering membranes 2 and are in suspension in the space between the two teflon surfaces facing each other on the said membranes 2 which surround the membrane. plate 4 concerned.
En commandant en même temps pendant un court instant un débit d'eau pure dans les plaques de distribution 4, lequel débit d'eau entraine alors par un effet tangentiel l'ensemble des microalgues qui ont été décollées des parois des canaux 20, et on obtient ainsi à la sortie de récolte S2 un concentrât comprenant dans une suspension une forte densité de micro-algues qui se trouvent être en parfait état dès lors que le traitement qu'elles ont subi a été constamment doux, et toujours sous très basse pression. By simultaneously controlling for a short time a flow of pure water in the distribution plates 4, which flow of water then leads by a tangential effect all the microalgae that have been detached from the walls of the channels 20, and thus obtaining at harvest outlet S2 a concentrate comprising in a suspension a high density of micro-algae which are found in perfect condition since the treatment they have undergone has been constantly mild, and still under very low pressure.
Un exemple de réalisation du système de récolte de micro¬ algues décrit ci-dessus consiste à utiliser des plaques 4 et 6 qui sont métalliques ou en matière plastique, par exemple en plexiglas ou en polypropylène . An exemplary embodiment of the micro system ¬ harvesting algae described above is to use plates 4 and 6 which are made of metal or plastics, for example Plexiglas or polypropylene.
Les membranes filtrantes peuvent être du type de celles commercialisées sous la dénomination ML-2F par la société chinoise Minglie dont le siège est à Shanghai. La face présentant un coefficient de frottement extrêmement faible est constituée de polytétrafluoroéthylène (PTFE) et la face rugueuse est constituée de polyfluorure de vinylidène (PVDF) .  The filter membranes may be of the type marketed under the name ML-2F by the Chinese company Minglie, which is headquartered in Shanghai. The face having an extremely low coefficient of friction is composed of polytetrafluoroethylene (PTFE) and the rough side is made of polyvinylidene fluoride (PVDF).
La porosité de telles membranes peut être choisie dans une gamme allant de 0,05 μ à 1 μ.  The porosity of such membranes can be chosen in a range from 0.05 μ to 1 μ.
La figure 5 représente un exemple d' installation permettant de mettre en œuvre l'invention, cette installation comprenant un châssis 40 formant une cage réalisée en profilés d'aluminium, posée sur des roulettes 42 et disposant au-dessus de quatre anneaux de levage 44.  FIG. 5 represents an example of an installation making it possible to implement the invention, this installation comprising a chassis 40 forming a cage made of aluminum profiles, placed on rollers 42 and having above four lifting rings 44 .
L' empilement des sous-ensembles de panneaux 12 disposés entre les deux plaques de serrage 8 est fixé à l'intérieur du châssis 40, sur un bac 52 de récupération des eaux filtrées qui suintent en dehors de cet empilement, en particulier par les bords latéraux des membranes filtrantes après une traversée de leurs épaisseurs .  The stack of subassemblies of panels 12 arranged between the two clamping plates 8 is fixed inside the frame 40, on a tank 52 for recovering the filtered water which oozes outside this stack, in particular by the edges lateral filter membranes after crossing their thicknesses.
Le châssis 40 comporte un mât 48 supportant une colonne d'eau 46 reliée à l'entrée d'eau chargée venant des photo-bioréacteurs, comprenant un niveau d'eau équivalent, colonne qui est équipée à son sommet d'un flotteur 50 encadré par deux témoins de niveau supérieur et inférieur. Par cette colonne d'eau 46 formant un vase d'expansion, on obtient d'abord une protection contre les surpressions éventuelles risquant d'endommager les membranes filtrantes 2. The chassis 40 comprises a mast 48 supporting a water column 46 connected to the inlet of charged water coming from the photo-bioreactors, comprising an equivalent level of water, column which is equipped at its top with a float 50 framed by two upper and lower level witnesses. By this water column 46 forming an expansion vessel, it firstly obtains a protection against any excess pressure that may damage the filter membranes 2.
Lors du démarrage du débit d' eau chargée dans le système de récolte, juste après une récolte, les membranes filtrantes 2 n'étant donc pas colmatées, on obtient le débit d'eau maximum qui provoque une perte de charge et une baisse de la pression d'alimentation. Le flotteur 50 est alors à son niveau bas.  When starting the flow of water loaded into the harvesting system, just after a harvest, the filter membranes 2 are not clogged, we obtain the maximum water flow which causes a loss of load and a drop in the supply pressure. The float 50 is then at its low level.
Suivant l'avancement de la récolte, les membranes filtrantes 2 se colmatent, le débit d'eau chargée baisse et sa pression augmente légèrement. On provoque alors une montée du flotteur 50 qui, arrivant au témoin supérieur, indique que le colmatage est suffisant pour effectuer la récolte des micro-algues. On lance alors un cycle de récolte.  Depending on the progress of the harvest, the filter membranes 2 become clogged, the flow of charged water decreases and its pressure increases slightly. It then causes a rise of the float 50 which, arriving at the upper control, indicates that the clogging is sufficient to carry out the harvest of micro-algae. We then launch a harvest cycle.
Par ailleurs, on renvoie en permanence une petite partie de l'eau filtrée en haut de la colonne 46, pour repousser en continu la montée d'eau chargée dans la colonne sans en modifier son niveau, et donc son principe de fonctionnement. On conserve ainsi une eau filtrée dans la colonne qui évite une stagnation d'eau chargée et une salissure des parois transparentes.  Furthermore, a small portion of the filtered water is continuously returned to the top of the column 46, to continuously repel the rise of water loaded into the column without modifying its level, and therefore its operating principle. Filtered water is thus preserved in the column which avoids stagnation of charged water and soiling of the transparent walls.
L'eau filtrée est renvoyée en continu dans les photo- bioréacteurs afin de la recycler et de limiter la consommation d'eau extérieure. Avantageusement, on réalise un traitement aux rayons ultraviolets du flux d'eau filtrée en sortie du système de récolte, ce qui, avec la filtration par les membranes, maintient un niveau sanitaire acceptable du milieu de culture en réduisant la concentration de bactéries ou de micro-organismes qui peuvent coloniser les circuits de fluide.  Filtered water is continuously returned to the photo bioreactors for recycling and limiting outside water consumption. Advantageously, ultraviolet treatment of the stream of filtered water is carried out at the outlet of the harvesting system, which, with filtration by the membranes, maintains an acceptable sanitary level of the culture medium by reducing the concentration of bacteria or micro-organisms. -organisms that can colonize the fluid circuits.
On obtient ainsi un système de récolte simple et efficace, demandant peu d'entretien, comportant un bon rendement et consommant peu d'énergie.  This results in a simple and efficient harvesting system that requires little maintenance, is efficient and consumes little energy.
Comme il va de soi, l'invention ne se limite pas aux seuls modes d'exécution préférentiels décrits ci-dessus. Elle embrasse au contraire toutes les variantes possibles de réalisation, pour autant que ces dernières ne sortent pas du cadre délimité par les revendications ci-jointes qui définissent la portée de la présente invention. It goes without saying that the invention is not limited to the only preferred embodiments described above. On the contrary, it embraces all the possible variants of embodiment, insofar as the latter do not go beyond the scope delimited by the appended claims which define the scope of the present invention.

Claims

REVENDICATIONS
1 - Système de récolte de micro-algues et d'exsudats de micro¬ algues contenu (e) s dans une eau de culture chargée, ledit système comprenant une membrane filtrante (2A) présentant des porosités filtrant l'eau chargée en retenant ces micro-algues, une plaque (4) de distribution de l'eau chargée qui est appliquée contre la face de la membrane filtrante (2A) située du côté de l'arrivée de l'eau chargée (22) et qui présente au moins un canal (20) de circulation tangentielle d'eau chargée, et une plaque (6) de circulation de l'eau filtrée qui est appliquée contre la face opposée de la membrane filtrante (2A) et qui comprend au moins un canal (38) de circulation d'eau filtrée, le système de récolte comportant au moins un sous-ensemble (12), comprenant successivement une plaque (4) de distribution de l'eau chargée, une première membrane filtrante (2A), une plaque (6) de circulation de l'eau filtrée et une deuxième membrane filtrante (2B) qui est appliquée contre la face de la plaque (6) de circulation de l'eau filtrée qui est située du côté opposé à celui de la première membrane (2A) , l'assemblage constitué de la plaque de distribution (4) et de la première membrane filtrante (2A) comporte une entrée d'alimentation (22) se trouvant à une extrémité du canal (20) ou des canaux de circulation tangentielle d'eau chargée et une sortie de collecte (24) se trouvant à l'autre extrémité du canal (20) ou de ces canaux d'eau chargée, le ou chaque sous-ensemble (12) présentant des perçages traversant ledit sous-ensemble (12) et comprenant un perçage (22, 32) d'alimentation en eau chargée, un perçage (24, 36) de récolte de micro-algues et un perçage (26, 34) de sortie d'eau filtrée 1 - microalgae harvesting system and micro algae exudates ¬ content (s) in a charged culture water, said system comprising a filter membrane (2A) having filter pores contaminated water retaining these micro algae, a plate (4) for dispensing the charged water which is applied against the face of the filtering membrane (2A) located on the side of the arrival of the charged water (22) and which has at least one channel (20) tangential circulation of charged water, and a plate (6) for circulating the filtered water which is applied against the opposite face of the filter membrane (2A) and which comprises at least one circulation channel (38). of filtered water, the harvesting system comprising at least one subassembly (12), successively comprising a plate (4) for distributing the charged water, a first filtering membrane (2A), a circulation plate (6). filtered water and a second filter membrane (2B) which is applied against the face of the filtered water circulation plate (6) which is situated on the side opposite to that of the first membrane (2A), the assembly consisting of the distribution plate (4) and the first filter membrane ( 2A) has a supply inlet (22) at one end of the channel (20) or tangential circulation channels of charged water and a collection outlet (24) at the other end of the channel (20). ) or of these channels of charged water, the or each subassembly (12) having bores passing through said subassembly (12) and comprising a piercing hole (22, 32) charged with water, a piercing (24) , 36) microalgae harvesting and a filtered water outlet bore (26, 34)
caractérisé en ce qu' il comprend en outre un moyen pour insuffler un flux d'air sous pression à travers le canal (38) de circulation d'eau filtrée de chaque plaque (6) de collecte de l'eau filtrée, à travers la membrane filtrante (2A), afin de décoller les micro-algues et de décolmater la surface de chaque membrane filtrante (2A) sur laquelle lesdites micro-algues se sont accumulées, en ce qu'au moins un canal (20) de circulation tangentielle d'eau chargée et au moins le canal (38) de circulation d'eau filtrée qui lui fait face forment chacun une spirale, et en ce que le ou les canaux (38) de circulation d'eau filtrée sont sensiblement disposés en face du canal (20) ou, respectivement, en face du ou des canaux (20) de circulation tangentielle d'eau chargée. 2 - Système de récolte selon la revendication 1, caractérisé en ce que le ou chaque sous-ensemble (12) présente des perçages traversant chaque sous-ensemble et comprenant un perçage d'alimentation en eau chargée (32) pratiqué de façon isolée dans chaque membrane filtrante (2) et dans chaque plaque (6) de circulation de l'eau filtrée en regard de l'entrée d'alimentation (22) du canal (20) de chaque plaque de distribution (4) , un perçage de récolte (36) de micro-algues relié à la sortie de collecte (24) du canal (20) de chaque plaque (4) de distribution et à l'orifice (36) qui lui correspond percé en regard dans la membrane filtrante (2A) collée sous ladite plaque (4) et dans chaque plaque (6) de circulation de l'eau filtrée, un perçage d'eau filtrée (26) relié à la sortie (34) de collecte de chaque plaque (6) de circulation de l'eau filtrée et à l'orifice (26) qui lui correspond percé en regard dans la membrane filtrante (2B) située sous ladite plaque (6) de circulation de l'eau filtrée et un trou traversant d'injection d'air comprimé (37) percé dans la plaque de circulation d'eau filtrée (6) . characterized in that it further comprises means for blowing a stream of pressurized air through the filtered water circulation channel (38) of each filtered water collecting plate (6) through the filtering membrane (2A), in order to take off the micro-algae and to unclog the surface of each filter membrane (2A) on which said micro-algae have accumulated, in that at least one channel (20) of tangential circulation of charged water and at least the channel (38) of filtered water circulation which makes it face each form a spiral, and in that the channel or channels (38) of filtered water circulation are substantially arranged in front of the channel (20) or, respectively, in front of the channel or channels (20) of tangential flow of charged water. 2 - harvesting system according to claim 1, characterized in that the or each subassembly (12) has bores passing through each subassembly and comprising a filled water supply bore (32) made in isolation in each filter membrane (2) and in each plate (6) for circulating the filtered water opposite the supply inlet (22) of the channel (20) of each distribution plate (4), a crop piercing ( 36) of micro-algae connected to the collection outlet (24) of the channel (20) of each distribution plate (4) and to the orifice (36) which corresponds thereto pierced opposite in the adhered filtering membrane (2A) under said plate (4) and in each filtered water circulation plate (6), a filtered water bore (26) connected to the collection outlet (34) of each circulation plate (6) of the filtered water and the orifice (26) corresponding thereto pierced opposite in the filtering membrane (2B) located under said plate (6) d e circulation of the filtered water and a through hole of compressed air injection (37) pierced in the filtered water circulation plate (6).
3 - Système de récolte selon l'une quelconque des revendications 1 et 2, caractérisé en ce que l'extrémité amont ou entrée (30) du canal (38) de circulation d'eau filtrée de la plaque (6) de circulation de l'eau filtrée est située à proximité mais légèrement en retrait de la projection, sur ladite plaque de circulation de l'eau filtrée (6) , de l'alimentation 22 de la plaque de distribution (4) et en ce que l'autre extrémité du canal (38) de circulation d'eau filtrée débouche dans une sortie (34) qui est distincte de la projection (36) , sur ladite plaque (6) de circulation de l'eau filtrée, de la sortie de collecte (24) . 3 - Harvesting system according to any one of claims 1 and 2, characterized in that the upstream end or inlet (30) of the channel (38) filtered water circulation of the plate (6) circulation of the filtered water is located nearby but slightly set back from the projection, on said filtered water circulation plate (6), from the feed 22 of the distribution plate (4) and in that the other end of the filtered water circulation channel (38) opens into an outlet (34) which is distinct from the projection (36) on said circulation plate (6) filtered water, from the collection outlet (24).
4 - Système de récolte selon l'une quelconque des revendications 1 à 3, caractérisé en ce que la première membrane filtrante (2A) est collée sous la plaque de distribution (4) . 4 - Harvesting system according to any one of claims 1 to 3, characterized in that the first filter membrane (2A) is glued under the distribution plate (4).
5 - Système de récolte selon l'une quelconque des revendications 1 à 4, caractérisé en ce que la conduite d'air sous pression traverse de bas en haut le sous-ensemble, en formant une succession de coudes (37) au niveau des plaques de collecte de l'eau filtrée (6) , la conduite d'air sous pression débouchant dans le canal (38) de circulation d'eau filtrée découpé dans chaque plaque (6) de collecte de l'eau filtrée et, à l'inverse, ne débouchant dans aucun canal (20) de circulation d'eau chargée découpé dans chaque plaque (4) de distribution. 5 - harvesting system according to any one of claims 1 to 4, characterized in that the pressurized air duct passes from below upwards the subassembly, forming a succession of bends (37) at the plates for collecting the filtered water (6), the pressurized air duct opening into the channel (38) for circulating filtered water cut from each plate (6) for collecting the filtered water and, at reverse, not opening into any channel (20) charged water circulation cut in each plate (4) distribution.
6 - Système de récolte selon l'une quelconque des revendications 1 à 5, caractérisé en ce que au moins une face de chaque membrane filtrante (2) présente un revêtement d'un matériau présentant un coefficient de frottement extrêmement faible, la face ainsi revêtue étant la face supérieure pour ce qui est de la membrane filtrante (2A) collée à la plaque de distribution (4) et la face inférieure pour ce qui est de la membrane filtrante (2B) collée à la plaque (6) de circulation de l'eau filtrée. 7 - Système de récolte selon l'une quelconque des revendications 1 à 6, caractérisé en ce que l'arrivée d'eau chargée (E) est reliée à une colonne d'eau (46) comportant à son sommet un flotteur (50) . 6 - harvesting system according to any one of claims 1 to 5, characterized in that at least one face of each filter membrane (2) has a coating of a material having an extremely low coefficient of friction, the face thus coated being the upper face with respect to the filter membrane (2A) adhered to the distribution plate (4) and the lower face with respect to the filter membrane (2B) adhered to the circulation plate (6) of the filtered water. 7 - harvesting system according to any one of claims 1 to 6, characterized in that the inflow of charged water (E) is connected to a water column (46) having at its top a float (50) .
PCT/FR2018/000203 2017-08-03 2018-08-03 System for harvesting microalgae and microalga exudates from culture water loaded with same, comprising tangential flow on a membrane filter WO2019025670A1 (en)

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FR1700822A FR3069785A1 (en) 2017-08-03 2017-08-03 MICRO-ALGAE HARVESTING SYSTEM AND MICRO-ALGAE EXUDATES IN CHARGED CULTIVATED WATER, COMPRISING A TANGENTIAL CIRCULATION ON A FILTERING MEMBRANE
FR17.00822 2017-08-03

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