WO2019019519A1 - Ferromagnetic resonance probe - Google Patents

Ferromagnetic resonance probe Download PDF

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Publication number
WO2019019519A1
WO2019019519A1 PCT/CN2017/114902 CN2017114902W WO2019019519A1 WO 2019019519 A1 WO2019019519 A1 WO 2019019519A1 CN 2017114902 W CN2017114902 W CN 2017114902W WO 2019019519 A1 WO2019019519 A1 WO 2019019519A1
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Prior art keywords
disposed
planar waveguide
base
ferromagnetic resonance
resonance probe
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PCT/CN2017/114902
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French (fr)
Chinese (zh)
Inventor
何世坤
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中电海康集团有限公司
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Publication of WO2019019519A1 publication Critical patent/WO2019019519A1/en

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N24/00Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects
    • G01N24/08Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects by using nuclear magnetic resonance
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01RMEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00Arrangements or instruments for measuring magnetic variables
    • G01R33/20Arrangements or instruments for measuring magnetic variables involving magnetic resonance
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01RMEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00Arrangements or instruments for measuring magnetic variables
    • G01R33/20Arrangements or instruments for measuring magnetic variables involving magnetic resonance
    • G01R33/28Details of apparatus provided for in groups G01R33/44 - G01R33/64
    • G01R33/32Excitation or detection systems, e.g. using radio frequency signals
    • G01R33/34Constructional details, e.g. resonators, specially adapted to MR

Definitions

  • the present invention relates to the field of ferromagnetic resonance and, in particular, to a ferromagnetic resonance probe.
  • FIG. 1 to 3 A typical design schematic of a wide-band ferromagnetic resonance in a parallel magnetic field is shown in Figures 1 to 3.
  • the basic components are the back ground plane waveguide 1, the high frequency connector 2, and the electromagnet 3.
  • the back ground plane waveguide generates a high frequency microwave (RF) magnetic field to drive and maintain a small angular precession of the sample 4 magnetic moment. Since the ferromagnetic resonance requires the microwave magnetic field generated by the principle to be perpendicular to the external magnetic field, the waveguide below the sample 4 must be parallel to the external magnetic field; an electromagnet usually has a magnetic pole gap of several inches, and further reduction is required in order to achieve a higher magnetic field.
  • RF microwave
  • the U-shaped planar waveguide 1 is a common design, and the sample 4 corresponding to the planar waveguide 1 is placed in a flipping manner or flipped and then fixed with a non-residual tape 5, so that the film surface is close to the planar waveguide 1 but must be avoided Electrically conductive.
  • the surface of the film sample is generally not parallel to the horizontal plane.
  • the existing ferromagnetic resonance probe is loaded with a sample
  • the above installation is difficult when the sample is mounted in a limited space or the sample is mounted on a plane perpendicular to the horizontal plane.
  • the installation method has poor temperature stability. Since the waveguide is a low thermal conductivity material, when the temperature of the base is significantly different from the ambient temperature, there is a large temperature difference between the sample and the base.
  • the main object of the present invention is to provide a ferromagnetic resonance probe to solve the problem that the sample to be tested which is observed in the prior art of the ferromagnetic resonance probe is inclined to the planar waveguide.
  • the present invention provides a ferromagnetic resonance probe comprising a planar waveguide, the ferromagnetic resonance probe further comprising: a base, the planar waveguide is disposed on the base; the ballast assembly, the ballast assembly is disposed on the base, and the ballast is The assembly has a carrying platform for carrying the sample to be tested, and the carrying platform and the planar waveguide are relatively movably disposed to press the sample to be tested onto the planar waveguide.
  • the ballast assembly includes: a fixing seat disposed on the base to allow the ballast assembly to be disposed on the base through the fixing base; wherein at least a portion of the carrying platform is movably disposed in the fixing seat.
  • the carrying platform includes: a carrying platform for carrying the sample to be tested, the carrying platform is disposed opposite to the planar waveguide, so that the sample to be tested on the carrying platform is attached to the planar waveguide; and the connecting rod and the connecting rod are movably disposed In the mount, the carrier is disposed at one end of the connecting rod adjacent to the planar waveguide such that the carrier is movably disposed relative to the planar waveguide by the connecting rod.
  • the ballast assembly further includes: an elastic member, the elastic member is sleeved on the connecting rod, and the elastic member is disposed between the fixing seat and the carrying platform, so that the carrying platform is close to or away from the planar waveguide under the action of the elastic member.
  • the direction is set retractably.
  • the fixing seat is provided with a mounting hole, and the connecting rod is disposed in the mounting hole;
  • the mounting hole comprises a first hole segment and a second hole segment, and one end of the elastic member is disposed in the second hole segment, and the elastic member is further One end abuts the carrier; wherein the outer peripheral surface of the elastic member is in clearance with the inner wall of the second hole segment.
  • the ballast assembly further includes: a moving handle, one end of the connecting rod is used for connecting with the carrying platform, and the other end of the connecting rod is connected to the moving handle after passing through the mounting hole to drive the connecting rod to move by driving the moving handle.
  • the moving handle is provided with an internal thread
  • the connecting rod has an external thread adapted to the internal thread to screw the moving handle with the connecting rod.
  • the fixing seat is provided with a fastening hole through which the fastener passes, and the fastening hole communicates with the first hole segment to make the fastener abut the connecting rod after passing through the fastening hole.
  • the base includes a support table and a support plate disposed on the support table, and the planar waveguide is disposed on the support plate.
  • the support plate has a first bonding surface for conforming to the planar waveguide, and the first bonding surface is disposed in parallel with the vertical plane.
  • the support plate has a first bonding surface for conforming to the planar waveguide, and the first bonding surface is disposed in parallel with the horizontal plane.
  • the ferromagnetic resonance probe further comprises: a temperature sensing unit, the temperature sensing unit is disposed on the base to determine the temperature of the planar waveguide by monitoring the temperature of the base; the heating component, the heating component is disposed on the base, and the temperature sensing unit A signal is coupled to the heating assembly to control the heating assembly through the temperature sensing unit to change the temperature of the planar waveguide by heating the base.
  • the ferromagnetic resonance probe further includes: a binding post, the binding post is disposed on the base, the binding post has a first terminal group for connecting with the temperature sensing unit, and a connection line for connecting with the heating component
  • the second terminal group is such that the temperature sensing unit and the heating assembly are in communication with the external line through the first terminal group and the second terminal group.
  • the manufacturing materials of the base and the carrying platform are both thermally conductive metal materials, and the outer surface of the carrying platform is coated with a thermal conductive adhesive.
  • the ferromagnetic resonance probe of the invention realizes the flat fitting of the sample to be tested and the plane waveguide through the base and the ballast assembly, wherein the plane waveguide is disposed on the base, the ballast assembly is disposed on the base, and the sample to be tested is set in the ballast
  • the component is on the carrying platform.
  • the sample to be tested is placed on the carrying platform.
  • the carrying platform is relatively movably disposed with the planar waveguide
  • the sample to be tested is placed close to the planar waveguide by moving the carrying platform until the sample to be tested is attached to the planar waveguide.
  • the mobile bearer platform is stopped.
  • the sample to be tested needs to be stabilized on the planar waveguide by the tape, thereby causing the sample to be tested to tilt relative to the planar waveguide, affecting the subsequent test results, and the ferromagnetic resonance probe of the present invention passes through the base and the ballast assembly. It is realized that the sample to be tested is quickly pressed onto the planar waveguide, and the two do not have a relative tilt, thereby solving the problem that the sample to be tested which is observed in the prior art is inclined to the planar waveguide during the detection process.
  • the planar waveguide is a printed circuit board, and the sample is attached to the planar waveguide and has poor thermal conductivity between the base and the base.
  • the ballast assembly of the invention simultaneously establishes a rapid heat transfer path between the sample and the base, solves the heat conduction problem in the prior art, and designs a temperature control component on the probe, which is suitable for the variable temperature ferromagnetic resonance test.
  • Figure 1 is a schematic view showing the structure of a prior art ferromagnetic resonance system
  • FIG. 2 is a schematic view showing an angle between a sample of the prior art and a planar waveguide
  • Figure 3 shows a front view of the sample of Figure 2 and a planar waveguide
  • Figure 4 is an exploded perspective view showing a first embodiment of a ferromagnetic resonance probe according to the present invention
  • Figure 5 is a block diagram showing the structure of a first embodiment of a ferromagnetic resonance probe according to the present invention.
  • Figure 6 is a schematic exploded perspective view showing a second embodiment of a ferromagnetic resonance probe according to the present invention.
  • Figure 7 shows a comparison of the ferromagnetic resonance response of a conventional sample loading and loading using the ferromagnetic resonance probe of the present invention.
  • the present invention provides a ferromagnetic resonance probe.
  • the ferromagnetic resonance probe includes a planar waveguide 10, and the ferromagnetic resonance probe further includes: a base 20, the planar waveguide 10 is disposed on the base 20; and the ballast assembly 30, the ballast assembly 30 is disposed on the base 20, and the ballast assembly 30 has a carrying platform 31 for carrying the sample 40 to be tested.
  • the carrying platform 31 and the planar waveguide 10 are relatively movably disposed to press the sample 40 to be tested.
  • the ferromagnetic resonance probe of the present invention realizes a flat fit of the sample 40 to be tested and the planar waveguide 10 through the base 20 and the ballast assembly 30, wherein the planar waveguide 10 is disposed on the base 20, and the ballast assembly 30 is disposed on the base 20.
  • the sample to be tested 40 is disposed on the carrying platform 31 of the ballast assembly 30.
  • the sample to be tested 40 is placed on the carrying platform 31.
  • the carrying platform 31 is relatively movably disposed with the planar waveguide 10
  • the sample to be tested 40 is moved closer to the planar waveguide 10 by moving the carrying platform 31 until the standby
  • the test sample 40 is attached to the planar waveguide 10, and when the pressure demand is met, the mobile load bearing platform 31 is stopped.
  • the sample 40 to be tested needs to be stabilized on the planar waveguide 10 by tape, thereby causing the sample to be tested to tilt relative to the planar waveguide 10, affecting subsequent test results, and the ferromagnetic resonance probe of the present invention passes through the base 20.
  • the ballast assembly 30 realizes that the sample 40 to be tested is quickly pressed onto the planar waveguide 10 without relative tilting, thereby solving the sample to be tested in the prior art by the ferromagnetic resonance probe during the detection process.
  • the ballast assembly 30 includes a fixing base 32 that is disposed on the base 20 such that the ballast assembly 30 is disposed through the fixing base 32.
  • the base 20 is; wherein at least a portion of the carrying platform 31 is movably disposed within the mount 32.
  • the fixing seat 32 is disposed on the base 20, so that the ballast assembly 30 is disposed on the base 20 through the fixing base 32, in order to be able to be
  • the sample 40 is pressed onto the planar waveguide 10.
  • at least a portion of the carrying platform 31 is movably disposed in the fixing base 32, so that the sample 40 to be tested can be realized by the moving bearing platform 31. Pressing.
  • the carrying platform 31 includes: a carrying platform 311 for carrying a sample to be tested, and the carrying platform 311 is disposed opposite to the planar waveguide 10, so that the sample to be tested on the carrying platform 311 40 is attached to the planar waveguide 10; the connecting rod 312 is movably disposed in the fixing base 32.
  • the carrying platform 311 is disposed at one end of the connecting rod 312 near the planar waveguide 10, so that the carrying platform 311 passes through the connecting rod 312. It is movably disposed with respect to the planar waveguide 10.
  • the carrying platform 31 is composed of a carrying platform 311 and a connecting rod 312.
  • the connecting rod 312 is movably disposed in the fixing base 32.
  • the carrying platform 311 is disposed at one end of the connecting rod 312 near the planar waveguide 10.
  • the sample to be tested 40 is placed on the carrier 311. By placing the carrier 311 opposite to the planar waveguide 10, the sample 40 to be tested on the carrier 311 can be attached to the planar waveguide 10 by moving the connecting rod 312.
  • the ballast assembly 30 further includes: an elastic member 33, the elastic member 33 is sleeved on the connecting rod 312, and the elastic member 33 is disposed between the fixing base 32 and the carrying platform 311 so as to be carried Table 311 in elastic parts
  • the action of 33 is telescopically disposed in a direction toward or away from the planar waveguide 10.
  • the elastic member 33 is disposed on the ballast assembly 30, wherein the elastic member 33 is sleeved on the connecting rod 312, and the elastic member 33 is disposed between the fixing base 32 and the carrying platform 311, so that the elastic member 33 can be expanded and contracted.
  • the carrier 311 is telescopically disposed in a direction toward or away from the planar waveguide 10.
  • the elastic member 33 is a beryllium copper spring having an outer diameter of 5 mm.
  • the fixing base 32 is provided with a mounting hole, and the connecting rod 312 is disposed in the mounting hole;
  • the mounting hole includes a first hole section 321 and a second hole section, and one end of the elastic member 33 is disposed in the second hole section.
  • the other end of the elastic member 33 abuts against the carrier 311; wherein the outer peripheral surface of the elastic member 33 is in clearance with the inner wall of the second hole segment.
  • the outer peripheral surface of the elastic member 33 is clearance-fitted with the inner wall of the second hole section, and since the diameter of the second hole section for mounting the spring is slightly larger than the outer diameter of the spring, the spring will adaptively fine-tune the orientation. Therefore, it can be matched with the surface of the planar waveguide, which is beneficial to ensure that the surface of the sample to be tested 40 and the plane of the planar waveguide 10 are parallel to improve the degree of compression.
  • the ballast assembly 30 further includes a moving handle 34.
  • One end of the connecting rod 312 is connected to the carrying platform 311, and the other end of the connecting rod 312 is connected to the moving handle 34 through the mounting hole to be moved by the driving.
  • the handle 34 moves to drive the connecting rod 312.
  • a moving handle 34 is disposed on the ballast assembly 30, wherein one end of the connecting rod 312 is used for connecting with the carrying platform 311, and the other end of the connecting rod 312 is connected to the moving handle 34 after passing through the mounting hole.
  • the elastic member 33 is compressed by pulling the moving handle 34, and the sample 40 to be tested is away from the planar waveguide 10.
  • the moving handle 34 is released, and the carrying table 311 is released. Moving toward the side close to the planar waveguide 10 by the elastic member 33, the sample 40 to be tested is pressed onto the planar waveguide 10.
  • the moving handle 34 is provided with internal threads, and the connecting rod 312 has an external thread adapted to the internal thread to screw the moving handle 34 with the connecting rod 312.
  • the fixing seat 32 is provided with a fastening hole 322 through which the fastener 35 passes, the fastening hole 322 and the first hole.
  • the segment 321 is in communication such that the fastener 35 passes through the fastening hole 322 and abuts against the connecting rod 312.
  • the base 20 includes a support table 21 and a support plate 22 disposed on the support table 21, and the planar waveguide 10 is disposed on the support plate 22.
  • the support plate 22 has a first bonding surface 221 for conforming to the planar waveguide 10.
  • the first bonding surface 221 is disposed in parallel with the vertical plane.
  • the ballast assembly 30 is disposed on the support table 21, and the planar waveguide 10 is disposed on the support plate 22.
  • the support table 21 is a circular table
  • the support table 21 is horizontally disposed
  • the support plate 22 is disposed perpendicular to the horizontal plane.
  • the planar waveguide 10 is attached to the support plate 22 and disposed perpendicular to the horizontal plane.
  • the surface of the support plate 22 for bonding with the planar waveguide 10 is a first bonding surface 221, and the support table 21 is used for supporting The surface of the first bonding surface of the board 22 is connected to the second surface.
  • the first bonding surface 221 is perpendicular to the second bonding surface 211
  • the first bonding surface 221 is perpendicular to the horizontal plane
  • the second bonding surface 211 is parallel to the horizontal plane.
  • the support plate 22 has a first bonding surface 221 for bonding with the planar waveguide 10, the first bonding surface 221 is arranged in parallel with the horizontal plane.
  • the ballast assembly 30 and the planar waveguide 10 are both disposed on the support plate 22, wherein the support table 21 is a cylindrical table, and the surface of the support plate 22 for bonding with the planar waveguide 10 is the first bonding surface. 221, the surface of the support table 21 for bonding with the support plate 22 is a second bonding surface 211, and the first bonding surface 221 is parallel to the second bonding surface 211, wherein the first bonding surface 221 and the second surface The mating faces 211 are all parallel to the horizontal plane.
  • the ferromagnetic resonance probe further includes: a temperature sensing unit 70, and the temperature sensing unit 70 is disposed on the base 20 to determine the temperature of the planar waveguide 10 by monitoring the temperature of the base 20;
  • the assembly 50, the heating assembly 50 is disposed on the base 20, and the temperature sensing unit 70 is signally coupled to the heating assembly 50 to control the heating assembly 50 through the temperature sensing unit 70 to change the temperature of the planar waveguide 10 by heating the base 20.
  • the ferromagnetic resonance probe further comprises: a terminal 60, the terminal 60 is disposed on the base 20, the terminal 60 has a first terminal group for connecting with the temperature sensing unit 70, and is used for heating The second terminal group of the connection of the component 50 is connected such that the temperature sensing unit 70 and the heating assembly 50 communicate with the external line through the first terminal group and the second terminal group.
  • an insulating alumina gasket is disposed between the planar waveguide 10 and the base 20.
  • the base 20 and the load-bearing platform 31 are made of a thermally conductive metal material, and the outer surface of the load-bearing platform 31 is coated with a thermal conductive adhesive.
  • the base 20 and the load-bearing platform 31 are made of gold-plated copper.
  • the outer dimensions of the ferromagnetic resonance probe of the present invention are designed according to the dimensions of the electromagnet or cryostat, and are guaranteed to match the peripheral equipment. Mounted to the peripheral device or to the stage by screws, wherein the probe base 20 will be used to secure the waveguide assembly, the temperature control unit and the sample loading (ballast assembly 30) assembly.
  • the planar waveguide 10 for the waveguide assembly is U-shaped with a nominal impedance of 50 ohms, by the waveguide by Rogers (RT/ 6010, thickness 254 ⁇ m) printed circuit board, the center conductor is 100 ⁇ m wide, the circuit board is installed with a high-frequency connector 80 through the through hole, and then mounted on the probe base.
  • FIG. 7 is a test result of the sample loading mode and the conventional sample loading mode of the present invention, wherein the dotted line is the test result of the conventional sample loading mode, and the solid line is the test result of the sample loading mode of the present invention.
  • a 2 nm cobalt iron boron (CFB) film sample was used with a microwave frequency of 20 GHz and a power of 0 dBm (1 mW). With this scheme, the height of one ferromagnetic resonance signal is increased by 20% compared with the maximum signal of six ordinary loading tests. In addition, the unique asymmetric peak shape of ferromagnetic resonance is more in line with theoretical expectations in this design.
  • the ferromagnetic resonance spectrum is a relative change curve of the microwave transmission coefficient S21 with the external magnetic field H(Oe) at a fixed frequency. In the absence of magnetic resonance, the microwave transmission coefficient S21 does not vary with the external magnetic field. When the resonance condition is satisfied, the ferromagnetic resonance causes microwave absorption, and the microwave transmission energy is lowered, so that a decrease in S21 occurs.
  • the resonance spectrum can generally be fitted by solving the magnetic moment dynamics equation. The stronger the resonance spectrum signal is, the more accurate the fitting is.
  • the ferromagnetic resonance probe of the present invention realizes a flat fit of the sample 40 to be tested and the planar waveguide 10 through the base 20 and the ballast assembly 30, wherein the planar waveguide 10 is disposed on the base 20, and the ballast assembly 30 is disposed on the base 20.
  • the sample to be tested 40 is disposed on the carrying platform 31 of the ballast assembly 30. During the specific installation process, the sample to be tested 40 is placed on the carrying platform 31.
  • the sample to be tested 40 is moved closer to the planar waveguide 10 by moving the carrying platform 31 until the standby The sample is attached to the planar waveguide 10, and a certain pressure is maintained by the elastic member 33 to ensure that the bonding state does not change with time, the probe temperature, and the probe orientation.
  • the sample 40 to be tested needs to be stabilized on the planar waveguide 10 by the tape, thereby causing the sample to be tested to tilt relative to the planar waveguide 10, and the change of the bonding state during the temperature change process affects the subsequent test results.
  • the ferromagnetic resonance probe of the present invention realizes the rapid pressing of the sample 40 to be tested onto the planar waveguide 10 through the base 20 and the ballast assembly 30, and the two do not appear to be relatively inclined, and are not affected by the measurement conditions and time, thereby solving the problem.
  • the prior art ferromagnetic resonance probe has a problem that the sample to be tested is inclined to the planar waveguide 10 during the detection process.

Abstract

A ferromagnetic resonance probe, comprising a planar waveguide (10). The ferromagnetic resonance probe further comprises: a base (20), the planar waveguide (10) being disposed on the base (20); a pressing and bearing assembly (30) disposed on the base (20) and having a bearing platform (31) used for bearing a sample to be tested (40), the bearing platform (31) and the planar waveguide (10) being movably disposed relative to each other, so as to press the sample to be tested (40) on the planar waveguide (10). The ferromagnetic resonance probe resolves the problem in the prior art it is difficult to prevent the sample to be tested (40) from tilting toward the planar waveguide (10) during the test of the ferromagnetic resonance probe; a channel with high heat conductivity is established between the sample to be tested (40) and the base (20), so as to implement quick and accurate control of the temperature of the sample to be tested (40).

Description

铁磁共振探头Ferromagnetic resonance probe 技术领域Technical field
本发明涉及铁磁共振领域,具体而言,涉及一种铁磁共振探头。The present invention relates to the field of ferromagnetic resonance and, in particular, to a ferromagnetic resonance probe.
背景技术Background technique
现有的平行磁场下宽频铁磁共振的典型设计示意图如图1至图3所示。基本部件为背面接地平面波导1、高频连接头2和电磁铁3。背面接地平面波导生成高频微波(RF)磁场来驱动和维持样品4磁矩的小角度进动。由于铁磁共振在原理上要求产生的微波磁场必须垂直于外部磁场,样品4下方的波导必须与外部磁场平行;一个电磁铁通常具有几英寸的磁极间隙,为了达到更高的磁场,需要进一步减小间隙,因此U型平面波导1为常用设计,和该平面波导1对应的样品4放置方式为翻转样品或翻转后再用无残留胶带5固定,让薄膜膜面紧贴平面波导1但必须避免电导通。A typical design schematic of a wide-band ferromagnetic resonance in a parallel magnetic field is shown in Figures 1 to 3. The basic components are the back ground plane waveguide 1, the high frequency connector 2, and the electromagnet 3. The back ground plane waveguide generates a high frequency microwave (RF) magnetic field to drive and maintain a small angular precession of the sample 4 magnetic moment. Since the ferromagnetic resonance requires the microwave magnetic field generated by the principle to be perpendicular to the external magnetic field, the waveguide below the sample 4 must be parallel to the external magnetic field; an electromagnet usually has a magnetic pole gap of several inches, and further reduction is required in order to achieve a higher magnetic field. A small gap, so the U-shaped planar waveguide 1 is a common design, and the sample 4 corresponding to the planar waveguide 1 is placed in a flipping manner or flipped and then fixed with a non-residual tape 5, so that the film surface is close to the planar waveguide 1 but must be avoided Electrically conductive.
然而,测量中需要调整外磁场相对与薄膜样品平面的相对取向,薄膜样品表面一般不平行于水平面。在此情况下,现有的铁磁共振探头装载样品时,样品表面和背部接地平面波导间很可能存在一个小的夹角,通常需要多次调整胶带5的位置来得到理想的响应曲线。另外,在有限的空间中安装样品或安装样品于垂直于水平面的平面时,上述安装是困难的。再有,该安装方法温度稳定性差,由于波导为低热导材料,当底座温度显著不同于环境温度时,样品和底座之间将存在较大温差。However, in the measurement, it is necessary to adjust the relative orientation of the external magnetic field relative to the plane of the film sample, and the surface of the film sample is generally not parallel to the horizontal plane. In this case, when the existing ferromagnetic resonance probe is loaded with a sample, there is a possibility that there is a small angle between the surface of the sample and the ground plane waveguide of the back, and it is usually necessary to adjust the position of the tape 5 a plurality of times to obtain an ideal response curve. In addition, the above installation is difficult when the sample is mounted in a limited space or the sample is mounted on a plane perpendicular to the horizontal plane. Moreover, the installation method has poor temperature stability. Since the waveguide is a low thermal conductivity material, when the temperature of the base is significantly different from the ambient temperature, there is a large temperature difference between the sample and the base.
其中,上述夹角对测量信号的影响评估如下:由于平面波导1作为特殊印刷电路板,表面偶有曲率和导电镀层导致的小凸起,而且胶带两端压力不一致,样品不可避免的发生小角度倾斜(约1度),如图3所示,样品一侧紧贴波导,而另一侧被抬起。假设样品具有L=5毫米的长度,那么在样品中部样品和波导的间隔d是:The influence of the above angle on the measurement signal is evaluated as follows: Since the planar waveguide 1 is used as a special printed circuit board, the surface has occasional curvature and a small bump caused by the conductive plating, and the pressure at both ends of the tape is inconsistent, and the sample inevitably has a small angle. Tilt (about 1 degree), as shown in Figure 3, one side of the sample is snug against the waveguide and the other side is lifted. Assuming the sample has a length of L = 5 mm, then the interval d between the sample and the waveguide in the middle of the sample is:
Figure PCTCN2017114902-appb-000001
Figure PCTCN2017114902-appb-000001
以平面波导的典型中心导体宽度为S=100微米计算,这会导致样品所处位置p2与波导有44μm的间隙,大致为中心导体宽度的一半。相比紧贴表面的P1位置,由安培定律可知,微波磁场有明面衰减;微波磁场垂直分量比重加大。同样测试条件下,这将导致较弱的信号和引入不同模式的共振响应。Calculated with a typical center conductor width of a planar waveguide of S = 100 microns, this would result in a position of p2 with a gap of 44 μm from the waveguide, roughly half the width of the center conductor. Compared with the P1 position close to the surface, it can be known from Ampere's law that the microwave magnetic field has a bright surface attenuation; the microwave magnetic field has a larger vertical component. Under the same test conditions, this will result in a weaker signal and a resonant response that introduces different modes.
发明内容Summary of the invention
本发明的主要目的在于提供一种铁磁共振探头,以解决现有技术中的铁磁共振探头在检测过程中出现的待测样品倾斜于平面波导的问题。 The main object of the present invention is to provide a ferromagnetic resonance probe to solve the problem that the sample to be tested which is observed in the prior art of the ferromagnetic resonance probe is inclined to the planar waveguide.
为了实现上述目的,本发明提供了一种铁磁共振探头,包括平面波导,铁磁共振探头还包括:底座,平面波导设置在底座上;压载组件,压载组件设置在底座上,压载组件具有用于承载待测样品的承载平台,承载平台和平面波导相对可移动地设置,以将待测样品压合在平面波导上。In order to achieve the above object, the present invention provides a ferromagnetic resonance probe comprising a planar waveguide, the ferromagnetic resonance probe further comprising: a base, the planar waveguide is disposed on the base; the ballast assembly, the ballast assembly is disposed on the base, and the ballast is The assembly has a carrying platform for carrying the sample to be tested, and the carrying platform and the planar waveguide are relatively movably disposed to press the sample to be tested onto the planar waveguide.
进一步地,压载组件包括:固定座,固定座设置在底座上,以使压载组件通过固定座设置在底座上;其中,承载平台的至少部分可移动地穿设在固定座内。Further, the ballast assembly includes: a fixing seat disposed on the base to allow the ballast assembly to be disposed on the base through the fixing base; wherein at least a portion of the carrying platform is movably disposed in the fixing seat.
进一步地,承载平台包括:用于承载待测样品的承载台,承载台与平面波导相对设置,以使承载台上的待测样品与平面波导贴合;连接杆,连接杆可移动地穿设在固定座内,承载台设置在连接杆靠近平面波导的一端,以使承载台通过连接杆相对于平面波导可移动地设置。Further, the carrying platform includes: a carrying platform for carrying the sample to be tested, the carrying platform is disposed opposite to the planar waveguide, so that the sample to be tested on the carrying platform is attached to the planar waveguide; and the connecting rod and the connecting rod are movably disposed In the mount, the carrier is disposed at one end of the connecting rod adjacent to the planar waveguide such that the carrier is movably disposed relative to the planar waveguide by the connecting rod.
进一步地,压载组件还包括:弹性件,弹性件套设在连接杆上,弹性件设置在固定座与承载台之间,以使承载台在弹性件的作用下沿靠近或远离平面波导的方向可伸缩地设置。Further, the ballast assembly further includes: an elastic member, the elastic member is sleeved on the connecting rod, and the elastic member is disposed between the fixing seat and the carrying platform, so that the carrying platform is close to or away from the planar waveguide under the action of the elastic member. The direction is set retractably.
进一步地,固定座上设置有安装孔,连接杆穿设在安装孔内;安装孔包括第一孔段和第二孔段,弹性件的一端穿设在第二孔段内,弹性件的另一端与承载台抵接;其中,弹性件的外周面与第二孔段的内壁间隙配合。Further, the fixing seat is provided with a mounting hole, and the connecting rod is disposed in the mounting hole; the mounting hole comprises a first hole segment and a second hole segment, and one end of the elastic member is disposed in the second hole segment, and the elastic member is further One end abuts the carrier; wherein the outer peripheral surface of the elastic member is in clearance with the inner wall of the second hole segment.
进一步地,压载组件还包括:移动柄,连接杆的一端用于与承载台连接,连接杆的另一端穿过安装孔后与移动柄连接,以通过驱动移动柄以带动连接杆移动。Further, the ballast assembly further includes: a moving handle, one end of the connecting rod is used for connecting with the carrying platform, and the other end of the connecting rod is connected to the moving handle after passing through the mounting hole to drive the connecting rod to move by driving the moving handle.
进一步地,移动柄上设置有内螺纹,连接杆具有与内螺纹相适配的外螺纹,以使移动柄与连接杆螺纹连接。Further, the moving handle is provided with an internal thread, and the connecting rod has an external thread adapted to the internal thread to screw the moving handle with the connecting rod.
进一步地,固定座上设置有供紧固件穿过的紧固孔,紧固孔与第一孔段连通,以使紧固件穿过紧固孔后与连接杆抵接。Further, the fixing seat is provided with a fastening hole through which the fastener passes, and the fastening hole communicates with the first hole segment to make the fastener abut the connecting rod after passing through the fastening hole.
进一步地,底座包括支撑台和设置在支撑台上的支撑板,平面波导设置在支撑板上。Further, the base includes a support table and a support plate disposed on the support table, and the planar waveguide is disposed on the support plate.
进一步地,支撑板具有用于与平面波导相贴合的第一贴合面,第一贴合面与竖直平面平行设置。Further, the support plate has a first bonding surface for conforming to the planar waveguide, and the first bonding surface is disposed in parallel with the vertical plane.
进一步地,支撑板具有用于与平面波导相贴合的第一贴合面,第一贴合面与水平平面平行设置。Further, the support plate has a first bonding surface for conforming to the planar waveguide, and the first bonding surface is disposed in parallel with the horizontal plane.
进一步地,铁磁共振探头还包括:温度传感单元,温度传感单元设置在底座上,以通过监测底座的温度确定平面波导的温度;加热组件,加热组件设置在底座上,温度传感单元与加热组件信号连接,以通过温度传感单元控制加热组件通过加热底座改变平面波导的温度。Further, the ferromagnetic resonance probe further comprises: a temperature sensing unit, the temperature sensing unit is disposed on the base to determine the temperature of the planar waveguide by monitoring the temperature of the base; the heating component, the heating component is disposed on the base, and the temperature sensing unit A signal is coupled to the heating assembly to control the heating assembly through the temperature sensing unit to change the temperature of the planar waveguide by heating the base.
进一步地,铁磁共振探头还包括:接线柱,接线柱设置在底座上,接线柱具有用于与温度传感单元的连接线的第一接线端组,以及用于与加热组件的连接线连接的第二接线端组,以使温度传感单元和加热组件通过第一接线端组和第二接线端组与外部线路连通。 Further, the ferromagnetic resonance probe further includes: a binding post, the binding post is disposed on the base, the binding post has a first terminal group for connecting with the temperature sensing unit, and a connection line for connecting with the heating component The second terminal group is such that the temperature sensing unit and the heating assembly are in communication with the external line through the first terminal group and the second terminal group.
进一步地,底座和承载平台的制作材料均为导热金属材料,承载平台的外表面涂覆有导热胶。Further, the manufacturing materials of the base and the carrying platform are both thermally conductive metal materials, and the outer surface of the carrying platform is coated with a thermal conductive adhesive.
本发明的铁磁共振探头通过底座和压载组件实现了待测样品与平面波导的平整贴合,其中,平面波导设置在底座上,压载组件设置在底座上,待测样品设置在压载组件的承载平台上。在具体安装过程中,将待测样品放置在承载平台上,考虑到承载平台与平面波导相对可移动地设置,通过移动承载平台使得待测样品靠近平面波导,直到待测样品与平面波导贴合,在满足二者压力需求时,停止移动承载平台。The ferromagnetic resonance probe of the invention realizes the flat fitting of the sample to be tested and the plane waveguide through the base and the ballast assembly, wherein the plane waveguide is disposed on the base, the ballast assembly is disposed on the base, and the sample to be tested is set in the ballast The component is on the carrying platform. During the specific installation process, the sample to be tested is placed on the carrying platform. Considering that the carrying platform is relatively movably disposed with the planar waveguide, the sample to be tested is placed close to the planar waveguide by moving the carrying platform until the sample to be tested is attached to the planar waveguide. When the pressure demand of both is met, the mobile bearer platform is stopped.
相比现有技术中,需要通过胶带将待测样品稳定在平面波导上,从而导致待测样品相对平面波导会出现倾斜,影响后续测试结果,本发明的铁磁共振探头通过底座和压载组件实现了将待测样品快速压合到平面波导上,二者不会出现相对倾斜,从而解决了现有技术中的铁磁共振探头在检测过程中出现的待测样品倾斜于平面波导的问题。Compared with the prior art, the sample to be tested needs to be stabilized on the planar waveguide by the tape, thereby causing the sample to be tested to tilt relative to the planar waveguide, affecting the subsequent test results, and the ferromagnetic resonance probe of the present invention passes through the base and the ballast assembly. It is realized that the sample to be tested is quickly pressed onto the planar waveguide, and the two do not have a relative tilt, thereby solving the problem that the sample to be tested which is observed in the prior art is inclined to the planar waveguide during the detection process.
此外,现有技术中,平面波导为印刷电路板,样品贴在平面波导上后和底座间导热差。本发明的压载组件同时建立了样品和底座间的快速传热通道,解决了现有技术中的导热问题,并在探头上设计了温度控制部件,适用于变温铁磁共振测试。In addition, in the prior art, the planar waveguide is a printed circuit board, and the sample is attached to the planar waveguide and has poor thermal conductivity between the base and the base. The ballast assembly of the invention simultaneously establishes a rapid heat transfer path between the sample and the base, solves the heat conduction problem in the prior art, and designs a temperature control component on the probe, which is suitable for the variable temperature ferromagnetic resonance test.
附图说明DRAWINGS
构成本申请的一部分的说明书附图用来提供对本发明的进一步理解,本发明的示意性实施例及其说明用于解释本发明,并不构成对本发明的不当限定。在附图中:The accompanying drawings, which are incorporated in the claims of the claims In the drawing:
图1示出了现有技术的铁磁共振系统结构示意图;Figure 1 is a schematic view showing the structure of a prior art ferromagnetic resonance system;
图2示出了现有技术的样品与平面波导间具有夹角的示意图;2 is a schematic view showing an angle between a sample of the prior art and a planar waveguide;
图3示出了图2的样品与平面波导的主视图;Figure 3 shows a front view of the sample of Figure 2 and a planar waveguide;
图4示出了根据本发明的铁磁共振探头的第一个实施例的分解示意图;Figure 4 is an exploded perspective view showing a first embodiment of a ferromagnetic resonance probe according to the present invention;
图5示出了根据本发明的铁磁共振探头的第一个实施例的结构示意图;Figure 5 is a block diagram showing the structure of a first embodiment of a ferromagnetic resonance probe according to the present invention;
图6示出了根据本发明的铁磁共振探头的第二个实施例的分解结构示意图;以及Figure 6 is a schematic exploded perspective view showing a second embodiment of a ferromagnetic resonance probe according to the present invention;
图7示出了传统样品装载和使用本发明的铁磁共振探头装载的铁磁共振响应对比图。Figure 7 shows a comparison of the ferromagnetic resonance response of a conventional sample loading and loading using the ferromagnetic resonance probe of the present invention.
其中,上述附图包括以下附图标记:Wherein, the above figures include the following reference numerals:
1、平面波导;2、高频连接头;3、电磁铁;4、样品;5、胶带;10、平面波导;20、底座;21、支撑台;211、第二贴合面;22、支撑板;221、第一贴合面;30、压载组件;31、承载平台;311、承载台;312、连接杆;32、固定座;321、第一孔段;322、紧固孔;33、弹性件;34、移动柄;35、紧固件;40、待测样品;50、加热组件;60、接线柱;70、温度传感单元;80、高频接头。 1, plane waveguide; 2, high frequency connector; 3, electromagnet; 4, sample; 5, tape; 10, plane waveguide; 20, base; 21, support table; 211, second bonding surface; Plate; 221, first bonding surface; 30, ballast assembly; 31, carrying platform; 311, carrying platform; 312, connecting rod; 32, fixing seat; 321, first hole section; 322, fastening hole; , elastic member; 34, moving handle; 35, fasteners; 40, sample to be tested; 50, heating components; 60, binding posts; 70, temperature sensing unit; 80, high frequency connector.
具体实施方式Detailed ways
需要说明的是,在不冲突的情况下,本申请中的实施例及实施例中的特征可以相互组合。下面将参考附图并结合实施例来详细说明本发明。It should be noted that the embodiments in the present application and the features in the embodiments may be combined with each other without conflict. The invention will be described in detail below with reference to the drawings in conjunction with the embodiments.
本发明提供了一种铁磁共振探头,请参考图4至图6,铁磁共振探头包括平面波导10,铁磁共振探头还包括:底座20,平面波导10设置在底座20上;压载组件30,压载组件30设置在底座20上,压载组件30具有用于承载待测样品40的承载平台31,承载平台31和平面波导10相对可移动地设置,以将待测样品40压合在平面波导10上。The present invention provides a ferromagnetic resonance probe. Referring to FIG. 4 to FIG. 6, the ferromagnetic resonance probe includes a planar waveguide 10, and the ferromagnetic resonance probe further includes: a base 20, the planar waveguide 10 is disposed on the base 20; and the ballast assembly 30, the ballast assembly 30 is disposed on the base 20, and the ballast assembly 30 has a carrying platform 31 for carrying the sample 40 to be tested. The carrying platform 31 and the planar waveguide 10 are relatively movably disposed to press the sample 40 to be tested. On the planar waveguide 10.
本发明的铁磁共振探头通过底座20和压载组件30实现了待测样品40与平面波导10的平整贴合,其中,平面波导10设置在底座20上,压载组件30设置在底座20上,待测样品40设置在压载组件30的承载平台31上。在具体安装过程中,将待测样品40放置在承载平台31上,考虑到承载平台31与平面波导10相对可移动地设置,通过移动承载平台31使得待测样品40靠近平面波导10,直到待测样品40与平面波导10贴合,在满足二者压力需求时,停止移动承载平台31。The ferromagnetic resonance probe of the present invention realizes a flat fit of the sample 40 to be tested and the planar waveguide 10 through the base 20 and the ballast assembly 30, wherein the planar waveguide 10 is disposed on the base 20, and the ballast assembly 30 is disposed on the base 20. The sample to be tested 40 is disposed on the carrying platform 31 of the ballast assembly 30. During the specific installation process, the sample to be tested 40 is placed on the carrying platform 31. Considering that the carrying platform 31 is relatively movably disposed with the planar waveguide 10, the sample to be tested 40 is moved closer to the planar waveguide 10 by moving the carrying platform 31 until the standby The test sample 40 is attached to the planar waveguide 10, and when the pressure demand is met, the mobile load bearing platform 31 is stopped.
相比现有技术中,需要通过胶带将待测样品40稳定在平面波导10上,从而导致待测样品相对平面波导10会出现倾斜,影响后续测试结果,本发明的铁磁共振探头通过底座20和压载组件30实现了将待测样品40快速压合到平面波导10上,二者不会出现相对倾斜,从而解决了现有技术中的铁磁共振探头在检测过程中出现的待测样品倾斜于平面波导10的问题。Compared with the prior art, the sample 40 to be tested needs to be stabilized on the planar waveguide 10 by tape, thereby causing the sample to be tested to tilt relative to the planar waveguide 10, affecting subsequent test results, and the ferromagnetic resonance probe of the present invention passes through the base 20. And the ballast assembly 30 realizes that the sample 40 to be tested is quickly pressed onto the planar waveguide 10 without relative tilting, thereby solving the sample to be tested in the prior art by the ferromagnetic resonance probe during the detection process. The problem of tilting to the planar waveguide 10.
为了能够将压载组件30设置在底座20上,如图4所示,压载组件30包括:固定座32,固定座32设置在底座20上,以使压载组件30通过固定座32设置在底座20上;其中,承载平台31的至少部分可移动地穿设在固定座32内。In order to be able to mount the ballast assembly 30 on the base 20, as shown in FIG. 4, the ballast assembly 30 includes a fixing base 32 that is disposed on the base 20 such that the ballast assembly 30 is disposed through the fixing base 32. The base 20 is; wherein at least a portion of the carrying platform 31 is movably disposed within the mount 32.
在本实施例中,通过在压载组件30上设置有固定座32,通过将固定座32设置在底座20上,从而使得压载组件30通过固定座32设置在底座20上,为了能够将待测样品40压合在平面波导10上,在本实施例中,承载平台31的至少部分可移动地穿设在固定座32内,从而可以通过移动承载平台31实现待测样品40余平面波导10的压合。In the present embodiment, by providing the fixing seat 32 on the ballast assembly 30, the fixing seat 32 is disposed on the base 20, so that the ballast assembly 30 is disposed on the base 20 through the fixing base 32, in order to be able to be The sample 40 is pressed onto the planar waveguide 10. In this embodiment, at least a portion of the carrying platform 31 is movably disposed in the fixing base 32, so that the sample 40 to be tested can be realized by the moving bearing platform 31. Pressing.
针对承载平台31的具体结构,如图4所示,承载平台31包括:用于承载待测样品的承载台311,承载台311与平面波导10相对设置,以使承载台311上的待测样品40与平面波导10贴合;连接杆312,连接杆312可移动地穿设在固定座32内,承载台311设置在连接杆312靠近平面波导10的一端,以使承载台311通过连接杆312相对于平面波导10可移动地设置。For the specific structure of the carrying platform 31, as shown in FIG. 4, the carrying platform 31 includes: a carrying platform 311 for carrying a sample to be tested, and the carrying platform 311 is disposed opposite to the planar waveguide 10, so that the sample to be tested on the carrying platform 311 40 is attached to the planar waveguide 10; the connecting rod 312 is movably disposed in the fixing base 32. The carrying platform 311 is disposed at one end of the connecting rod 312 near the planar waveguide 10, so that the carrying platform 311 passes through the connecting rod 312. It is movably disposed with respect to the planar waveguide 10.
在本实施例中,承载平台31由承载台311和连接杆312组成,其中,连接杆312可移动地穿设在固定座32内,承载台311设置在连接杆312靠近平面波导10的一端,待测样品40放置在承载台311上,通过将承载台311与平面波导10相对设置,从而可以通过移动连接杆312使承载台311上的待测样品40与平面波导10贴合。In this embodiment, the carrying platform 31 is composed of a carrying platform 311 and a connecting rod 312. The connecting rod 312 is movably disposed in the fixing base 32. The carrying platform 311 is disposed at one end of the connecting rod 312 near the planar waveguide 10. The sample to be tested 40 is placed on the carrier 311. By placing the carrier 311 opposite to the planar waveguide 10, the sample 40 to be tested on the carrier 311 can be attached to the planar waveguide 10 by moving the connecting rod 312.
为了能够实现连接杆312的自动移动,压载组件30还包括:弹性件33,弹性件33套设在连接杆312上,弹性件33设置在固定座32与承载台311之间,以使承载台311在弹性件 33的作用下沿靠近或远离平面波导10的方向可伸缩地设置。通过在压载组件30上设置有弹性件33,其中,弹性件33套设在连接杆312上,弹性件33设置在固定座32与承载台311之间,从而可以通过弹性件33的伸缩使承载台311沿靠近或远离平面波导10的方向可伸缩地设置。In order to enable automatic movement of the connecting rod 312, the ballast assembly 30 further includes: an elastic member 33, the elastic member 33 is sleeved on the connecting rod 312, and the elastic member 33 is disposed between the fixing base 32 and the carrying platform 311 so as to be carried Table 311 in elastic parts The action of 33 is telescopically disposed in a direction toward or away from the planar waveguide 10. The elastic member 33 is disposed on the ballast assembly 30, wherein the elastic member 33 is sleeved on the connecting rod 312, and the elastic member 33 is disposed between the fixing base 32 and the carrying platform 311, so that the elastic member 33 can be expanded and contracted. The carrier 311 is telescopically disposed in a direction toward or away from the planar waveguide 10.
在本实施例中,弹性件33为铍铜弹簧,其外径为5毫米。In the present embodiment, the elastic member 33 is a beryllium copper spring having an outer diameter of 5 mm.
优选地,固定座32上设置有安装孔,连接杆312穿设在安装孔内;安装孔包括第一孔段321和第二孔段,弹性件33的一端穿设在第二孔段内,弹性件33的另一端与承载台311抵接;其中,弹性件33的外周面与第二孔段的内壁间隙配合。Preferably, the fixing base 32 is provided with a mounting hole, and the connecting rod 312 is disposed in the mounting hole; the mounting hole includes a first hole section 321 and a second hole section, and one end of the elastic member 33 is disposed in the second hole section. The other end of the elastic member 33 abuts against the carrier 311; wherein the outer peripheral surface of the elastic member 33 is in clearance with the inner wall of the second hole segment.
在本实施例中,弹性件33的外周面与第二孔段的内壁间隙配合,由于用于安装弹簧的第二孔段直径比弹簧的外径稍大,所以弹簧将自适应地微调方位,从而能够与平面波导表面相匹配,有利于保证待测样品40和平面波导10表面平行,以提高压合度。In the present embodiment, the outer peripheral surface of the elastic member 33 is clearance-fitted with the inner wall of the second hole section, and since the diameter of the second hole section for mounting the spring is slightly larger than the outer diameter of the spring, the spring will adaptively fine-tune the orientation. Therefore, it can be matched with the surface of the planar waveguide, which is beneficial to ensure that the surface of the sample to be tested 40 and the plane of the planar waveguide 10 are parallel to improve the degree of compression.
为了能够方便操作,压载组件30还包括:移动柄34,连接杆312的一端用于与承载台311连接,连接杆312的另一端穿过安装孔后与移动柄34连接,以通过驱动移动柄34以带动连接杆312移动。In order to facilitate the operation, the ballast assembly 30 further includes a moving handle 34. One end of the connecting rod 312 is connected to the carrying platform 311, and the other end of the connecting rod 312 is connected to the moving handle 34 through the mounting hole to be moved by the driving. The handle 34 moves to drive the connecting rod 312.
在本实施例中,通过在压载组件30上设置有移动柄34,其中,连接杆312的一端用于与承载台311连接,连接杆312的另一端穿过安装孔后与移动柄34连接,在需要安装待测样品40时,通过拉动移动柄34,从而使得弹性件33压缩,待测样品40远离平面波导10,在安装好待测样品40后,松开移动柄34,承载台311在弹性件33的作用下向靠近平面波导10的一侧移动,从而实现将待测样品40压合在平面波导10上。In this embodiment, a moving handle 34 is disposed on the ballast assembly 30, wherein one end of the connecting rod 312 is used for connecting with the carrying platform 311, and the other end of the connecting rod 312 is connected to the moving handle 34 after passing through the mounting hole. When the sample to be tested 40 needs to be installed, the elastic member 33 is compressed by pulling the moving handle 34, and the sample 40 to be tested is away from the planar waveguide 10. After the sample 40 to be tested is installed, the moving handle 34 is released, and the carrying table 311 is released. Moving toward the side close to the planar waveguide 10 by the elastic member 33, the sample 40 to be tested is pressed onto the planar waveguide 10.
为了保证安装稳定性,移动柄34上设置有内螺纹,连接杆312具有与内螺纹相适配的外螺纹,以使移动柄34与连接杆312螺纹连接。In order to ensure mounting stability, the moving handle 34 is provided with internal threads, and the connecting rod 312 has an external thread adapted to the internal thread to screw the moving handle 34 with the connecting rod 312.
为了能够在安装或拆卸待测样品40时防止连接杆312移动,如图4所示,固定座32上设置有供紧固件35穿过的紧固孔322,紧固孔322与第一孔段321连通,以使紧固件35穿过紧固孔322后与连接杆312抵接。In order to prevent the connecting rod 312 from moving when the sample 40 to be tested is installed or disassembled, as shown in FIG. 4, the fixing seat 32 is provided with a fastening hole 322 through which the fastener 35 passes, the fastening hole 322 and the first hole. The segment 321 is in communication such that the fastener 35 passes through the fastening hole 322 and abuts against the connecting rod 312.
为了能够方便平面波导10的安装以及方便测试,如图4至6所示,底座20包括支撑台21和设置在支撑台21上的支撑板22,平面波导10设置在支撑板22上。In order to facilitate the mounting of the planar waveguide 10 and facilitate testing, as shown in FIGS. 4 to 6, the base 20 includes a support table 21 and a support plate 22 disposed on the support table 21, and the planar waveguide 10 is disposed on the support plate 22.
针对压载组件30和平面波导10的安装方式的第一个应用实施例,如图4和图5所示,支撑板22具有用于与平面波导10相贴合的第一贴合面221,第一贴合面221与竖直平面平行设置。For the first application embodiment of the mounting manner of the ballast assembly 30 and the planar waveguide 10, as shown in FIGS. 4 and 5, the support plate 22 has a first bonding surface 221 for conforming to the planar waveguide 10. The first bonding surface 221 is disposed in parallel with the vertical plane.
在本实施例中,压载组件30设置在支撑台21上,平面波导10设置在支撑板22上,其中,支撑台21为圆形台,支撑台21水平设置,支撑板22垂直于水平面设置,其中,平面波导10贴合在支撑板22上,相对于水平面垂直设置,其中,支撑板22用于与平面波导10贴合的表面为第一贴合面221,支撑台21用于与支撑板22的第一贴合面连接的表面为第二贴合 面211,第一贴合面221垂直于第二贴合面211,第一贴合面221垂直于水平面,第二贴合面211平行于水平面。In this embodiment, the ballast assembly 30 is disposed on the support table 21, and the planar waveguide 10 is disposed on the support plate 22. wherein the support table 21 is a circular table, the support table 21 is horizontally disposed, and the support plate 22 is disposed perpendicular to the horizontal plane. The planar waveguide 10 is attached to the support plate 22 and disposed perpendicular to the horizontal plane. The surface of the support plate 22 for bonding with the planar waveguide 10 is a first bonding surface 221, and the support table 21 is used for supporting The surface of the first bonding surface of the board 22 is connected to the second surface. The first bonding surface 221 is perpendicular to the second bonding surface 211, the first bonding surface 221 is perpendicular to the horizontal plane, and the second bonding surface 211 is parallel to the horizontal plane.
针对压载组件30和平面波导10的安装方式的第二个应用实施例,如图6,支撑板22具有用于与平面波导10相贴合的第一贴合面221,第一贴合面221与水平平面平行设置。For a second application embodiment of the mounting manner of the ballast assembly 30 and the planar waveguide 10, as shown in FIG. 6, the support plate 22 has a first bonding surface 221 for bonding with the planar waveguide 10, the first bonding surface 221 is arranged in parallel with the horizontal plane.
在本实施例中,压载组件30和平面波导10均设置在支撑板22上,其中,支撑台21为圆柱台,支撑板22用于与平面波导10贴合的表面为第一贴合面221,支撑台21用于与支撑板22的贴合的表面为第二贴合面211,第一贴合面221平行于第二贴合面211,其中,第一贴合面221和第二贴合面211均平行于水平面。In this embodiment, the ballast assembly 30 and the planar waveguide 10 are both disposed on the support plate 22, wherein the support table 21 is a cylindrical table, and the surface of the support plate 22 for bonding with the planar waveguide 10 is the first bonding surface. 221, the surface of the support table 21 for bonding with the support plate 22 is a second bonding surface 211, and the first bonding surface 221 is parallel to the second bonding surface 211, wherein the first bonding surface 221 and the second surface The mating faces 211 are all parallel to the horizontal plane.
为了实现变温测试,如图4所示,铁磁共振探头还包括:温度传感单元70,温度传感单元70设置在底座20上,以通过监测底座20的温度确定平面波导10的温度;加热组件50,加热组件50设置在底座20上,温度传感单元70与加热组件50信号连接,以通过温度传感单元70控制加热组件50通过加热底座20改变平面波导10的温度。In order to realize the temperature change test, as shown in FIG. 4, the ferromagnetic resonance probe further includes: a temperature sensing unit 70, and the temperature sensing unit 70 is disposed on the base 20 to determine the temperature of the planar waveguide 10 by monitoring the temperature of the base 20; The assembly 50, the heating assembly 50 is disposed on the base 20, and the temperature sensing unit 70 is signally coupled to the heating assembly 50 to control the heating assembly 50 through the temperature sensing unit 70 to change the temperature of the planar waveguide 10 by heating the base 20.
优选地,铁磁共振探头还包括:接线柱60,接线柱60设置在底座20上,接线柱60具有用于与温度传感单元70的连接线的第一接线端组,以及用于与加热组件50的连接线连接的第二接线端组,以使温度传感单元70和加热组件50通过第一接线端组和第二接线端组与外部线路连通。Preferably, the ferromagnetic resonance probe further comprises: a terminal 60, the terminal 60 is disposed on the base 20, the terminal 60 has a first terminal group for connecting with the temperature sensing unit 70, and is used for heating The second terminal group of the connection of the component 50 is connected such that the temperature sensing unit 70 and the heating assembly 50 communicate with the external line through the first terminal group and the second terminal group.
在本实施例中,平面波导10和底座20之间设置有绝缘氧化铝垫片。In the present embodiment, an insulating alumina gasket is disposed between the planar waveguide 10 and the base 20.
为了能够提供待测样品40和底座20的热传导能力,底座20和承载平台31的制作材料均为导热金属材料,承载平台31的外表面涂覆有导热胶。In order to provide the heat transfer capability of the sample to be tested 40 and the base 20, the base 20 and the load-bearing platform 31 are made of a thermally conductive metal material, and the outer surface of the load-bearing platform 31 is coated with a thermal conductive adhesive.
常用导热金属材料如铝、铜、金、银等,在本实施例中,底座20和承载平台31的制作材料均为镀金铜。Commonly used thermally conductive metal materials such as aluminum, copper, gold, silver, etc., in this embodiment, the base 20 and the load-bearing platform 31 are made of gold-plated copper.
针对本发明的铁磁共振探头的具体结构以及使用过程进行说明:The specific structure and use process of the ferromagnetic resonance probe of the present invention are described:
本发明的铁磁共振探头的外围尺寸按照电磁体或低温恒温器相关尺寸设计,保障与外围设备相匹配。通过螺丝装载到外围设备或者选择台上,其中,探头底座20将用于固定波导组件,温度控制单元和样品装载(压载组件30)组件。The outer dimensions of the ferromagnetic resonance probe of the present invention are designed according to the dimensions of the electromagnet or cryostat, and are guaranteed to match the peripheral equipment. Mounted to the peripheral device or to the stage by screws, wherein the probe base 20 will be used to secure the waveguide assembly, the temperature control unit and the sample loading (ballast assembly 30) assembly.
针对波导组件的平面波导10为U形,具有50欧姆的标称阻抗,由波导由罗杰斯(RT/
Figure PCTCN2017114902-appb-000002
6010,厚度为254μm)印刷电路板加工而成,中心导体为100μm宽,电路板上做通孔安装高频接头80,然后整体安装到探针底座上。
The planar waveguide 10 for the waveguide assembly is U-shaped with a nominal impedance of 50 ohms, by the waveguide by Rogers (RT/
Figure PCTCN2017114902-appb-000002
6010, thickness 254μm) printed circuit board, the center conductor is 100μm wide, the circuit board is installed with a high-frequency connector 80 through the through hole, and then mounted on the probe base.
对于温度控制单元由温度传感器(温度传感单元70)、加热丝(加热组件50)和接线柱60组成。所有加工部件均采用镀金铜块,具高热传导系数k。因此具有小的温度控制的响应特征时间t=C/k,其中C是系统热容量。当加热器处于工作状态时波导和传感器之间的温度差将被最小化。 The temperature control unit is composed of a temperature sensor (temperature sensing unit 70), a heating wire (heating assembly 50), and a terminal 60. All machined parts are gold-plated copper with a high thermal conductivity k. Therefore, the response characteristic time t=C/k with small temperature control, where C is the system heat capacity. The temperature difference between the waveguide and the sensor will be minimized when the heater is in operation.
如图7为本发明的的样品装载方式和传统样品装载方式的测试结果,其中,点化线为传统样品装载方式的测试结果,实线为本发明的的样品装载方式的测试结果。采用2纳米钴铁硼(CFB)薄膜样品,微波频率为20GHz,功率为0dBm(1mW)。采用本方案装载方式,其一次铁磁共振信号高度比六次普通装载测试的最大信号增加了20%。另外铁磁共振的特有非对称峰形在本设计中也更符合理论预期。7 is a test result of the sample loading mode and the conventional sample loading mode of the present invention, wherein the dotted line is the test result of the conventional sample loading mode, and the solid line is the test result of the sample loading mode of the present invention. A 2 nm cobalt iron boron (CFB) film sample was used with a microwave frequency of 20 GHz and a power of 0 dBm (1 mW). With this scheme, the height of one ferromagnetic resonance signal is increased by 20% compared with the maximum signal of six ordinary loading tests. In addition, the unique asymmetric peak shape of ferromagnetic resonance is more in line with theoretical expectations in this design.
铁磁共振谱为固定频率下,微波透射系数S21随外磁场H(Oe)的相对变化曲线。在没有磁共振的情况下,微波透射系数S21不随外磁场变化。当共振条件满足时,铁磁共振导致微波吸收,微波透射能量降低,因而出现S21的降低。共振谱一般可以通过求解磁矩动力学方程拟合,在材料一定的情况下,共振谱信号越强,拟合越准确。The ferromagnetic resonance spectrum is a relative change curve of the microwave transmission coefficient S21 with the external magnetic field H(Oe) at a fixed frequency. In the absence of magnetic resonance, the microwave transmission coefficient S21 does not vary with the external magnetic field. When the resonance condition is satisfied, the ferromagnetic resonance causes microwave absorption, and the microwave transmission energy is lowered, so that a decrease in S21 occurs. The resonance spectrum can generally be fitted by solving the magnetic moment dynamics equation. The stronger the resonance spectrum signal is, the more accurate the fitting is.
从以上的描述中,可以看出,本发明上述的实施例实现了如下技术效果:From the above description, it can be seen that the above-described embodiments of the present invention achieve the following technical effects:
本发明的铁磁共振探头通过底座20和压载组件30实现了待测样品40与平面波导10的平整贴合,其中,平面波导10设置在底座20上,压载组件30设置在底座20上,待测样品40设置在压载组件30的承载平台31上。在具体安装过程中,将待测样品40放置在承载平台31上,考虑到承载平台31与平面波导10相对可移动地设置,通过移动承载平台31使得待测样品40靠近平面波导10,直到待测样品与平面波导10贴合,通过弹性件33维持一定压力,保证二者贴合状态不随时间,探头温度,以及探头方位变化。The ferromagnetic resonance probe of the present invention realizes a flat fit of the sample 40 to be tested and the planar waveguide 10 through the base 20 and the ballast assembly 30, wherein the planar waveguide 10 is disposed on the base 20, and the ballast assembly 30 is disposed on the base 20. The sample to be tested 40 is disposed on the carrying platform 31 of the ballast assembly 30. During the specific installation process, the sample to be tested 40 is placed on the carrying platform 31. Considering that the carrying platform 31 is relatively movably disposed with the planar waveguide 10, the sample to be tested 40 is moved closer to the planar waveguide 10 by moving the carrying platform 31 until the standby The sample is attached to the planar waveguide 10, and a certain pressure is maintained by the elastic member 33 to ensure that the bonding state does not change with time, the probe temperature, and the probe orientation.
相比现有技术中,需要通过胶带将待测样品40稳定在平面波导10上,从而导致待测样品相对平面波导10会出现倾斜,在变温过程中出现贴合状态变化等影响后续测试结果,本发明的铁磁共振探头通过底座20和压载组件30实现了将待测样品40快速压合到平面波导10上,二者不会出现相对倾斜,不受测量条件和时间影响,从而解决了现有技术中的铁磁共振探头在检测过程中出现的待测样品倾斜于平面波导10的问题。Compared with the prior art, the sample 40 to be tested needs to be stabilized on the planar waveguide 10 by the tape, thereby causing the sample to be tested to tilt relative to the planar waveguide 10, and the change of the bonding state during the temperature change process affects the subsequent test results. The ferromagnetic resonance probe of the present invention realizes the rapid pressing of the sample 40 to be tested onto the planar waveguide 10 through the base 20 and the ballast assembly 30, and the two do not appear to be relatively inclined, and are not affected by the measurement conditions and time, thereby solving the problem. The prior art ferromagnetic resonance probe has a problem that the sample to be tested is inclined to the planar waveguide 10 during the detection process.
以上所述仅为本发明的优选实施例而已,并不用于限制本发明,对于本领域的技术人员来说,本发明可以有各种更改和变化。凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。 The above description is only the preferred embodiment of the present invention, and is not intended to limit the present invention, and various modifications and changes can be made to the present invention. Any modifications, equivalent substitutions, improvements, etc. made within the spirit and scope of the present invention are intended to be included within the scope of the present invention.

Claims (14)

  1. 一种铁磁共振探头,包括平面波导(10),其特征在于,所述铁磁共振探头还包括:A ferromagnetic resonance probe comprising a planar waveguide (10), characterized in that the ferromagnetic resonance probe further comprises:
    底座(20),所述平面波导(10)设置在所述底座(20)上;a base (20), the planar waveguide (10) is disposed on the base (20);
    压载组件(30),所述压载组件(30)设置在所述底座(20)上,所述压载组件(30)具有用于承载待测样品(40)的承载平台(31),所述承载平台(31)和所述平面波导(10)相对可移动地设置,以将所述待测样品(40)压合在所述平面波导(10)上。a ballast assembly (30), the ballast assembly (30) being disposed on the base (20), the ballast assembly (30) having a load bearing platform (31) for carrying a sample (40) to be tested, The carrying platform (31) and the planar waveguide (10) are relatively movably disposed to press the sample to be tested (40) onto the planar waveguide (10).
  2. 根据权利要求1所述的铁磁共振探头,其特征在于,所述压载组件(30)包括:The ferromagnetic resonance probe of claim 1 wherein said ballast assembly (30) comprises:
    固定座(32),所述固定座(32)设置在所述底座(20)上,以使所述压载组件(30)通过所述固定座(32)设置在所述底座(20)上;其中,所述承载平台(31)的至少部分可移动地穿设在所述固定座(32)内。a fixing seat (32), the fixing seat (32) is disposed on the base (20), so that the ballast assembly (30) is disposed on the base (20) through the fixing base (32) Wherein at least a portion of the carrier platform (31) is movably disposed within the mount (32).
  3. 根据权利要求2所述的铁磁共振探头,其特征在于,所述承载平台(31)包括:The ferromagnetic resonance probe according to claim 2, wherein the carrying platform (31) comprises:
    用于承载所述待测样品的承载台(311),所述承载台(311)与所述平面波导(10)相对设置,以使所述承载台(311)上的待测样品(40)与所述平面波导(10)贴合;a carrying platform (311) for carrying the sample to be tested, the carrying platform (311) is disposed opposite to the planar waveguide (10), so that the sample to be tested (40) on the carrying platform (311) Bonding with the planar waveguide (10);
    连接杆(312),所述连接杆(312)可移动地穿设在所述固定座(32)内,所述承载台(311)设置在所述连接杆(312)靠近所述平面波导(10)的一端,以使所述承载台(311)通过所述连接杆(312)相对于所述平面波导(10)可移动地设置。a connecting rod (312), the connecting rod (312) is movably disposed in the fixing base (32), and the carrying platform (311) is disposed on the connecting rod (312) adjacent to the planar waveguide ( One end of 10) is such that the carrier (311) is movably disposed relative to the planar waveguide (10) through the connecting rod (312).
  4. 根据权利要求3所述的铁磁共振探头,其特征在于,所述压载组件(30)还包括:The ferromagnetic resonance probe according to claim 3, wherein the ballast assembly (30) further comprises:
    弹性件(33),所述弹性件(33)套设在所述连接杆(312)上,所述弹性件(33)设置在所述固定座(32)与所述承载台(311)之间,以使所述承载台(311)在弹性件(33)的作用下沿靠近或远离所述平面波导(10)的方向可伸缩地设置。An elastic member (33), the elastic member (33) is sleeved on the connecting rod (312), and the elastic member (33) is disposed on the fixing base (32) and the carrying platform (311) In order to enable the carrying platform (311) to be telescopically disposed in the direction of being close to or away from the planar waveguide (10) by the elastic member (33).
  5. 根据权利要求4所述的铁磁共振探头,其特征在于,所述固定座(32)上设置有安装孔,所述连接杆(312)穿设在所述安装孔内;所述安装孔包括第一孔段(321)和第二孔段,所述弹性件(33)的一端穿设在所述第二孔段内,所述弹性件(33)的另一端与所述承载台(311)抵接;其中,所述弹性件(33)的外周面与所述第二孔段的内壁间隙配合。The ferromagnetic resonance probe according to claim 4, wherein the fixing base (32) is provided with a mounting hole, and the connecting rod (312) is disposed in the mounting hole; the mounting hole comprises a first hole section (321) and a second hole section, one end of the elastic member (33) is disposed in the second hole section, and the other end of the elastic member (33) is opposite to the carrying platform (311) Abutting; wherein an outer peripheral surface of the elastic member (33) is in clearance fit with an inner wall of the second hole segment.
  6. 根据权利要求5所述的铁磁共振探头,其特征在于,所述压载组件(30)还包括:The ferromagnetic resonance probe according to claim 5, wherein the ballast assembly (30) further comprises:
    移动柄(34),所述连接杆(312)的一端用于与所述承载台(311)连接,所述连接杆(312)的另一端穿过所述安装孔后与所述移动柄(34)连接,以通过驱动所述移动柄(34)以带动所述连接杆(312)移动。Moving the handle (34), one end of the connecting rod (312) is for connecting with the carrying platform (311), and the other end of the connecting rod (312) passes through the mounting hole and the moving handle ( 34) connecting to drive the connecting rod (312) to move by driving the moving handle (34).
  7. 根据权利要求6所述的铁磁共振探头,其特征在于,所述移动柄(34)上设置有内螺纹,所述连接杆(312)具有与所述内螺纹相适配的外螺纹,以使所述移动柄(34)与所述连接杆(312)螺纹连接。 The ferromagnetic resonance probe according to claim 6, wherein the moving handle (34) is provided with an internal thread, and the connecting rod (312) has an external thread adapted to the internal thread, The moving handle (34) is threadedly coupled to the connecting rod (312).
  8. 根据权利要求6所述的铁磁共振探头,其特征在于,所述固定座(32)上设置有供紧固件(35)穿过的紧固孔(322),所述紧固孔(322)与所述第一孔段(321)连通,以使所述紧固件(35)穿过所述紧固孔(322)后与所述连接杆(312)抵接。The ferromagnetic resonance probe according to claim 6, wherein the fixing base (32) is provided with a fastening hole (322) through which the fastener (35) passes, the fastening hole (322) And communicating with the first hole section (321) such that the fastener (35) abuts the connecting rod (312) after passing through the fastening hole (322).
  9. 根据权利要求1所述的铁磁共振探头,其特征在于,所述底座(20)包括支撑台(21)和设置在所述支撑台(21)上的支撑板(22),所述平面波导(10)设置在所述支撑板(22)上。The ferromagnetic resonance probe according to claim 1, wherein the base (20) comprises a support table (21) and a support plate (22) disposed on the support table (21), the planar waveguide (10) is disposed on the support plate (22).
  10. 根据权利要求9所述的铁磁共振探头,其特征在于,所述支撑板(22)具有用于与所述平面波导(10)相贴合的第一贴合面(221),所述第一贴合面(221)与竖直平面平行设置。The ferromagnetic resonance probe according to claim 9, wherein said support plate (22) has a first bonding surface (221) for conforming to said planar waveguide (10), said A mating surface (221) is disposed in parallel with the vertical plane.
  11. 根据权利要求9所述的铁磁共振探头,其特征在于,所述支撑板(22)具有用于与所述平面波导(10)相贴合的第一贴合面(221),所述第一贴合面(221)与水平平面平行设置。The ferromagnetic resonance probe according to claim 9, wherein said support plate (22) has a first bonding surface (221) for conforming to said planar waveguide (10), said A mating surface (221) is disposed in parallel with the horizontal plane.
  12. 根据权利要求1所述的铁磁共振探头,其特征在于,所述铁磁共振探头还包括:The ferromagnetic resonance probe according to claim 1, wherein the ferromagnetic resonance probe further comprises:
    温度传感单元(70),所述温度传感单元(70)设置在所述底座(20)上,以通过监测所述底座(20)的温度确定所述平面波导(10)的温度;a temperature sensing unit (70), the temperature sensing unit (70) is disposed on the base (20) to determine a temperature of the planar waveguide (10) by monitoring a temperature of the base (20);
    加热组件(50),所述加热组件(50)设置在所述底座(20)上,所述温度传感单元(70)与所述加热组件(50)信号连接,以通过所述温度传感单元(70)控制所述加热组件(50)通过加热所述底座(20)改变所述平面波导(10)的温度。a heating assembly (50) disposed on the base (20), the temperature sensing unit (70) being signally coupled to the heating assembly (50) for sensing by the temperature The unit (70) controls the heating assembly (50) to change the temperature of the planar waveguide (10) by heating the base (20).
  13. 根据权利要求12所述的铁磁共振探头,其特征在于,所述铁磁共振探头还包括:The ferromagnetic resonance probe according to claim 12, wherein the ferromagnetic resonance probe further comprises:
    接线柱(60),所述接线柱(60)设置在所述底座(20)上,所述接线柱(60)具有用于与所述温度传感单元(70)的连接线的第一接线端组,以及用于与所述加热组件(50)的连接线连接的第二接线端组,以使所述温度传感单元(70)和所述加热组件(50)通过所述第一接线端组和所述第二接线端组与外部线路连通。a terminal (60) disposed on the base (20), the terminal (60) having a first connection for a connection with the temperature sensing unit (70) An end set, and a second set of terminals for connection to a connection line of the heating assembly (50) to pass the temperature sensing unit (70) and the heating assembly (50) through the first wiring The end group and the second terminal group are in communication with an external line.
  14. 根据权利要求1所述的铁磁共振探头,其特征在于,所述底座(20)和所述承载平台(31)的制作材料均为导热金属材料,所述承载平台(31)的外表面涂覆有导热胶。 The ferromagnetic resonance probe according to claim 1, wherein the base (20) and the bearing platform (31) are made of a thermally conductive metal material, and the outer surface of the bearing platform (31) is coated. Covered with thermal paste.
PCT/CN2017/114902 2017-07-24 2017-12-07 Ferromagnetic resonance probe WO2019019519A1 (en)

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CN203658564U (en) * 2013-12-11 2014-06-18 广州赛宝计量检测中心服务有限公司 Sample adjustment frame for measurement of ferromagnetic resonance parameters
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